data_global _audit_creation_method 'SHELXL-2018/3' # 1. Submission Details _publ_contact_author_name 'Michael E. Tauchert' _publ_contact_author_address ; Institut f\"ur Anorganische Chemie RWTH Aachen University Landoltweg 1 52074 Aachen Germany ; _publ_contact_author_email 'michael.tauchert@ac.rwth-aachen.de' _publ_contact_author_fax '' _publ_contact_author_phone '0049-241-8094648' _publ_requested_journal 'Chemical Communications' _publ_requested_category ? _publ_requested_coeditor_name ? _publ_contact_letter ; ? ; # 2. Processing Summary (IUCr Office Use Only) _journal_date_recd_electronic ? _journal_date_to_coeditor ? _journal_date_from_coeditor ? _journal_date_accepted ? _journal_date_printers_first ? _journal_date_printers_final ? _journal_date_proofs_out ? _journal_date_proofs_in ? _journal_coeditor_name ? _journal_coeditor_code ? _journal_coeditor_notes ; ? ; _journal_techeditor_code ? _journal_techeditor_notes ; ? ; _journal_coden_ASTM ? _journal_name_full ? _journal_year ? _journal_volume ? _journal_issue ? _journal_page_first ? _journal_page_last ? _journal_suppl_publ_number ? _journal_suppl_publ_pages ? # 3. Titl and Author List _publ_section_title ; ? ; # The loop structure below should contain the names and addresses of all # authors, in the required order of publication. Repeat as necessary. loop_ _publ_author_name _publ_author_address 'Eltester, M. Alexander' ; Institut f\"ur Anorganische Chemie RWTH Aachen University Landoltweg 1 52074 Aachen Germany ; 'Claudia Roth' ; Institut f\"ur Anorganische Chemie RWTH Aachen University Landoltweg 1 52074 Aachen Germany ; 'Tauchert, Michael E.' ; Institut f\"ur Anorganische Chemie RWTH Aachen University Landoltweg 1 52074 Aachen Germany ; # 4. Text _publ_section_abstract ; ? ; _publ_section_comment ; ? ; _publ_section_exptl_prep ; ? ; _publ_section_exptl_refinement ; ? ; _publ_section_references ; ? ; _publ_section_figure_captions ; ? ; _publ_section_table_legends ; ? ; _publ_section_acknowledgements ; ? ; data_[AuFe(L)] _audit_creation_method 'SHELXL-2018/3' _shelx_SHELXL_version_number '2018/3' _chemical_name_systematic ? _chemical_name_common '[AuFe(L)]' _chemical_melting_point ? _chemical_formula_moiety ; C44 H36 Au F6 Fe N5 O4 P2 S2, 2(C2 F6 N O4 S2), C7 H8, C H2 Cl2 ; _chemical_formula_sum 'C56 H46 Au Cl2 F18 Fe N7 O12 P2 S6' _chemical_formula_weight 1929.01 loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source 'C' 'C' 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 'H' 'H' 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 'N' 'N' 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 'O' 'O' 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 'F' 'F' 0.0171 0.0103 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 'P' 'P' 0.1023 0.0942 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 'S' 'S' 0.1246 0.1234 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 'Cl' 'Cl' 0.1484 0.1585 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 'Fe' 'Fe' 0.3463 0.8444 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 'Au' 'Au' -2.0133 8.8022 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' _space_group_crystal_system monoclinic _space_group_IT_number 14 _space_group_name_H-M_alt 'P 21/c' _space_group_name_Hall '-P 2ybc' _shelx_space_group_comment ; The symmetry employed for this shelxl refinement is uniquely defined by the following loop, which should always be used as a source of symmetry information in preference to the above space-group names. They are only intended as comments. ; loop_ _space_group_symop_operation_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' _cell_length_a 22.1627(6) _cell_length_b 13.3594(3) _cell_length_c 24.6684(6) _cell_angle_alpha 90 _cell_angle_beta 106.2350(10) _cell_angle_gamma 90 _cell_volume 7012.6(3) _cell_formula_units_Z 4 _cell_measurement_temperature 100(2) _cell_measurement_reflns_used 9981 _cell_measurement_theta_min 2.30 _cell_measurement_theta_max 26.34 _exptl_crystal_description 'block' _exptl_crystal_colour 'yellow' _exptl_crystal_density_meas ? _exptl_crystal_density_method ? _exptl_crystal_density_diffrn 1.827 _exptl_crystal_F_000 3816 _exptl_transmission_factor_min ? _exptl_transmission_factor_max ? _exptl_crystal_size_max 0.150 _exptl_crystal_size_mid 0.150 _exptl_crystal_size_min 0.150 _exptl_absorpt_coefficient_mu 2.709 _shelx_estimated_absorpt_T_min 0.687 _shelx_estimated_absorpt_T_max 0.687 _exptl_absorpt_correction_type 'multi-scan' _exptl_absorpt_correction_T_min 0.4617 _exptl_absorpt_correction_T_max 0.6465 _exptl_absorpt_process_details 'SADABS' _exptl_absorpt_special_details ? _diffrn_ambient_temperature 100(2) _diffrn_radiation_wavelength 0.71073 _diffrn_radiation_type MoK\a _diffrn_source ? _diffrn_measurement_device_type 'CCD area detector' _diffrn_measurement_method 'omega scans' _diffrn_detector_area_resol_mean ? _diffrn_reflns_number 123049 _diffrn_reflns_av_unetI/netI 0.0426 _diffrn_reflns_av_R_equivalents 0.0751 _diffrn_reflns_limit_h_min -27 _diffrn_reflns_limit_h_max 27 _diffrn_reflns_limit_k_min -16 _diffrn_reflns_limit_k_max 16 _diffrn_reflns_limit_l_min -30 _diffrn_reflns_limit_l_max 30 _diffrn_reflns_theta_min 1.718 _diffrn_reflns_theta_max 26.373 _diffrn_reflns_theta_full 25.242 _diffrn_measured_fraction_theta_max 0.999 _diffrn_measured_fraction_theta_full 1.000 _diffrn_reflns_Laue_measured_fraction_max 0.999 _diffrn_reflns_Laue_measured_fraction_full 1.000 _diffrn_reflns_point_group_measured_fraction_max 0.999 _diffrn_reflns_point_group_measured_fraction_full 1.000 _reflns_number_total 14346 _reflns_number_gt 13149 _reflns_threshold_expression 'I > 2\s(I)' _reflns_Friedel_coverage 0.000 _reflns_Friedel_fraction_max . _reflns_Friedel_fraction_full . _reflns_special_details ; Reflections were merged by SHELXL according to the crystal class for the calculation of statistics and refinement. _reflns_Friedel_fraction is defined as the number of unique Friedel pairs measured divided by the number that would be possible theoretically, ignoring centric projections and systematic absences. ; _computing_data_collection 'SMART (Bruker, 2001)' _computing_cell_refinement 'SMART' _computing_data_reduction 'SAINT-PLUS (Bruker, 2009)' _computing_structure_solution 'SHELXT 2018/2 (Sheldrick, 2018)' _computing_structure_refinement 'SHELXL-2018/3 (Sheldrick, 2018)' _computing_molecular_graphics 'PLATON (Spek, 2009)' _computing_publication_material 'SHELXL2018' _refine_special_details ? _refine_ls_structure_factor_coef Fsqd _refine_ls_matrix_type full _refine_ls_weighting_scheme calc _refine_ls_weighting_details 'w=1/[\s^2^(Fo^2^)+(0.0288P)^2^+21.0056P] where