2026-07-11T23:30:13Zhttp://localhost:3000{"from"=>"2022-08-01T14:15:00Z", "until"=>"2022-09-01T14:20:00Z", "metadataPrefix"=>"oai_dc", "verb"=>"ListRecords"}

10.14272/FERUHHWVLZNKMW-UHFFFAOYSA-N/CHMO0000595.22022-08-11T20:02:11Zpublicationpublication:datasets

13C nuclear magnetic resonance spectroscopy (13C NMR) (6,13-dimethyl-6,13-diazatetracyclo[6.6.2.04,16.011,15]hexadeca-1(15),2,4(16),8,10-pentaene-5,7,12,14-tetrone)Krämer, JoanaChemistry dataset for 13C nuclear magnetic resonance spectroscopy (13C NMR) 13C NMR (126 Hz, chloroform-d1, ppm) δ = 163.3 (4Cq), 131.2 (4Cq), 126.8 (2Cq), 126.8 (4CH), 27.6 (2CH3). chemotion.net2022-08-1110.14272/FERUHHWVLZNKMW-UHFFFAOYSA-N/CHMO0000595.2chemotionenhttps://dx.doi.org/10.14272/FERUHHWVLZNKMW-UHFFFAOYSA-N.3Attribution-ShareAlike 4.0 International (CC BY-SA 4.0)

10.14272/FERUHHWVLZNKMW-UHFFFAOYSA-N.32022-08-11T20:02:11Zpublicationpublication:samples

6,13-dimethyl-6,13-diazatetracyclo[6.6.2.04,16.011,15]hexadeca-1(15),2,4(16),8,10-pentaene-5,7,12,14-tetroneKrämer, JoanaChemistry This dataset contains experimental data from a sample (6,13-dimethyl-6,13-diazatetracyclo[6.6.2.04,16.011,15]hexadeca-1(15),2,4(16),8,10-pentaene-5,7,12,14-tetrone, InChI=1S/C16H10N2O4/c1-17-13(19)7-3-5-9-12-10(16(22)18(2)15(9)21)6-4-8(11(7)12)14(17)20/h3-6H,1-2H3). The datasets from the following experiments are available: 1H nuclear magnetic resonance spectroscopy (1H NMR) 13C nuclear magnetic resonance spectroscopy (13C NMR) chemotion.net2022-08-1110.14272/FERUHHWVLZNKMW-UHFFFAOYSA-N.3chemotionenhttps://dx.doi.org/10.14272/FERUHHWVLZNKMW-UHFFFAOYSA-N/CHMO0000593.2https://dx.doi.org/10.14272/FERUHHWVLZNKMW-UHFFFAOYSA-N/CHMO0000595.2https://dx.doi.org/10.14272/reaction/SA-FUHFF-UHFFFADPSC-FERUHHWVLZ-UHFFFADPSC-NUHFF-NUHFF-NUHFF-ZZZ.1Attribution-ShareAlike 4.0 International (CC BY-SA 4.0)

10.14272/FERUHHWVLZNKMW-UHFFFAOYSA-N/CHMO0000593.22022-08-11T20:02:11Zpublicationpublication:datasets

1H nuclear magnetic resonance spectroscopy (1H NMR) (6,13-dimethyl-6,13-diazatetracyclo[6.6.2.04,16.011,15]hexadeca-1(15),2,4(16),8,10-pentaene-5,7,12,14-tetrone)Krämer, JoanaChemistry dataset for 1H nuclear magnetic resonance spectroscopy (1H NMR) 1H NMR (500 MHz, chloroform-d1, ppm) δ = 8.78 (s, 4H, H-Ar), 3.61 (s, 6H, CH3). chemotion.net2022-08-1110.14272/FERUHHWVLZNKMW-UHFFFAOYSA-N/CHMO0000593.2chemotionenhttps://dx.doi.org/10.14272/FERUHHWVLZNKMW-UHFFFAOYSA-N.3Attribution-ShareAlike 4.0 International (CC BY-SA 4.0)

10.14272/reaction/SA-FUHFF-UHFFFADPSC-FERUHHWVLZ-UHFFFADPSC-NUHFF-NUHFF-NUHFF-ZZZ.12022-08-11T20:02:10Zpublicationpublication:reactions

Short-RInChIKey=SA-FUHFF-UHFFFADPSC-FERUHHWVLZ-UHFFFADPSC-NUHFF-NUHFF-NUHFF-ZZZKrämer, Joanachemical reaction: structures conditions A three-neck flask equipped with a reflux condenser was filled with 120 mL aqueous methylamine (40.0 wt%, 1.39 mol, 74.6 eq) and 5.00 g of 1,4,5,8‑naphtalenetetracarboxylic dianhydride (18.6 mmol, 1.00 eq) were slowly added under vigorous stirring. The orange-brown solution was refluxed at 100 °C for 3 h, cooled down to 25 °C and stirred for 2 days. The formed precipitate was collected by filtration, washed with 100 mL of methanol and dried in vacuo. The product was isolated as a nude-coloured solid with a yield of 56 % (3.09 g, 10.5 mmol). chemotion.net2022-08-1110.14272/reaction/SA-FUHFF-UHFFFADPSC-FERUHHWVLZ-UHFFFADPSC-NUHFF-NUHFF-NUHFF-ZZZ.1chemotionenhttps://dx.doi.org/10.14272/FERUHHWVLZNKMW-UHFFFAOYSA-N.3https://dx.doi.org/10.1021/ja00128a015Attribution-ShareAlike 4.0 International (CC BY-SA 4.0)