P=(Fo^2^+2Fc^2^)/3' _atom_sites_solution_primary dual _atom_sites_solution_secondary ? _atom_sites_solution_hydrogens geom _refine_ls_hydrogen_treatment constr _refine_ls_extinction_method none _refine_ls_extinction_coef . _refine_ls_number_reflns 14346 _refine_ls_number_parameters 1122 _refine_ls_number_restraints 348 _refine_ls_R_factor_all 0.0400 _refine_ls_R_factor_gt 0.0368 _refine_ls_wR_factor_ref 0.0888 _refine_ls_wR_factor_gt 0.0874 _refine_ls_goodness_of_fit_ref 1.114 _refine_ls_restrained_S_all 1.108 _refine_ls_shift/su_max 0.002 _refine_ls_shift/su_mean 0.000 loop_ _atom_site_label _atom_site_type_symbol _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_occupancy _atom_site_site_symmetry_order _atom_site_calc_flag _atom_site_refinement_flags_posn _atom_site_refinement_flags_adp _atom_site_refinement_flags_occupancy _atom_site_disorder_assembly _atom_site_disorder_group Au1 Au 0.20339(2) 0.36895(2) 0.37105(2) 0.01114(5) Uani 1 1 d . . . . . Fe1 Fe 0.23562(2) 0.37387(4) 0.27523(2) 0.01314(11) Uani 1 1 d . . . . . Cl1 Cl 0.47778(5) 0.63569(8) 0.52107(5) 0.0339(2) Uani 1 1 d . . . . . Cl2 Cl 0.40969(7) 0.82423(10) 0.51245(6) 0.0472(3) Uani 1 1 d . . . . . S5 S 0.16931(4) 0.31851(7) 0.50508(4) 0.01927(19) Uani 1 1 d . . . . . P1 P 0.10540(4) 0.33153(7) 0.31113(4) 0.01237(18) Uani 1 1 d . . . . . P2 P 0.30989(4) 0.39146(7) 0.41343(4) 0.01219(18) Uani 1 1 d . . . . . F13 F 0.19112(15) 0.4692(2) 0.57433(12) 0.0463(7) Uani 1 1 d . . . . . F14 F 0.09343(15) 0.4492(3) 0.52888(13) 0.0584(10) Uani 1 1 d . . . . . F15 F 0.13726(15) 0.3504(3) 0.59808(12) 0.0538(9) Uani 1 1 d . . . . . O9 O 0.22312(14) 0.2663(2) 0.53829(12) 0.0265(6) Uani 1 1 d . . . . . O10 O 0.17819(14) 0.3891(2) 0.46331(12) 0.0251(6) Uani 1 1 d . . . . . N1 N 0.14635(14) 0.4230(2) 0.23151(12) 0.0132(6) Uani 1 1 d . . . . . N2 N 0.31935(13) 0.4468(2) 0.31096(12) 0.0129(6) Uani 1 1 d . . . . . N3 N 0.25956(14) 0.2368(2) 0.24814(13) 0.0157(6) Uani 1 1 d . . . . . N4 N 0.25364(14) 0.4226(2) 0.19821(12) 0.0143(6) Uani 1 1 d . . . . . C1 C 0.03738(16) 0.3501(3) 0.33678(15) 0.0147(7) Uani 1 1 d . . . . . C2 C 0.03987(17) 0.4264(3) 0.37559(16) 0.0178(8) Uani 1 1 d . . . . . H2 H 0.076298 0.467214 0.387634 0.021 Uiso 1 1 calc R U . . . C3 C -0.01089(19) 0.4427(3) 0.39653(17) 0.0239(9) Uani 1 1 d . . . . . H3 H -0.009479 0.494651 0.423168 0.029 Uiso 1 1 calc R U . . . C4 C -0.06409(19) 0.3829(3) 0.37854(18) 0.0235(9) Uani 1 1 d . . . . . H4 H -0.098983 0.393899 0.393056 0.028 Uiso 1 1 calc R U . . . C5 C -0.06646(18) 0.3068(3) 0.33930(17) 0.0231(8) Uani 1 1 d . . . . . H5 H -0.103045 0.266510 0.326924 0.028 Uiso 1 1 calc R U . . . C6 C -0.01540(17) 0.2900(3) 0.31831(16) 0.0191(8) Uani 1 1 d . . . . . H6 H -0.016617 0.238132 0.291685 0.023 Uiso 1 1 calc R U . . . C7 C 0.10747(16) 0.2016(3) 0.29083(15) 0.0151(7) Uani 1 1 d . . . . . C8 C 0.1248(2) 0.1320(3) 0.33411(18) 0.0237(9) Uani 1 1 d . . . . . H8 H 0.130912 0.152257 0.372180 0.028 Uiso 1 1 calc R U . . . C9 C 0.1331(2) 0.0326(3) 0.32158(19) 0.0256(9) Uani 1 1 d . . . . . H9 H 0.144342 -0.015243 0.351176 0.031 Uiso 1 1 calc R U . . . C10 C 0.12525(19) 0.0029(3) 0.26678(19) 0.0259(9) Uani 1 1 d . . . . . H10 H 0.132053 -0.064996 0.258662 0.031 Uiso 1 1 calc R U . . . C11 C 0.1074(2) 0.0719(3) 0.22335(19) 0.0302(10) Uani 1 1 d . . . . . H11 H 0.101584 0.051173 0.185390 0.036 Uiso 1 1 calc R U . . . C12 C 0.0980(2) 0.1713(3) 0.23526(17) 0.0245(9) Uani 1 1 d . . . . . H12 H 0.085215 0.218481 0.205442 0.029 Uiso 1 1 calc R U . . . C13 C 0.32784(16) 0.4573(3) 0.47954(15) 0.0139(7) Uani 1 1 d . . . . . C14 C 0.29490(17) 0.5465(3) 0.48072(16) 0.0181(8) Uani 1 1 d . . . . . H14 H 0.265439 0.570261 0.447399 0.022 Uiso 1 1 calc R U . . . C15 C 0.30550(19) 0.6000(3) 0.53078(17) 0.0226(8) Uani 1 1 d . . . . . H15 H 0.283770 0.660955 0.531718 0.027 Uiso 1 1 calc R U . . . C16 C 0.3476(2) 0.5643(3) 0.57901(17) 0.0245(9) Uani 1 1 d . . . . . H16 H 0.354748 0.601427 0.613062 0.029 Uiso 1 1 calc R U . . . C17 C 0.38002(19) 0.4747(3) 0.57902(16) 0.0220(8) Uani 1 1 d . . . . . H17 H 0.408206 0.450337 0.612884 0.026 Uiso 1 1 calc R U . . . C18 C 0.37059(18) 0.4217(3) 0.52890(15) 0.0186(8) Uani 1 1 d . . . . . H18 H 0.393057 0.361403 0.528108 0.022 Uiso 1 1 calc R U . . . C19 C 0.34961(17) 0.2715(3) 0.42276(15) 0.0161(7) Uani 1 1 d . . . . . C20 C 0.39005(18) 0.2455(3) 0.39114(17) 0.0197(8) Uani 1 1 d . . . . . H20 H 0.400153 0.293189 0.366486 0.024 Uiso 1 1 calc R U . . . C21 C 0.41600(18) 0.1496(3) 0.3953(2) 0.0262(9) Uani 1 1 d . . . . . H21 H 0.444372 0.132264 0.374239 0.031 Uiso 1 1 calc R U . . . C22 C 0.3999(2) 0.0799(3) 0.4306(2) 0.0359(11) Uani 1 1 d . . . . . H22 H 0.416396 0.013935 0.432903 0.043 Uiso 1 1 calc R U . . . C23 C 0.3604(3) 0.1060(4) 0.4619(2) 0.0368(11) Uani 1 1 d . . . . . H23 H 0.350596 0.057877 0.486545 0.044 Uiso 1 1 calc R U . . . C24 C 0.3343(2) 0.2011(3) 0.45879(19) 0.0277(9) Uani 1 1 d . . . . . H24 H 0.306607 0.217991 0.480636 0.033 Uiso 1 1 calc R U . . . C25 C 0.09277(17) 0.4041(3) 0.24584(15) 0.0145(7) Uani 1 1 d . . . . . C26 C 0.03488(18) 0.4373(3) 0.21374(16) 0.0205(8) Uani 1 1 d . . . . . H26 H -0.002060 0.423927 0.224840 0.025 Uiso 1 1 calc R U . . . C27 C 0.03190(19) 0.4911(3) 0.16444(16) 0.0230(8) Uani 1 1 d . . . . . H27 H -0.007344 0.514738 0.141401 0.028 Uiso 1 1 calc R U . . . C28 C 0.08662(17) 0.5097(3) 0.14944(16) 0.0178(8) Uani 1 1 d . . . . . H28 H 0.085280 0.545802 0.115929 0.021 Uiso 1 1 calc R U . . . C29 C 0.14349(17) 0.4750(3) 0.18406(15) 0.0143(7) Uani 1 1 d . . . . . C30 C 0.20535(17) 0.4988(3) 0.17240(15) 0.0160(7) Uani 1 1 d . . . . . H30A H 0.199333 0.500770 0.131110 0.019 Uiso 1 1 calc R U . . . H30B H 0.219997 0.565628 0.187948 0.019 Uiso 1 1 calc R U . . . C31 C 0.34618(16) 0.4611(3) 0.36711(15) 0.0135(7) Uani 1 1 d . . . . . C32 C 0.39952(17) 0.5179(3) 0.38682(17) 0.0192(8) Uani 1 1 d . . . . . H32 H 0.416980 0.528199 0.426205 0.023 Uiso 1 1 calc R U . . . C33 C 0.42769(18) 0.5601(3) 0.34836(17) 0.0228(8) Uani 1 1 d . . . . . H33 H 0.464437 0.600031 0.361022 0.027 Uiso 1 1 calc R U . . . C34 C 0.40119(18) 0.5429(3) 0.29150(17) 0.0201(8) Uani 1 1 d . . . . . H34 H 0.420289 0.569754 0.264664 0.024 Uiso 1 1 calc R U . . . C35 C 0.34656(17) 0.4864(3) 0.27342(15) 0.0145(7) Uani 1 1 d . . . . . C36 C 0.31865(17) 0.4633(3) 0.21185(16) 0.0185(8) Uani 1 1 d . . . . . H36A H 0.318262 0.525341 0.189775 0.022 Uiso 1 1 calc R U . . . H36B H 0.345881 0.414216 0.199946 0.022 Uiso 1 1 calc R U . . . C37 C 0.27394(19) 0.1526(3) 0.27957(16) 0.0199(8) Uani 1 1 d . . . . . H37 H 0.267611 0.151178 0.316094 0.024 Uiso 1 1 calc R U . . . C38 C 0.2975(2) 0.0686(3) 0.26001(18) 0.0260(9) Uani 1 1 d . . . . . H38 H 0.307324 0.010138 0.282677 0.031 Uiso 1 1 calc R U . . . C39 C 0.3067(2) 0.0712(3) 0.20671(18) 0.0277(9) Uani 1 1 d . . . . . H39 H 0.322813 0.014231 0.192374 0.033 Uiso 1 1 calc R U . . . C40 C 0.29222(19) 0.1574(3) 0.17449(17) 0.0215(8) Uani 1 1 d . . . . . H40 H 0.298782 0.160631 0.138084 0.026 Uiso 1 1 calc R U . . . C41 C 0.26800(17) 0.2388(3) 0.19624(15) 0.0168(7) Uani 1 1 d . . . . . C42 C 0.24621(18) 0.3319(3) 0.16152(15) 0.0171(7) Uani 1 1 d . . . . . H42A H 0.270983 0.340518 0.134087 0.021 Uiso 1 1 calc R U . . . H42B H 0.201489 0.324319 0.140023 0.021 Uiso 1 1 calc R U . . . C47 C 0.1463(2) 0.4014(4) 0.55479(18) 0.0346(11) Uani 1 1 d . . . . . C49 C 0.4648(2) 0.7545(4) 0.4890(2) 0.0354(11) Uani 1 1 d . . . . . H49A H 0.505032 0.791608 0.497638 0.042 Uiso 1 1 calc R U . . . H49B H 0.449442 0.746224 0.447482 0.042 Uiso 1 1 calc R U . . . C50A C 0.2176(7) -0.0074(9) 0.4859(5) 0.070(4) Uani 0.650(13) 1 d D . P A 1 H50A H 0.239149 -0.030368 0.458457 0.105 Uiso 0.650(13) 1 calc R U P A 1 H50B H 0.235998 0.056092 0.502485 0.105 Uiso 0.650(13) 1 calc R U P A 1 H50C H 0.172861 0.002181 0.466874 0.105 Uiso 0.650(13) 1 calc R U P A 1 C51A C 0.2250(3) -0.0838(5) 0.5313(2) 0.036(2) Uani 0.650(13) 1 d DG U P A 1 C52A C 0.2841(2) -0.0994(6) 0.5687(3) 0.045(3) Uani 0.650(13) 1 d G U P A 1 H52A H 0.318863 -0.060554 0.565559 0.054 Uiso 0.650(13) 1 calc R U P A 1 C53A C 0.2923(3) -0.1719(7) 0.6105(3) 0.058(3) Uani 0.650(13) 1 d G U P A 1 H53A H 0.332706 -0.182624 0.636007 0.070 Uiso 0.650(13) 1 calc R U P A 1 C54A C 0.2414(5) -0.2288(5) 0.6150(3) 0.075(3) Uani 0.650(13) 1 d G U P A 1 H54A H 0.247061 -0.278399 0.643646 0.090 Uiso 0.650(13) 1 calc R U P A 1 C55A C 0.1823(4) -0.2132(6) 0.5777(4) 0.065(3) Uani 0.650(13) 1 d G U P A 1 H55A H 0.147571 -0.252106 0.580837 0.078 Uiso 0.650(13) 1 calc R U P A 1 C56A C 0.1741(2) -0.1407(7) 0.5359(3) 0.051(3) Uani 0.650(13) 1 d G U P A 1 H56A H 0.133727 -0.130035 0.510389 0.061 Uiso 0.650(13) 1 calc R U P A 1 C50B C 0.2563(9) -0.0337(13) 0.5114(8) 0.047(5) Uiso 0.350(13) 1 d D U P A 2 H50D H 0.217059 -0.011867 0.484426 0.070 Uiso 0.350(13) 1 calc R U P A 2 H50E H 0.284276 -0.062016 0.490861 0.070 Uiso 0.350(13) 1 calc R U P A 2 H50F H 0.276786 0.023731 0.533818 0.070 Uiso 0.350(13) 1 calc R U P A 2 C51B C 0.2425(5) -0.1096(8) 0.5488(5) 0.024(3) Uiso 0.350(13) 1 d DG U P A 2 C52B C 0.2902(4) -0.1456(8) 0.5939(5) 0.020(3) Uiso 0.350(13) 1 d G U P A 2 H52B H 0.331869 -0.121041 0.600348 0.024 Uiso 0.350(13) 1 calc R U P A 2 C53B C 0.2770(3) -0.2175(8) 0.6297(4) 0.019(3) Uiso 0.350(13) 1 d G U P A 2 H53B H 0.309660 -0.242168 0.660558 0.023 Uiso 0.350(13) 1 calc R U P A 2 C54B C 0.2161(4) -0.2535(7) 0.6203(4) 0.022(3) Uiso 0.350(13) 1 d G U P A 2 H54B H 0.207106 -0.302656 0.644761 0.026 Uiso 0.350(13) 1 calc R U P A 2 C55B C 0.1684(3) -0.2175(10) 0.5752(5) 0.024(3) Uiso 0.350(13) 1 d G U P A 2 H55B H 0.126761 -0.242020 0.568756 0.029 Uiso 0.350(13) 1 calc R U P A 2 C56B C 0.1816(4) -0.1455(10) 0.5394(5) 0.024(4) Uiso 0.350(13) 1 d G U P A 2 H56B H 0.148969 -0.120894 0.508545 0.029 Uiso 0.350(13) 1 calc R U P A 2 C43 C 0.2968(2) 0.7932(4) 0.3523(2) 0.0384(11) Uani 1 1 d D . . . . F1 F 0.35395(16) 0.8053(3) 0.34418(15) 0.0602(9) Uani 1 1 d D . . . . F2 F 0.30234(15) 0.7249(2) 0.39243(12) 0.0490(8) Uani 1 1 d D . . . . F3 F 0.28013(15) 0.8797(2) 0.37001(13) 0.0461(7) Uani 1 1 d D . . . . S1 S 0.24088(6) 0.75522(9) 0.28594(5) 0.0371(3) Uani 1 1 d D . . . . O1 O 0.24183(19) 0.8370(3) 0.24878(15) 0.0464(9) Uani 1 1 d D . . . . O2 O 0.2627(2) 0.6593(3) 0.27386(17) 0.0562(11) Uani 1 1 d D . . . . N5 N 0.17504(19) 0.7548(3) 0.29873(16) 0.0339(9) Uani 1 1 d D . . . . S2 S 0.14649(7) 0.66376(8) 0.32388(5) 0.0416(3) Uani 1 1 d D . . . . O3 O 0.0866(2) 0.6366(3) 0.28791(19) 0.0662(14) Uani 1 1 d D . . . . O4 O 0.1891(2) 0.5849(2) 0.34806(16) 0.0568(12) Uani 1 1 d D . . . . C44 C 0.1296(3) 0.7253(4) 0.3840(2) 0.0546(15) Uani 1 1 d D . . . . F4 F 0.1820(2) 0.7607(3) 0.41934(14) 0.0698(11) Uani 1 1 d D . . . . F5 F 0.0900(2) 0.8007(3) 0.3674(2) 0.0803(13) Uani 1 1 d D . . . . F6 F 0.1042(2) 0.6608(3) 0.41217(19) 0.0818(13) Uani 1 1 d D . . . . C45A C 0.5282(3) 0.9396(5) 0.3746(4) 0.0281(14) Uani 0.786(4) 1 d D . P B 1 F7A F 0.5250(2) 0.9522(3) 0.42748(19) 0.0394(10) Uani 0.786(4) 1 d D . P B 1 F8A F 0.4695(3) 0.9380(9) 0.3412(5) 0.044(3) Uani 0.786(4) 1 d D . P B 1 F9A F 0.55829(19) 1.0162(3) 0.36095(19) 0.0457(10) Uani 0.786(4) 1 d D . P B 1 S3A S 0.56858(14) 0.8213(2) 0.37112(13) 0.0182(6) Uani 0.786(4) 1 d D . P B 1 O5A O 0.5315(3) 0.7461(4) 0.3878(2) 0.0222(11) Uani 0.786(4) 1 d D . P B 1 O6A O 0.63089(18) 0.8387(3) 0.40655(19) 0.0304(9) Uani 0.786(4) 1 d D . P B 1 N6A N 0.5693(2) 0.8230(3) 0.30786(17) 0.0222(10) Uani 0.786(4) 1 d D . P B 1 S4A S 0.54214(19) 0.7410(3) 0.26100(18) 0.0193(6) Uani 0.786(4) 1 d D . P B 1 O7A O 0.53111(18) 0.6454(3) 0.28133(16) 0.0266(9) Uani 0.786(4) 1 d D . P B 1 O8A O 0.5765(2) 0.7476(4) 0.22024(19) 0.0328(10) Uani 0.786(4) 1 d D . P B 1 C46A C 0.4643(3) 0.7876(5) 0.2240(3) 0.0345(19) Uani 0.786(4) 1 d D . P B 1 F10A F 0.4659(4) 0.8808(5) 0.2066(4) 0.057(2) Uani 0.786(4) 1 d D . P B 1 F11A F 0.4398(2) 0.7308(4) 0.17855(18) 0.0601(14) Uani 0.786(4) 1 d D . P B 1 F12A F 0.42548(15) 0.7853(3) 0.25628(18) 0.0453(10) Uani 0.786(4) 1 d D . P B 1 C45B C 0.5235(9) 0.9267(12) 0.3546(8) 0.033(10) Uiso 0.214(4) 1 d D . P B 2 F7B F 0.5425(8) 0.9758(11) 0.4037(7) 0.040(4) Uani 0.214(4) 1 d D . P B 2 F8B F 0.4610(9) 0.927(3) 0.3384(12) 0.027(7) Uani 0.214(4) 1 d D . P B 2 F9B F 0.5433(6) 0.9783(9) 0.3170(6) 0.040(4) Uani 0.214(4) 1 d D . P B 2 S3B S 0.5537(5) 0.7986(8) 0.3631(5) 0.019(2) Uani 0.214(4) 1 d D . P B 2 O5B O 0.5333(9) 0.7613(15) 0.4102(6) 0.023(5) Uani 0.214(4) 1 d D . P B 2 O6B O 0.6198(5) 0.8107(10) 0.3710(6) 0.021(3) Uani 0.214(4) 1 d D . P B 2 N6B N 0.5162(6) 0.7440(11) 0.3078(5) 0.021(4) Uani 0.214(4) 1 d D . P B 2 S4B S 0.5333(7) 0.7359(11) 0.2502(6) 0.027(4) Uani 0.214(4) 1 d D . P B 2 O7B O 0.5265(8) 0.6351(8) 0.2309(7) 0.037(4) Uani 0.214(4) 1 d D . P B 2 O8B O 0.5866(6) 0.7894(11) 0.2451(6) 0.020(3) Uani 0.214(4) 1 d D . P B 2 C46B C 0.4662(8) 0.8010(15) 0.2030(7) 0.045(11) Uani 0.214(4) 1 d D . P B 2 F10B F 0.4690(14) 0.8977(15) 0.2165(12) 0.038(7) Uiso 0.214(4) 1 d D . P B 2 F11B F 0.4689(7) 0.7900(11) 0.1505(5) 0.045(4) Uiso 0.214(4) 1 d D . P B 2 F12B F 0.4125(7) 0.7628(13) 0.2072(8) 0.065(5) Uiso 0.214(4) 1 d D . P B 2 N7A N 0.1008(12) 0.2724(11) 0.4824(11) 0.026(5) Uani 0.308(8) 1 d D . P C 1 S6A S 0.0782(3) 0.1702(5) 0.5031(3) 0.0215(13) Uani 0.308(8) 1 d D . P C 1 O11A O 0.0483(7) 0.1096(10) 0.4553(5) 0.039(3) Uani 