10.14272/JMHFTDFPRQWUAN-UHFFFAOYSA-H.192022-08-10T07:16:45Zpublicationpublication:samples

dicopper;benzene-1,3,5-tricarboxylatePilz, LenaChemistry This dataset contains experimental data from a sample (dicopper;benzene-1,3,5-tricarboxylate, InChI=1S/2C9H6O6.2Cu/c2*10-7(11)4-1-5(8(12)13)3-6(2-4)9(14)15;;/h2*1-3H,(H,10,11)(H,12,13)(H,14,15);;/q;;2*+2/p-6). The datasets from the following experiments are available: X-ray diffraction (XRD) X-ray diffraction (XRD) single crystal X-ray diffraction (single-crystal X-ray diffraction) chemotion.net2022-08-1010.14272/JMHFTDFPRQWUAN-UHFFFAOYSA-H.19chemotionenhttps://dx.doi.org/10.14272/JMHFTDFPRQWUAN-UHFFFAOYSA-H/CHMO0000156.35https://dx.doi.org/10.14272/JMHFTDFPRQWUAN-UHFFFAOYSA-H/CHMO0000159.17https://dx.doi.org/10.14272/JMHFTDFPRQWUAN-UHFFFAOYSA-H/CHMO0000156.36https://dx.doi.org/10.14272/reaction/SA-FUHFF-UHFFFADPSC-JMHFTDFPRQ-UHFFFADPSC-NUHFF-HUHFF-NUHFF-ZZZ.18Attribution-ShareAlike 4.0 International (CC BY-SA 4.0)

10.14272/JMHFTDFPRQWUAN-UHFFFAOYSA-H.152022-08-10T07:16:45Zpublicationpublication:samples

dicopper;benzene-1,3,5-tricarboxylatePilz, LenaChemistry This dataset contains experimental data from a sample (dicopper;benzene-1,3,5-tricarboxylate, InChI=1S/2C9H6O6.2Cu/c2*10-7(11)4-1-5(8(12)13)3-6(2-4)9(14)15;;/h2*1-3H,(H,10,11)(H,12,13)(H,14,15);;/q;;2*+2/p-6). The datasets from the following experiments are available: X-ray diffraction (XRD) X-ray diffraction (XRD) single crystal X-ray diffraction (single-crystal X-ray diffraction) chemotion.net2022-08-1010.14272/JMHFTDFPRQWUAN-UHFFFAOYSA-H.15chemotionenhttps://dx.doi.org/10.14272/JMHFTDFPRQWUAN-UHFFFAOYSA-H/CHMO0000156.28https://dx.doi.org/10.14272/JMHFTDFPRQWUAN-UHFFFAOYSA-H/CHMO0000156.27https://dx.doi.org/10.14272/JMHFTDFPRQWUAN-UHFFFAOYSA-H/CHMO0000159.13https://dx.doi.org/10.14272/reaction/SA-FUHFF-UHFFFADPSC-JMHFTDFPRQ-UHFFFADPSC-NUHFF-HUHFF-NUHFF-ZZZ.14Attribution-ShareAlike 4.0 International (CC BY-SA 4.0)

10.14272/JMHFTDFPRQWUAN-UHFFFAOYSA-H.132022-08-10T07:16:45Zpublicationpublication:samples

dicopper;benzene-1,3,5-tricarboxylatePilz, LenaChemistry This dataset contains experimental data from a sample (dicopper;benzene-1,3,5-tricarboxylate, InChI=1S/2C9H6O6.2Cu/c2*10-7(11)4-1-5(8(12)13)3-6(2-4)9(14)15;;/h2*1-3H,(H,10,11)(H,12,13)(H,14,15);;/q;;2*+2/p-6). The datasets from the following experiments are available: X-ray diffraction (XRD) X-ray diffraction (XRD) single crystal X-ray diffraction (single-crystal X-ray diffraction) chemotion.net2022-08-1010.14272/JMHFTDFPRQWUAN-UHFFFAOYSA-H.13chemotionenhttps://dx.doi.org/10.14272/JMHFTDFPRQWUAN-UHFFFAOYSA-H/CHMO0000156.24https://dx.doi.org/10.14272/JMHFTDFPRQWUAN-UHFFFAOYSA-H/CHMO0000156.23https://dx.doi.org/10.14272/JMHFTDFPRQWUAN-UHFFFAOYSA-H/CHMO0000159.11https://dx.doi.org/10.14272/reaction/SA-FUHFF-UHFFFADPSC-JMHFTDFPRQ-UHFFFADPSC-NUHFF-HUHFF-NUHFF-ZZZ.12Attribution-ShareAlike 4.0 International (CC BY-SA 4.0)