0.308(8) 1 d D . P C 1 O12A O 0.1236(14) 0.126(2) 0.5490(10) 0.048(9) Uani 0.308(8) 1 d D . P C 1 C48A C 0.0162(6) 0.2141(10) 0.5324(6) 0.019(4) Uiso 0.308(8) 1 d D . P C 1 F16A F -0.0227(5) 0.2751(8) 0.4970(5) 0.055(3) Uiso 0.308(8) 1 d D . P C 1 F17A F 0.0400(5) 0.2574(8) 0.5816(5) 0.046(3) Uiso 0.308(8) 1 d D . P C 1 F18A F -0.0169(5) 0.1368(8) 0.5422(5) 0.040(3) Uiso 0.308(8) 1 d D . P C 1 N7B N 0.1135(5) 0.2478(6) 0.4752(4) 0.024(2) Uani 0.692(8) 1 d D . P C 2 S6B S 0.09654(19) 0.1438(3) 0.49830(13) 0.0311(7) Uani 0.692(8) 1 d D . P C 2 O11B O 0.0846(4) 0.0701(5) 0.4542(2) 0.058(2) Uani 0.692(8) 1 d D . P C 2 O12B O 0.1314(6) 0.1148(9) 0.5534(3) 0.025(2) Uani 0.692(8) 1 d D . P C 2 C48B C 0.0188(3) 0.1716(7) 0.5062(4) 0.053(2) Uani 0.692(8) 1 d D . P C 2 F16B F -0.0209(2) 0.1932(5) 0.4559(3) 0.099(3) Uani 0.692(8) 1 d D . P C 2 F17B F 0.0204(3) 0.2496(6) 0.5402(3) 0.075(2) Uani 0.692(8) 1 d D . P C 2 F18B F -0.0039(2) 0.0943(5) 0.5271(3) 0.063(2) Uani 0.692(8) 1 d D . P C 2 loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_23 _atom_site_aniso_U_13 _atom_site_aniso_U_12 Au1 0.00938(7) 0.01197(8) 0.01096(8) -0.00052(5) 0.00100(5) -0.00041(5) Fe1 0.0106(2) 0.0154(3) 0.0122(2) 0.00030(19) 0.00120(19) 0.00027(19) Cl1 0.0308(6) 0.0300(6) 0.0336(6) -0.0024(4) -0.0030(4) -0.0040(4) Cl2 0.0536(8) 0.0344(7) 0.0515(8) -0.0077(6) 0.0113(6) 0.0059(6) S5 0.0180(5) 0.0247(5) 0.0145(4) -0.0006(4) 0.0034(3) -0.0035(4) P1 0.0096(4) 0.0138(4) 0.0126(4) -0.0009(3) 0.0012(3) -0.0006(3) P2 0.0114(4) 0.0114(4) 0.0123(4) -0.0005(3) 0.0008(3) -0.0002(3) F13 0.060(2) 0.0411(17) 0.0325(15) -0.0144(13) 0.0034(14) 0.0084(14) F14 0.0465(18) 0.094(3) 0.0369(16) 0.0063(17) 0.0148(14) 0.0431(18) F15 0.0490(19) 0.095(3) 0.0252(15) 0.0132(15) 0.0237(13) 0.0210(17) O9 0.0252(15) 0.0278(16) 0.0252(15) 0.0010(12) 0.0049(12) 0.0039(12) O10 0.0269(15) 0.0263(15) 0.0248(15) 0.0021(12) 0.0119(12) -0.0069(12) N1 0.0123(14) 0.0123(14) 0.0135(14) -0.0025(11) 0.0011(11) 0.0007(11) N2 0.0105(14) 0.0129(14) 0.0141(14) -0.0007(11) 0.0014(11) 0.0006(11) N3 0.0119(15) 0.0147(15) 0.0186(15) -0.0006(12) 0.0011(12) -0.0009(12) N4 0.0131(15) 0.0134(15) 0.0158(15) -0.0008(12) 0.0027(12) 0.0004(12) C1 0.0091(16) 0.0173(18) 0.0167(18) 0.0035(14) 0.0019(13) 0.0029(13) C2 0.0120(17) 0.0189(19) 0.0204(19) 0.0001(15) 0.0010(14) 0.0006(14) C3 0.022(2) 0.026(2) 0.025(2) -0.0008(17) 0.0093(16) 0.0075(16) C4 0.019(2) 0.027(2) 0.028(2) 0.0056(17) 0.0115(16) 0.0057(16) C5 0.0129(18) 0.028(2) 0.028(2) 0.0052(17) 0.0056(16) -0.0017(15) C6 0.0164(18) 0.023(2) 0.0166(18) 0.0000(15) 0.0029(14) -0.0020(15) C7 0.0094(16) 0.0165(18) 0.0185(18) -0.0009(14) 0.0027(13) -0.0012(13) C8 0.027(2) 0.020(2) 0.022(2) 0.0001(16) 0.0047(17) -0.0007(16) C9 0.027(2) 0.0126(19) 0.034(2) 0.0039(16) 0.0030(18) -0.0024(16) C10 0.021(2) 0.0161(19) 0.039(2) -0.0055(17) 0.0067(18) -0.0016(16) C11 0.040(3) 0.023(2) 0.027(2) -0.0096(18) 0.0092(19) -0.0026(19) C12 0.030(2) 0.020(2) 0.021(2) -0.0004(16) 0.0029(17) -0.0029(17) C13 0.0114(17) 0.0157(17) 0.0133(17) -0.0008(14) 0.0014(13) -0.0027(13) C14 0.0168(18) 0.0172(19) 0.0179(18) -0.0030(15) 0.0012(14) 0.0011(14) C15 0.027(2) 0.0155(19) 0.024(2) -0.0054(16) 0.0053(17) 0.0000(16) C16 0.027(2) 0.028(2) 0.0191(19) -0.0086(16) 0.0074(16) -0.0079(17) C17 0.021(2) 0.028(2) 0.0133(18) 0.0005(16) -0.0009(15) -0.0010(16) C18 0.0168(18) 0.022(2) 0.0153(18) 0.0009(15) 0.0014(14) 0.0014(15) C19 0.0125(17) 0.0154(18) 0.0165(18) 0.0000(14) -0.0022(14) -0.0008(14) C20 0.0176(19) 0.0167(19) 0.0230(19) -0.0002(15) 0.0028(15) 0.0016(15) C21 0.0084(18) 0.024(2) 0.044(3) -0.0050(18) 0.0040(17) -0.0012(15) C22 0.035(3) 0.021(2) 0.051(3) -0.003(2) 0.010(2) 0.0106(19) C23 0.057(3) 0.026(2) 0.037(3) 0.006(2) 0.028(2) 0.002(2) C24 0.029(2) 0.023(2) 0.035(2) 0.0039(18) 0.0150(19) 0.0018(17) C25 0.0146(17) 0.0144(17) 0.0134(17) -0.0028(14) 0.0020(13) -0.0003(14) C26 0.0157(19) 0.026(2) 0.0197(19) -0.0005(16) 0.0040(15) 0.0029(15) C27 0.0177(19) 0.029(2) 0.0196(19) 0.0041(16) 0.0002(15) 0.0075(16) C28 0.0177(18) 0.0179(19) 0.0163(18) 0.0029(14) 0.0022(14) 0.0061(14) C29 0.0157(18) 0.0128(17) 0.0137(17) -0.0015(13) 0.0027(14) 0.0017(13) C30 0.0147(17) 0.0164(18) 0.0163(18) 0.0051(14) 0.0035(14) 0.0035(14) C31 0.0141(17) 0.0105(16) 0.0163(17) -0.0008(13) 0.0047(14) 0.0029(13) C32 0.0116(17) 0.023(2) 0.0215(19) -0.0034(15) 0.0019(14) -0.0040(14) C33 0.0163(19) 0.023(2) 0.028(2) -0.0029(17) 0.0043(16) -0.0065(15) C34 0.0187(19) 0.0176(19) 0.025(2) 0.0013(15) 0.0072(16) -0.0027(15) C35 0.0144(17) 0.0123(17) 0.0180(18) 0.0013(14) 0.0063(14) 0.0039(13) C36 0.0139(18) 0.024(2) 0.0183(18) 0.0013(15) 0.0062(14) -0.0012(15) C37 0.023(2) 0.0174(19) 0.0174(19) 0.0030(15) 0.0027(15) -0.0030(15) C38 0.031(2) 0.0162(19) 0.027(2) 0.0034(16) 0.0033(18) 0.0018(17) C39 0.034(2) 0.019(2) 0.028(2) -0.0034(17) 0.0045(18) 0.0057(17) C40 0.021(2) 0.024(2) 0.0190(19) -0.0027(16) 0.0047(15) 0.0028(16) C41 0.0130(17) 0.0177(18) 0.0174(18) -0.0025(14) 0.0007(14) 0.0007(14) C42 0.0200(19) 0.0182(19) 0.0121(17) -0.0028(14) 0.0027(14) 0.0022(15) C47 0.028(2) 0.059(3) 0.017(2) -0.003(2) 0.0065(17) 0.015(2) C49 0.041(3) 0.034(3) 0.031(2) -0.001(2) 0.008(2) -0.006(2) C50A 0.117(11) 0.058(6) 0.053(6) -0.010(5) 0.054(7) -0.024(7) C51A 0.034(4) 0.050(5) 0.027(4) -0.014(4) 0.014(3) -0.006(4) C52A 0.032(4) 0.066(6) 0.034(4) -0.026(4) 0.004(3) 0.010(4) C53A 0.083(6) 0.045(6) 0.039(5) -0.017(5) 0.004(4) 0.030(4) C54A 0.130(8) 0.048(6) 0.060(6) -0.017(5) 0.049(6) 0.012(6) C55A 0.090(7) 0.047(6) 0.076(7) -0.028(4) 0.054(6) -0.013(6) C56A 0.050(5) 0.061(6) 0.051(5) -0.037(4) 0.032(4) -0.033(4) C43 0.040(3) 0.033(3) 0.038(3) -0.003(2) 0.003(2) 0.001(2) F1 0.0453(19) 0.074(2) 0.061(2) -0.0051(18) 0.0160(16) -0.0016(17) F2 0.0539(19) 0.0389(16) 0.0382(16) 0.0054(13) -0.0135(14) -0.0072(14) F3 0.058(2) 0.0288(15) 0.0490(18) -0.0146(13) 0.0110(15) -0.0034(13) S1 0.0501(7) 0.0237(6) 0.0299(6) -0.0052(5) -0.0013(5) 0.0157(5) O1 0.059(2) 0.041(2) 0.041(2) 0.0071(16) 0.0172(18) 0.0184(18) O2 0.069(3) 0.036(2) 0.051(2) -0.0161(18) -0.005(2) 0.0264(19) N5 0.045(2) 0.0141(17) 0.033(2) -0.0001(15) -0.0057(17) 0.0064(16) S2 0.0555(8) 0.0147(5) 0.0350(6) 0.0036(5) -0.0195(6) -0.0032(5) O3 0.064(3) 0.042(2) 0.062(3) 0.0151(19) -0.033(2) -0.0212(19) O4 0.080(3) 0.0154(16) 0.049(2) 0.0079(15) -0.024(2) 0.0017(17) C44 0.072(4) 0.032(3) 0.060(4) 0.007(3) 0.018(3) -0.013(3) F4 0.101(3) 0.061(2) 0.047(2) -0.0248(17) 0.018(2) -0.033(2) F5 0.094(3) 0.041(2) 0.127(4) 0.013(2) 0.065(3) 0.006(2) F6 0.115(4) 0.049(2) 0.086(3) 0.011(2) 0.035(3) -0.031(2) C45A 0.026(3) 0.021(3) 0.039(5) -0.004(3) 0.012(3) 0.003(2) F7A 0.049(2) 0.036(2) 0.039(2) -0.0093(18) 0.0214(19) 0.0048(18) F8A 0.029(3) 0.038(4) 0.056(5) -0.004(3) 0.000(3) 0.010(3) F9A 0.060(3) 0.0209(18) 0.060(3) -0.0005(18) 0.022(2) -0.0056(16) S3A 0.0172(13) 0.0186(12) 0.0191(11) 0.0000(8) 0.0059(9) 0.0005(8) O5A 0.024(2) 0.023(2) 0.023(3) 0.004(2) 0.012(3) -0.0033(17) O6A 0.019(2) 0.043(2) 0.028(2) -0.006(2) 0.0030(17) 0.0016(17) N6A 0.021(2) 0.023(2) 0.024(2) 0.0005(18) 0.0080(17) -0.0055(17) S4A 0.0155(10) 0.0238(12) 0.0182(13) 0.0013(9) 0.0044(10) -0.0005(8) O7A 0.029(2) 0.023(2) 0.028(2) -0.0022(15) 0.0073(16) -0.0034(15) O8A 0.031(2) 0.047(3) 0.024(2) -0.005(2) 0.0139(19) -0.007(2) C46A 0.020(4) 0.034(4) 0.041(5) -0.005(3) -0.006(3) 0.000(3) F10A 0.053(3) 0.047(4) 0.053(4) 0.020(3) -0.014(3) 0.008(3) F11A 0.039(2) 0.074(3) 0.046(2) -0.022(2) -0.0230(19) 0.001(2) F12A 0.0194(17) 0.049(2) 0.066(3) -0.0106(19) 0.0088(17) 0.0020(15) F7B 0.057(11) 0.019(8) 0.038(11) -0.012(7) 0.004(8) 0.006(7) F8B 0.024(11) 0.035(15) 0.026(12) 0.005(10) 0.013(9) 0.024(9) F9B 0.041(8) 0.024(7) 0.066(10) 0.014(7) 0.034(7) 0.006(6) S3B 0.021(5) 0.020(5) 0.018(4) -0.002(3) 0.006(3) 0.004(3) O5B 0.022(8) 0.037(10) 0.007(9) 0.005(8) -0.001(8) 0.001(7) O6B 0.007(7) 0.025(7) 0.026(8) -0.004(6) -0.002(5) -0.001(5) N6B 0.013(7) 0.030(9) 0.014(7) -0.004(6) -0.004(6) -0.012(6) S4B 0.031(6) 0.030(5) 0.019(6) -0.006(3) 0.006(4) -0.007(4) O7B 0.059(11) 0.011(7) 0.048(10) 0.001(6) 0.027(8) -0.010(6) O8B 0.021(7) 0.028(8) 0.014(7) -0.002(6) 0.009(6) 0.000(6) C46B 0.016(13) 0.07(3) 0.05(2) 0.036(19) 0.010(13) 0.014(14) N7A 0.029(10) 0.028(9) 0.024(9) 0.002(8) 0.009(6) 0.001(7) S6A 0.019(3) 0.024(3) 0.018(2) 0.0036(18) -0.0017(17) -0.0004(18) O11A 0.044(8) 0.036(7) 0.030(6) -0.002(5) -0.003(6) -0.026(6) O12A 0.048(14) 0.043(15) 0.051(17) 0.020(10) 0.011(11) 0.001(10) N7B 0.023(5) 0.028(4) 0.014(4) 0.004(3) -0.005(3) -0.012(4) S6B 0.0354(17) 0.0306(16) 0.0194(11) 0.0068(10) -0.0054(11) -0.0164(12) O11B 0.097(6) 0.042(4) 0.025(3) -0.004(3) -0.001(3) -0.036(4) O12B 0.037(4) 0.020(4) 0.013(4) 0.006(3) -0.002(3) -0.007(3) C48B 0.029(4) 0.058(5) 0.061(5) 0.034(4) -0.006(3) -0.017(4) F16B 0.038(3) 0.124(6) 0.100(5) 0.082(4) -0.037(3) -0.039(3) F17B 0.030(3) 0.084(5) 0.116(7) 0.011(4) 0.032(4) -0.011(3) F18B 0.035(3) 0.071(4) 0.077(4) 0.041(3) 0.003(3) -0.024(3) _geom_special_details ; All esds (except the esd in the dihedral angle between two l.s. planes) are estimated using the full covariance matrix. The cell esds are taken into account individually in the estimation of esds in distances, angles and torsion angles; correlations between esds in cell parameters are only used when they are defined by crystal symmetry. An approximate (isotropic) treatment of cell esds is used for estimating esds involving l.s. planes. ; loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_distance _geom_bond_site_symmetry_2 _geom_bond_publ_flag Au1 P1 2.3145(9) . ? Au1 P2 2.3182(9) . ? Au1 O10 2.505(3) . ? Au1 Fe1 2.6545(5) . ? Fe1 N2 2.063(3) . ? Fe1 N3 2.069(3) . ? Fe1 N1 2.077(3) . ? Fe1 N4 2.149(3) . ? Cl1 C49 1.761(5) . ? Cl2 C49 1.758(5) . ? S5 O9 1.426(3) . ? S5 O10 1.451(3) . ? S5 N7B 1.567(9) . ? S5 N7A 1.59(2) . ? S5 C47 1.827(5) . ? P1 C1 1.808(4) . ? P1 C7 1.811(4) . ? P1 C25 1.833(4) . ? P2 C13 1.797(4) . ? P2 C19 1.812(4) . ? P2 C31 1.825(4) . ? F13 C47 1.331(6) . ? F14 C47 1.331(5) . ? F15 C47 1.329(6) . ? N1 C29 1.347(5) . ? N1 C25 1.354(5) . ? N2 C35 1.346(5) . ? N2 C31 1.360(5) . ? N3 C41 1.345(5) . ? N3 C37 1.353(5) . ? N4 C30 1.485(4) . ? N4 C36 1.488(5) . ? N4 C42 1.493(5) . ? C1 C6 1.386(5) . ? C1 C2 1.390(5) . ? C2 C3 1.380(5) . ? C2 H2 0.9500 . ? C3 C4 1.391(6) . ? C3 H3 0.9500 . ? C4 C5 1.394(6) . ? C4 H4 0.9500 . ? C5 C6 1.388(5) . ? C5 H5 0.9500 . ? C6 H6 0.9500 . ? C7 C8 1.386(5) . ? C7 C12 1.388(5) . ? C8 C9 1.387(6) . ? C8 H8 0.9500 . ? C9 C10 1.373(6) . ? C9 H9 0.9500 . ? C10 C11 1.384(6) . ? C10 H10 0.9500 . ? C11 C12 1.388(6) . ? C11 H11 0.9500 . ? C12 H12 0.9500 . ? C13 C18 1.401(5) . ? C13 C14 1.402(5) . ? C14 C15 1.389(5) . ? C14 H14 0.9500 . ? C15 C16 1.376(6) . ? C15 H15 0.9500 . ? C16 C17 1.396(6) . ? C16 H16 0.9500 . ? C17 C18 1.389(5) . ? C17 H17 0.9500 . ? C18 H18 0.9500 . ? C19 C20 1.387(5) . ? C19 C24 1.399(6) . ? C20 C21 1.396(6) . ? C20 H20 0.9500 . ? C21 C22 1.387(7) . ? C21 H21 0.9500 . ? C22 C23 1.365(7) . ? C22 H22 0.9500 . ? C23 C24 1.390(6) . ? C23 H23 0.9500 . ? C24 H24 0.9500 . ? C25 C26 1.379(5) . ? C26 C27 1.398(6) . ? C26 H26 0.9500 . ? C27 C28 1.386(6) . ? C27 H27 0.9500 . ? C28 C29 1.390(5) . ? C28 H28 0.9500 . ? C29 C30 1.511(5) . ? C30 H30A 0.9900 . ? C30 H30B 0.9900 . ? C31 C32 1.374(5) . ? C32 C33 1.393(6) . ? C32 H32 0.9500 . ? C33 C34 1.380(6) . ? C33 H33 0.9500 . ? C34 C35 1.391(5) . ? C34 H34 0.9500 . ? C35 C36 1.503(5) . ? C36 H36A 0.9900 . ? C36 H36B 0.9900 . ? C37 C38 1.380(6) . ? C37 H37 0.9500 . ? C38 C39 1.386(6) . ? C38 H38 0.9500 . ? C39 C40 1.385(6) . ? C39 H39 0.9500 . ? C40 C41 1.386(5) . ? C40 H40 0.9500 . ? C41 C42 1.511(5) . ? C42 H42A 0.9900 . ? C42 H42B 0.9900 . ? C49 H49A 0.9900 . ? C49 H49B 0.9900 . ? C50A C51A 1.491(11) . ? C50A H50A 0.9800 . ? C50A H50B 0.9800 . ? C50A H50C 0.9800 . ? C51A C52A 1.3900 . ? C51A C56A 1.3900 . ? C52A C53A 1.3900 . ? C52A H52A 0.9500 . ? C53A C54A 1.3900 . ? C53A H53A 0.9500 . ? C54A C55A 1.3900 . ? C54A H54A 0.9500 . ? C55A C56A 1.3900 . ? C55A H55A 0.9500 . ? C56A H56A 0.9500 . ? C50B C51B 1.459(15) . ? C50B H50D 0.9800 . ? C50B H50E 0.9800 . ? C50B H50F 0.9800 . ? C51B C52B 1.3900 . ? C51B C56B 1.3900 . ? C52B C53B 1.3900 . ? C52B H52B 0.9500 . ? C53B C54B 1.3900 . ? C53B H53B 0.9500 . ? C54B C55B 1.3900 . ? C54B H54B 0.9500 . ? C55B C56B 1.3900 . ? C55B H55B 0.9500 . ? C56B H56B 0.9500 . ? C43 F3 1.323(5) . ? C43 F2 1.325(6) . ? C43 F1 1.347(6) . ? C43 S1 1.828(5) . ? S1 O2 1.430(3) . ? S1 O1 1.430(4) . ? S1 N5 1.577(4) . ? N5 S2 1.576(4) . ? S2 O3 1.422(4) . ? S2 O4 1.428(4) . ? S2 C44 1.824(6) . ? C44 F5 1.324(7) . ? C44 F6 1.328(6) . ? C44 F4 1.328(7) . ? C45A F9A 1.316(7) . ? C45A F8A 1.330(9) . ? C45A F7A 1.337(9) . ? C45A S3A 1.831(7) . ? S3A O5A 1.429(5) . ? S3A O6A 1.432(5) . ? S3A N6A 1.565(5) . ? N6A S4A 1.584(6) . ? S4A O7A 1.418(5) . ? S4A O8A 1.424(5) . ? S4A C46A 1.822(7) . ? C46A F10A 1.321(8) . ? C46A F12A 1.325(8) . ? C46A F11A 1.338(8) . ? C45B F9B 1.325(15) . ? C45B F8B 1.330(16) . ? C45B F7B 1.337(15) . ? C45B S3B 1.829(14) . ? S3B O6B 1.433(12) . ? S3B O5B 1.448(13) . ? S3B N6B 1.565(11) . ? N6B S4B 1.575(13) . ? S4B O8B 1.416(13) . ? S4B O7B 1.422(13) . ? S4B C46B 1.831(14) . ? C46B F11B 1.322(15) . ? C46B F12B 1.323(15) . ? C46B F10B 1.331(15) . ? N7A S6A 1.588(12) . ? S6A O12A 1.418(13) . ? S6A