10.14272/JMHFTDFPRQWUAN-UHFFFAOYSA-H.182022-08-10T07:16:45Zpublicationpublication:samples

dicopper;benzene-1,3,5-tricarboxylatePilz, LenaChemistry This dataset contains experimental data from a sample (dicopper;benzene-1,3,5-tricarboxylate, InChI=1S/2C9H6O6.2Cu/c2*10-7(11)4-1-5(8(12)13)3-6(2-4)9(14)15;;/h2*1-3H,(H,10,11)(H,12,13)(H,14,15);;/q;;2*+2/p-6). The datasets from the following experiments are available: X-ray diffraction (XRD) X-ray diffraction (XRD) single crystal X-ray diffraction (single-crystal X-ray diffraction) chemotion.net2022-08-1010.14272/JMHFTDFPRQWUAN-UHFFFAOYSA-H.18chemotionenhttps://dx.doi.org/10.14272/JMHFTDFPRQWUAN-UHFFFAOYSA-H/CHMO0000156.33https://dx.doi.org/10.14272/JMHFTDFPRQWUAN-UHFFFAOYSA-H/CHMO0000159.16https://dx.doi.org/10.14272/JMHFTDFPRQWUAN-UHFFFAOYSA-H/CHMO0000156.34https://dx.doi.org/10.14272/reaction/SA-FUHFF-UHFFFADPSC-JMHFTDFPRQ-UHFFFADPSC-NUHFF-HUHFF-NUHFF-ZZZ.17Attribution-ShareAlike 4.0 International (CC BY-SA 4.0)

10.14272/JMHFTDFPRQWUAN-UHFFFAOYSA-H.212022-08-10T07:16:45Zpublicationpublication:samples

dicopper;benzene-1,3,5-tricarboxylatePilz, LenaChemistry This dataset contains experimental data from a sample (dicopper;benzene-1,3,5-tricarboxylate, InChI=1S/2C9H6O6.2Cu/c2*10-7(11)4-1-5(8(12)13)3-6(2-4)9(14)15;;/h2*1-3H,(H,10,11)(H,12,13)(H,14,15);;/q;;2*+2/p-6). The datasets from the following experiments are available: X-ray diffraction (XRD) X-ray diffraction (XRD) single crystal X-ray diffraction (single-crystal X-ray diffraction) chemotion.net2022-08-1010.14272/JMHFTDFPRQWUAN-UHFFFAOYSA-H.21chemotionenhttps://dx.doi.org/10.14272/JMHFTDFPRQWUAN-UHFFFAOYSA-H/CHMO0000156.40https://dx.doi.org/10.14272/JMHFTDFPRQWUAN-UHFFFAOYSA-H/CHMO0000156.39https://dx.doi.org/10.14272/JMHFTDFPRQWUAN-UHFFFAOYSA-H/CHMO0000159.20https://dx.doi.org/10.14272/reaction/SA-FUHFF-UHFFFADPSC-JMHFTDFPRQ-UHFFFADPSC-NUHFF-HUHFF-NUHFF-ZZZ.20Attribution-ShareAlike 4.0 International (CC BY-SA 4.0)

10.14272/JMHFTDFPRQWUAN-UHFFFAOYSA-H.202022-08-10T07:16:45Zpublicationpublication:samples

dicopper;benzene-1,3,5-tricarboxylatePilz, LenaChemistry This dataset contains experimental data from a sample (dicopper;benzene-1,3,5-tricarboxylate, InChI=1S/2C9H6O6.2Cu/c2*10-7(11)4-1-5(8(12)13)3-6(2-4)9(14)15;;/h2*1-3H,(H,10,11)(H,12,13)(H,14,15);;/q;;2*+2/p-6). The datasets from the following experiments are available: X-ray diffraction (XRD) X-ray diffraction (XRD) single crystal X-ray diffraction (single-crystal X-ray diffraction) chemotion.net2022-08-1010.14272/JMHFTDFPRQWUAN-UHFFFAOYSA-H.20chemotionenhttps://dx.doi.org/10.14272/JMHFTDFPRQWUAN-UHFFFAOYSA-H/CHMO0000159.18https://dx.doi.org/10.14272/JMHFTDFPRQWUAN-UHFFFAOYSA-H/CHMO0000156.37https://dx.doi.org/10.14272/JMHFTDFPRQWUAN-UHFFFAOYSA-H/CHMO0000156.38https://dx.doi.org/10.14272/reaction/SA-FUHFF-UHFFFADPSC-JMHFTDFPRQ-UHFFFADPSC-NUHFF-HUHFF-NUHFF-ZZZ.19Attribution-ShareAlike 4.0 International (CC BY-SA 4.0)oai_dc.f(2022-08-01T14:15:00Z).u(2022-09-01T14:20:00Z):10