O11A 1.431(10) . ? S6A C48A 1.820(12) . ? C48A F17A 1.314(14) . ? C48A F16A 1.322(13) . ? C48A F18A 1.327(13) . ? N7B S6B 1.586(7) . ? S6B O12B 1.417(8) . ? S6B O11B 1.436(6) . ? S6B C48B 1.825(8) . ? C48B F18B 1.316(8) . ? C48B F17B 1.332(10) . ? C48B F16B 1.337(8) . ? loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 _geom_angle_publ_flag P1 Au1 P2 166.24(3) . . ? P1 Au1 O10 101.29(7) . . ? P2 Au1 O10 91.94(7) . . ? P1 Au1 Fe1 82.80(3) . . ? P2 Au1 Fe1 84.54(3) . . ? O10 Au1 Fe1 171.99(7) . . ? N2 Fe1 N3 105.95(12) . . ? N2 Fe1 N1 133.25(12) . . ? N3 Fe1 N1 113.89(12) . . ? N2 Fe1 N4 82.38(12) . . ? N3 Fe1 N4 81.66(12) . . ? N1 Fe1 N4 80.26(12) . . ? N2 Fe1 Au1 93.73(8) . . ? N3 Fe1 Au1 115.01(9) . . ? N1 Fe1 Au1 90.90(8) . . ? N4 Fe1 Au1 163.26(8) . . ? O9 S5 O10 117.94(18) . . ? O9 S5 N7B 113.5(4) . . ? O10 S5 N7B 107.7(4) . . ? O9 S5 N7A 125.2(7) . . ? O10 S5 N7A 107.9(8) . . ? O9 S5 C47 104.85(19) . . ? O10 S5 C47 101.6(2) . . ? N7B S5 C47 110.5(4) . . ? N7A S5 C47 93.1(7) . . ? C1 P1 C7 108.43(17) . . ? C1 P1 C25 107.32(16) . . ? C7 P1 C25 105.89(17) . . ? C1 P1 Au1 118.19(12) . . ? C7 P1 Au1 106.96(12) . . ? C25 P1 Au1 109.41(12) . . ? C13 P2 C19 109.96(17) . . ? C13 P2 C31 107.09(16) . . ? C19 P2 C31 104.29(17) . . ? C13 P2 Au1 114.33(12) . . ? C19 P2 Au1 109.86(12) . . ? C31 P2 Au1 110.80(12) . . ? S5 O10 Au1 133.18(18) . . ? C29 N1 C25 119.4(3) . . ? C29 N1 Fe1 114.9(2) . . ? C25 N1 Fe1 125.7(2) . . ? C35 N2 C31 119.6(3) . . ? C35 N2 Fe1 114.5(2) . . ? C31 N2 Fe1 125.9(2) . . ? C41 N3 C37 119.3(3) . . ? C41 N3 Fe1 114.0(2) . . ? C37 N3 Fe1 126.3(3) . . ? C30 N4 C36 112.5(3) . . ? C30 N4 C42 110.6(3) . . ? C36 N4 C42 111.7(3) . . ? C30 N4 Fe1 107.3(2) . . ? C36 N4 Fe1 108.6(2) . . ? C42 N4 Fe1 105.9(2) . . ? C6 C1 C2 121.2(3) . . ? C6 C1 P1 121.0(3) . . ? C2 C1 P1 117.7(3) . . ? C3 C2 C1 119.6(4) . . ? C3 C2 H2 120.2 . . ? C1 C2 H2 120.2 . . ? C2 C3 C4 119.8(4) . . ? C2 C3 H3 120.1 . . ? C4 C3 H3 120.1 . . ? C3 C4 C5 120.3(4) . . ? C3 C4 H4 119.9 . . ? C5 C4 H4 119.9 . . ? C6 C5 C4 120.0(4) . . ? C6 C5 H5 120.0 . . ? C4 C5 H5 120.0 . . ? C1 C6 C5 119.0(4) . . ? C1 C6 H6 120.5 . . ? C5 C6 H6 120.5 . . ? C8 C7 C12 119.9(4) . . ? C8 C7 P1 116.9(3) . . ? C12 C7 P1 122.9(3) . . ? C7 C8 C9 119.7(4) . . ? C7 C8 H8 120.1 . . ? C9 C8 H8 120.1 . . ? C10 C9 C8 120.6(4) . . ? C10 C9 H9 119.7 . . ? C8 C9 H9 119.7 . . ? C9 C10 C11 120.0(4) . . ? C9 C10 H10 120.0 . . ? C11 C10 H10 120.0 . . ? C10 C11 C12 120.0(4) . . ? C10 C11 H11 120.0 . . ? C12 C11 H11 120.0 . . ? C7 C12 C11 119.8(4) . . ? C7 C12 H12 120.1 . . ? C11 C12 H12 120.1 . . ? C18 C13 C14 120.0(3) . . ? C18 C13 P2 123.1(3) . . ? C14 C13 P2 116.8(3) . . ? C15 C14 C13 119.7(3) . . ? C15 C14 H14 120.1 . . ? C13 C14 H14 120.1 . . ? C16 C15 C14 119.7(4) . . ? C16 C15 H15 120.1 . . ? C14 C15 H15 120.1 . . ? C15 C16 C17 121.5(4) . . ? C15 C16 H16 119.3 . . ? C17 C16 H16 119.3 . . ? C18 C17 C16 119.2(4) . . ? C18 C17 H17 120.4 . . ? C16 C17 H17 120.4 . . ? C17 C18 C13 119.8(4) . . ? C17 C18 H18 120.1 . . ? C13 C18 H18 120.1 . . ? C20 C19 C24 119.9(4) . . ? C20 C19 P2 121.2(3) . . ? C24 C19 P2 118.6(3) . . ? C19 C20 C21 120.4(4) . . ? C19 C20 H20 119.8 . . ? C21 C20 H20 119.8 . . ? C22 C21 C20 119.3(4) . . ? C22 C21 H21 120.4 . . ? C20 C21 H21 120.4 . . ? C23 C22 C21 120.2(4) . . ? C23 C22 H22 119.9 . . ? C21 C22 H22 119.9 . . ? C22 C23 C24 121.6(4) . . ? C22 C23 H23 119.2 . . ? C24 C23 H23 119.2 . . ? C23 C24 C19 118.6(4) . . ? C23 C24 H24 120.7 . . ? C19 C24 H24 120.7 . . ? N1 C25 C26 122.2(3) . . ? N1 C25 P1 113.5(3) . . ? C26 C25 P1 124.3(3) . . ? C25 C26 C27 118.4(4) . . ? C25 C26 H26 120.8 . . ? C27 C26 H26 120.8 . . ? C28 C27 C26 119.5(3) . . ? C28 C27 H27 120.3 . . ? C26 C27 H27 120.3 . . ? C27 C28 C29 119.1(3) . . ? C27 C28 H28 120.4 . . ? C29 C28 H28 120.4 . . ? N1 C29 C28 121.4(3) . . ? N1 C29 C30 116.7(3) . . ? C28 C29 C30 121.8(3) . . ? N4 C30 C29 110.9(3) . . ? N4 C30 H30A 109.5 . . ? C29 C30 H30A 109.5 . . ? N4 C30 H30B 109.5 . . ? C29 C30 H30B 109.5 . . ? H30A C30 H30B 108.0 . . ? N2 C31 C32 121.7(3) . . ? N2 C31 P2 115.0(3) . . ? C32 C31 P2 123.1(3) . . ? C31 C32 C33 119.2(4) . . ? C31 C32 H32 120.4 . . ? C33 C32 H32 120.4 . . ? C34 C33 C32 118.7(4) . . ? C34 C33 H33 120.6 . . ? C32 C33 H33 120.6 . . ? C33 C34 C35 120.1(4) . . ? C33 C34 H34 120.0 . . ? C35 C34 H34 120.0 . . ? N2 C35 C34 120.7(3) . . ? N2 C35 C36 118.5(3) . . ? C34 C35 C36 120.7(3) . . ? N4 C36 C35 113.7(3) . . ? N4 C36 H36A 108.8 . . ? C35 C36 H36A 108.8 . . ? N4 C36 H36B 108.8 . . ? C35 C36 H36B 108.8 . . ? H36A C36 H36B 107.7 . . ? N3 C37 C38 121.8(4) . . ? N3 C37 H37 119.1 . . ? C38 C37 H37 119.1 . . ? C37 C38 C39 118.8(4) . . ? C37 C38 H38 120.6 . . ? C39 C38 H38 120.6 . . ? C40 C39 C38 119.6(4) . . ? C40 C39 H39 120.2 . . ? C38 C39 H39 120.2 . . ? C39 C40 C41 118.9(4) . . ? C39 C40 H40 120.6 . . ? C41 C40 H40 120.6 . . ? N3 C41 C40 121.7(3) . . ? N3 C41 C42 116.7(3) . . ? C40 C41 C42 121.6(3) . . ? N4 C42 C41 111.1(3) . . ? N4 C42 H42A 109.4 . . ? C41 C42 H42A 109.4 . . ? N4 C42 H42B 109.4 . . ? C41 C42 H42B 109.4 . . ? H42A C42 H42B 108.0 . . ? F15 C47 F13 108.9(4) . . ? F15 C47 F14 108.7(4) . . ? F13 C47 F14 108.4(4) . . ? F15 C47 S5 111.2(4) . . ? F13 C47 S5 109.6(3) . . ? F14 C47 S5 110.0(3) . . ? Cl2 C49 Cl1 111.7(3) . . ? Cl2 C49 H49A 109.3 . . ? Cl1 C49 H49A 109.3 . . ? Cl2 C49 H49B 109.3 . . ? Cl1 C49 H49B 109.3 . . ? H49A C49 H49B 107.9 . . ? C51A C50A H50A 109.5 . . ? C51A C50A H50B 109.5 . . ? H50A C50A H50B 109.5 . . ? C51A C50A H50C 109.5 . . ? H50A C50A H50C 109.5 . . ? H50B C50A H50C 109.5 . . ? C52A C51A C56A 120.0 . . ? C52A C51A C50A 119.1(7) . . ? C56A C51A C50A 120.9(7) . . ? C51A C52A C53A 120.0 . . ? C51A C52A H52A 120.0 . . ? C53A C52A H52A 120.0 . . ? C54A C53A C52A 120.0 . . ? C54A C53A H53A 120.0 . . ? C52A C53A H53A 120.0 . . ? C55A C54A C53A 120.0 . . ? C55A C54A H54A 120.0 . . ? C53A C54A H54A 120.0 . . ? C54A C55A C56A 120.0 . . ? C54A C55A H55A 120.0 . . ? C56A C55A H55A 120.0 . . ? C55A C56A C51A 120.0 . . ? C55A C56A H56A 120.0 . . ? C51A C56A H56A 120.0 . . ? C51B C50B H50D 109.5 . . ? C51B C50B H50E 109.5 . . ? H50D C50B H50E 109.5 . . ? C51B C50B H50F 109.5 . . ? H50D C50B H50F 109.5 . . ? H50E C50B H50F 109.5 . . ? C52B C51B C56B 120.0 . . ? C52B C51B C50B 120.0(10) . . ? C56B C51B C50B 120.0(10) . . ? C53B C52B C51B 120.0 . . ? C53B C52B H52B 120.0 . . ? C51B C52B H52B 120.0 . . ? C52B C53B C54B 120.0 . . ? C52B C53B H53B 120.0 . . ? C54B C53B H53B 120.0 . . ? C55B C54B C53B 120.0 . . ? C55B C54B H54B 120.0 . . ? C53B C54B H54B 120.0 . . ? C54B C55B C56B 120.0 . . ? C54B C55B H55B 120.0 . . ? C56B C55B H55B 120.0 . . ? C55B C56B C51B 120.0 . . ? C55B C56B H56B 120.0 . . ? C51B C56B H56B 120.0 . . ? F3 C43 F2 109.4(4) . . ? F3 C43 F1 107.8(4) . . ? F2 C43 F1 107.3(4) . . ? F3 C43 S1 110.9(3) . . ? F2 C43 S1 112.1(3) . . ? F1 C43 S1 109.2(3) . . ? O2 S1 O1 119.0(3) . . ? O2 S1 N5 115.1(3) . . ? O1 S1 N5 108.1(2) . . ? O2 S1 C43 104.6(2) . . ? O1 S1 C43 103.6(2) . . ? N5 S1 C43 104.8(2) . . ? S2 N5 S1 125.2(2) . . ? O3 S2 O4 117.7(2) . . ? O3 S2 N5 111.0(2) . . ? O4 S2 N5 116.3(3) . . ? O3 S2 C44 104.8(3) . . ? O4 S2 C44 104.7(3) . . ? N5 S2 C44 99.7(2) . . ? F5 C44 F6 108.2(5) . . ? F5 C44 F4 108.4(5) . . ? F6 C44 F4 108.0(5) . . ? F5 C44 S2 111.2(4) . . ? F6 C44 S2 110.3(4) . . ? F4 C44 S2 110.7(4) . . ? F9A C45A F8A 109.4(7) . . ? F9A C45A F7A 108.7(7) . . ? F8A C45A F7A 107.4(7) . . ? F9A C45A S3A 111.7(4) . . ? F8A C45A S3A 111.3(8) . . ? F7A C45A S3A 108.3(4) . . ? O5A S3A O6A 118.2(4) . . ? O5A S3A N6A 117.6(3) . . ? O6A S3A N6A 109.2(3) . . ? O5A S3A C45A 105.4(3) . . ? O6A S3A C45A 103.5(4) . . ? N6A S3A C45A 100.1(4) . . ? S3A N6A S4A 127.6(3) . . ? O7A S4A O8A 119.0(4) . . ? O7A S4A N6A 115.6(3) . . ? O8A S4A N6A 107.7(4) . . ? O7A S4A C46A 104.6(4) . . ? O8A S4A C46A 104.1(4) . . ? N6A S4A C46A 104.0(3) . . ? F10A C46A F12A 107.4(6) . . ? F10A C46A F11A 107.7(7) . . ? F12A C46A F11A 108.1(5) . . ? F10A C46A S4A 112.1(5) . . ? F12A C46A S4A 112.0(5) . . ? F11A C46A S4A 109.4(5) . . ? F9B C45B F8B 107.9(18) . . ? F9B C45B F7B 107.3(17) . . ? F8B C45B F7B 107.9(18) . . ? F9B C45B S3B 112.7(12) . . ? F8B C45B S3B 110.9(17) . . ? F7B C45B S3B 110.1(12) . . ? O6B S3B O5B 117.9(12) . . ? O6B S3B N6B 116.4(10) . . ? O5B S3B N6B 109.3(11) . . ? O6B S3B C45B 103.7(9) . . ? O5B S3B C45B 103.2(11) . . ? N6B S3B C45B 104.3(10) . . ? S3B N6B S4B 128.1(10) . . ? O8B S4B O7B 117.5(13) . . ? O8B S4B N6B 117.5(11) . . ? O7B S4B N6B 109.7(12) . . ? O8B S4B C46B 104.8(11) . . ? O7B S4B C46B 104.2(11) . . ? N6B S4B C46B 100.5(10) . . ? F11B C46B F12B 108.8(15) . . ? F11B C46B F10B 109.9(17) . . ? F12B C46B F10B 109.6(17) . . ? F11B C46B S4B 108.5(12) . . ? F12B C46B S4B 110.8(13) . . ? F10B C46B S4B 109.2(16) . . ? S6A N7A S5 125.2(17) . . ? O12A S6A O11A 119.0(15) . . ? O12A S6A N7A 113.4(16) . . ? O11A S6A N7A 109.7(11) . . ? O12A S6A C48A 105.2(14) . . ? O11A S6A C48A 106.4(8) . . ? N7A S6A C48A 101.1(8) . . ? F17A C48A F16A 110.9(12) . . ? F17A C48A F18A 106.0(10) . . ? F16A C48A F18A 108.0(11) . . ? F17A C48A S6A 110.8(9) . . ? F16A C48A S6A 111.1(9) . . ? F18A C48A S6A 109.8(9) . . ? S5 N7B S6B 126.4(7) . . ? O12B S6B O11B 118.3(6) . . ? O12B S6B N7B 117.7(6) . . ? O11B S6B N7B 109.9(5) . . ? O12B S6B C48B 103.4(6) . . ? O11B S6B C48B 104.0(5) . . ? N7B S6B C48B 100.8(4) . . ? F18B C48B F17B 108.3(8) . . ? F18B C48B F16B 107.9(6) . . ? F17B C48B F16B 108.1(8) . . ? F18B C48B S6B 110.9(6) . . ? F17B C48B S6B 111.5(5) . . ? F16B C48B S6B 110.0(7) . . ? _refine_diff_density_max 2.381 _refine_diff_density_min -2.102 _refine_diff_density_rms 0.124 _shelx_res_file ; TITL .\x24_04_c.res in P2(1)/c x24_04_c.res created by SHELXL-2018/3 at 18:24:18 on 25-Mar-2024 REM Old TITL x24_04 in P2(1)/c REM SHELXT solution in P2(1)/c: R1 0.161, Rweak 0.008, Alpha 0.041 REM 0.875 for 648 systematic absences, Orientation as input REM Formula found by SHELXT: C65 N6 O11 F15 S2 Cl6 Fe Au CELL 0.71073 22.1627 13.3594 24.6684 90.000 106.235 90.000 ZERR 4.000 0.0006 0.0003 0.0006 0.000 0.001 0.000 LATT 1 SYMM -X, 1/2+Y, 1/2-Z SFAC C H N O F P S CL FE AU UNIT 224 184 28 48 72 8 24 8 4 4 RIGU 0.004 0.004 C48B F16B F17B F18B ACTA LIST 4 SIMU 0.04 0.08 2 C50B C51B C52B C53B C54B C55B C56B RIGU 0.004 0.004 C50B C51B C52B C53B C54B C55B C56B SIMU 0.04 0.08 2 C51A C56A C55A C54A C53A C52A RIGU 0.004 0.004 C51A C56A C55A C54A C53A C52A TEMP -173 L.S. 5 BOND $H Size 0.15 0.15 0.15 FMAP 2 PLAN 20 SADI C50A C51A C50B C51B WGHT 0.028800 21.005600 FVAR 0.15197 0.78638 0.30774 0.64968 AU1 10 0.203394 0.368951 0.371051 11.00000 0.00938 0.01197 = 0.01096 -0.00052 0.00100 -0.00041 FE1 9 0.235622 0.373869 0.275227 11.00000 0.01056 0.01545 = 0.01222 0.00030 0.00120 0.00027 CL1 8 0.477784 0.635691 0.521069 11.00000 0.03079 0.03002 = 0.03359 -0.00240 -0.00295 -0.00402 CL2 8 0.409686 0.824234 0.512450 11.00000 0.05361 0.03438 = 0.05154 -0.00767 0.01132 0.00586 S5 7 0.169309 0.318507 0.505082 11.00000 0.01797 0.02466 = 0.01448 -0.00059 0.00342 -0.00348 P1 6 0.105397 0.331530 0.311127 11.00000 0.00960 0.01377 = 0.01262 -0.00089 0.00122 -0.00055 P2 6 0.309886 0.391462 0.413430 11.00000 0.01136 0.01142 = 0.01228 -0.00049 0.00084 -0.00021 F13 5 0.191118 0.469206 0.574326 11.00000 0.05969 0.04107 = 0.03246 -0.01440 0.00339 0.00840 F14 5 0.093428 0.449188 0.528879 11.00000 0.04652 0.09358 = 0.03687 0.00630 0.01477 0.04314 F15 5 0.137258 0.350383 0.598084 11.00000 0.04904 0.09513 = 0.02523 0.01316 0.02370 0.02099 O9 4 0.223115 0.266271 0.538287 11.00000 0.02520 0.02776 = 0.02522 0.00100 0.00492 0.00391 O10 4 0.178187 0.389141 0.463306 11.00000 0.02687 0.02634 = 0.02483 0.00206 0.01194 -0.00691 N1 3 0.146350 0.422960 0.231512 11.00000 0.01234 0.01231 = 0.01352 -0.00250 0.00111 0.00068 N2 3 0.319352 0.446802 0.310958 11.00000 0.01048 0.01294 = 0.01413 -0.00071 0.00139 0.00063 N3 3 0.259564 0.236795 0.248145 11.00000 0.01194 0.01470 = 0.01857 -0.00056 0.00105 -0.00094 N4 3 0.253638 0.422610 0.198213 11.00000 0.01306 0.01338 = 0.01578 -0.00078 0.00270 0.00038 C1 1 0.037381 0.350062 0.336778 11.00000 0.00913 0.01727 = 0.01673 0.00349 0.00185 0.00289 C2 1 0.039872 0.426446 0.375591 11.00000 0.01199 0.01889 = 0.02044 0.00011 0.00100 0.00063 AFIX 43 H2 2 0.076298 0.467214 0.387634 11.00000 -1.20000 AFIX 0 C3 1 -0.010886 0.442720 0.396534 11.00000 0.02248 0.02644 = 0.02454 -0.00085 0.00931 0.00753 AFIX 43 H3 2 -0.009479 0.494651 0.423168 11.00000 -1.20000 AFIX 0 C4 1 -0.064092 0.382897 0.378543 11.00000 0.01855 0.02697 = 0.02810 0.00564 0.01151 0.00570 AFIX 43 H4 2 -0.098983 0.393899 0.393056 11.00000 -1.20000 AFIX 0 C5 1 -0.066462 0.306844 0.339303 11.00000 0.01292 0.02791 = 0.02833 0.00521 0.00559 -0.00167 AFIX 43 H5 2 -0.103045 0.266510 0.326924 11.00000 -1.20000 AFIX 0 C6 1 -0.015404 0.290013 0.318307 11.00000 0.01637 0.02339 = 0.01658 0.00004 0.00289 -0.00201 AFIX 43 H6 2 -0.016617 0.238132 0.291685 11.00000 -1.20000 AFIX 0 C7 1 0.107473 0.201559 0.290834 11.00000 0.00938 0.01651 = 0.01854 -0.00093 0.00268 -0.00120 C8 1 0.124782 0.131971 0.334111 11.00000 0.02745 0.02036 = 0.02190 0.00013 0.00474 -0.00065 AFIX 43 H8 2 0.130912 0.152257 0.372180 11.00000 -1.20000 AFIX 0 C9 1 0.133106 0.032639 0.321582 11.00000 0.02678 0.01256 = 0.03414 0.00388 0.00298 -0.00238 AFIX 43 H9 2 0.144342 -0.015243 0.351176 11.00000 -1.20000 AFIX 0 C10 1 0.125251 0.002900 0.266783 11.00000 0.02132 0.01606 = 0.03913 -0.00546 0.00671 -0.00161 AFIX 43 H10 2 0.132053 -0.064996 0.258662 11.00000 -1.20000 AFIX 0 C11 1 0.107415 0.071873 0.223353 11.00000 0.03989 0.02306 = 0.02738 -0.00964 0.00916 -0.00256 AFIX 43 H11 2 0.101584 0.051173 0.185390 11.00000 -1.20000 AFIX 0 C12 1 0.098047 0.171286 0.235261 11.00000 0.03026 0.02027 = 0.02054 -0.00043 0.00291 -0.00295 AFIX 43 H12 2 0.085215 0.218481 0.205442 11.00000 -1.20000 AFIX 0 C13 1 0.327843 0.457343 0.479540 11.00000 0.01143 0.01570 = 0.01326 -0.00082 0.00139 -0.00271 C14 1 0.294901 0.546503 0.480716 11.00000 0.01683 0.01725 = 0.01788 -0.00303 0.00118 0.00113 AFIX 43 H14 2 0.265439 0.570261 0.447399 11.00000 -1.20000 AFIX 0 C15 1 0.305502 0.599971 0.530779 11.00000 0.02726 0.01553 = 0.02403 -0.00540 0.00531 -0.00003 AFIX 43 H15 2 0.283770 0.660955 0.531718 11.00000 -1.20000 AFIX 0 C16 1 0.347594 0.564288 0.579009 11.00000 0.02703 0.02791 = 0.01913 -0.00861 0.00738 -0.00788 AFIX 43 H16 2 0.354748 0.601427 0.613062 11.00000 -1.20000 AFIX 0 C17 1 0.380023 0.474727 0.579017 11.00000 0.02077 0.02849 = 0.01328 0.00051 -0.00087 -0.00103 AFIX 43 H17 2 0.408206 0.450337 0.612884 11.00000 -1.20000 AFIX 0 C18 1 0.370586 0.421689 0.528901 11.00000 0.01678 0.02186 = 0.01530 0.00094 0.00138 0.00143 AFIX 43 H18 2 0.393057 0.361403 0.528108 11.00000 -1.20000 AFIX 0 C19 1 0.349614 0.271470 0.422762 11.00000 0.01253 0.01538 = 0.01650 -0.00003 -0.00216 -0.00080 C20 1 0.390051 0.245472 0.391139 11.00000 0.01761 0.01666 = 0.02295 -0.00022 0.00277 0.00159 AFIX 43 H20 2 0.400153 0.293189 0.366486 11.00000 -1.20000 AFIX 0 C21 1 0.415996 0.149601 0.395321 11.00000 0.00843 0.02389 = 0.04411 -0.00501 0.00400 -0.00119 AFIX 43 H21 2 0.444372 0.132264 0.374239 11.00000 -1.20000 AFIX 0 C22 1 0.399909 0.079935 0.430577 11.00000 0.03522 0.02061 = 0.05067 -0.00324 0.00989 0.01062 AFIX 43 H22 2 0.416396 0.013935 0.432903 11.00000 -1.20000 AFIX 0 C23 1 0.360436 0.105971 0.461950 11.00000 0.05669 0.02573 = 0.03693 0.00624 0.02769 0.00177 AFIX 43 H23 2 0.350596 0.057877 0.486545 11.00000 -1.20000 AFIX 0 C24 1 0.334291 0.201102 0.458794 11.00000 0.02898 0.02291 = 0.03473 0.00390 0.01496 0.00184 AFIX 43 H24 2 0.306607 0.217991 0.480636 11.00000 -1.20000 AFIX 0 C25 1 0.092771 0.404119 0.245845 11.00000 0.01458 0.01439 = 0.01342 -0.00283 0.00204 -0.00026 C26 1 0.034880 0.437300 0.213739 11.00000 0.01567 0.02563 = 0.01970 -0.00050 0.00396 0.00291 AFIX 43 H26 2 -0.002060 0.423927 0.224840 11.00000 -1.20000 AFIX 0 C27 1 0.031897 0.491119 0.164437 11.00000 0.01765 0.02880 = 0.01964 0.00406 0.00024 0.00754 AFIX 43 H27 2 -0.007344 0.514738 0.141401 11.00000 -1.20000 AFIX 0 C28 1 0.086621 0.509738 0.149437 11.00000 0.01774 0.01794 = 0.01626 0.00287 0.00216 0.00606 AFIX 43 H28 2 0.085280 0.545802 0.115929 11.00000 -1.20000 AFIX 0 C29 1 0.143492 0.474959 0.184057 11.00000 0.01571 0.01279 = 0.01367 -0.00146 0.00274 0.00174 C30 1 0.205348 0.498792 0.172402 11.00000 0.01467 0.01645 = 0.01630 0.00510 0.00352 0.00348 AFIX 23 H30A 2 0.199333 0.500770 0.131110 11.00000 -1.20000 H30B 2 0.219997 0.565628 0.187948 11.00000 -1.20000 AFIX 0 C31 1 0.346182 0.461088 0.367114 11.00000 0.01408 0.01050 = 0.01633 -0.00079 0.00470 0.00288 C32 1 0.399525 0.517882 0.386819 11.00000 0.01158 0.02269 = 0.02154 -0.00338 0.00185 -0.00403 AFIX 43 H32 2 0.416980 0.528199 0.426205 11.00000 -1.20000 AFIX 0 C33 1 0.427695 0.560136 0.348362 11.00000 0.01634 0.02311 = 0.02767 -0.00290 0.00427 -0.00645 AFIX 43 H33 2 0.464437 0.600031 0.361022 11.00000 -1.20000 AFIX 0 C34 1 0.401188 0.542919 0.291495 11.00000 0.01873 0.01765 = 0.02466 0.00135 0.00721 -0.00270 AFIX 43 H34 2 0.420289 0.569754 0.264664 11.00000 -1.20000 AFIX 0 C35 1 0.346564 0.486350 0.273423 11.00000 0.01436 0.01235 = 0.01800 0.00128 0.00628 0.00395 C36 1 0.318653 0.463337 0.211850 11.00000 0.01393 0.02446 = 0.01828 0.00131 0.00623 -0.00118 AFIX 23 H36A 2 0.318262 0.525341 0.189775 11.00000 -1.20000 H36B 2 0.345881 0.414216 0.199946 11.00000 -1.20000 AFIX 0 C37 1 0.273936 0.152580 0.279568 11.00000 0.02310 0.01743 = 0.01745 0.00301 0.00268 -0.00295 AFIX 43 H37 2 0.267611 0.151178 0.316094 11.00000 -1.20000 AFIX 0 C38 1 0.297539 0.068628 0.260008 11.00000 0.03138 0.01624 = 0.02744 0.00336 0.00333 0.00184 AFIX 43 H38 2 0.307324 0.010138 0.282677 11.00000 -1.20000 AFIX 0 C39 1 0.306704 0.071205 0.206711 11.00000 0.03362 0.01931 = 0.02765 -0.00341 0.00450 0.00567 AFIX 43 H39 2 0.322813 0.014231 0.192374 11.00000 -1.20000 AFIX 0 C40 1 0.292223 0.157383 0.174489 11.00000 0.02129 0.02382 = 0.01898 -0.00269 0.00472 0.00283 AFIX 43 H40 2 0.298782 0.160631 0.138084 11.00000 -1.20000 AFIX 0 C41 1 0.268003 0.238808 0.196243 11.00000 0.01300 0.01774 = 0.01741 -0.00245 0.00065 0.00067 C42 1 0.246212 0.331945 0.161517 11.00000 0.02005 0.01820 = 0.01206 -0.00283 0.00274 0.00215 AFIX 23 H42A 2 0.270983 0.340518 0.134087 11.00000 -1.20000 H42B 2 0.201489 0.324319 0.140023 11.00000 -1.20000 AFIX 0 C47 1 0.146328 0.401395 0.554793 11.00000 0.02842 0.05858 = 0.01692 -0.00299 0.00652 0.01518 C49 1 0.464797 0.754493 0.488957 11.00000 0.04079 0.03358 = 0.03078 -0.00111 0.00841 -0.00649 AFIX 23 H49A 2 0.505032 0.791608 0.497638 11.00000 -1.20000 H49B 2 0.449442 0.746224 0.447482 11.00000 -1.20000 AFIX 0 Part 1 41.0 C50A 1 0.217619 -0.007435 0.485898 41.00000 0.11676 0.05780 = 0.05324 -0.01004 0.05442 -0.02410 AFIX 137 H50A 2 0.239149 -0.030368 0.458457 41.00000 -1.50000 H50B 2 0.235998 0.056092 0.502485 41.00000 -1.50000 H50C 2 0.172861 0.002181 0.466874 41.00000 -1.50000 AFIX 66 C51A 1 0.224994 -0.083817 0.531350 41.00000 0.03408 0.05023 = 0.02709 -0.01395 0.01409 -0.00588 C52A 1 0.284092 -0.099437 0.568660 41.00000 0.03165 0.06640 = 0.03366 -0.02601 0.00373 0.00957 AFIX 43 H52A 2 0.318863 -0.060554 0.565559 41.00000 -1.20000 AFIX 65 C53A 1 0.292315 -0.171949 0.610507 41.00000 0.08320 0.04487 = 0.03871 -0.01705 0.00380 0.02970 AFIX 43 H53A 2 0.332706 -0.182624 0.636007 41.00000 -1.20000 AFIX 65 C54A 1 0.241440 -0.228841 0.615045 41.00000 0.12979 0.04804 = 0.06025 -0.01747 0.04926 0.01228 AFIX 43 H54A 2 0.247061 -0.278399 0.643646 41.00000 -1.20000 AFIX 65 C55A 1 0.182342 -0.213222 0.577735 41.00000 0.09016 0.04666 = 0.07635 -0.02796 0.05396 -0.01340 AFIX 43 H55A 2 0.147571 -0.252106 0.580837 41.00000 -1.20000 AFIX 65 C56A 1 0.174118 -0.140710 0.535888 41.00000 0.05031 0.06131 = 0.05133 -0.03746 0.03150 -0.03269 AFIX 43 H56A 2 0.133727 -0.130035 0.510389 41.00000 -1.20000 AFIX 0 Part 2 -41.0 C50B 1 0.256288 -0.033706 0.511405 -41.00000 0.04666 AFIX 137 H50D 2 0.217059 -0.011867 0.484426 -41.00000 -1.50000 H50E 2 0.284276 -0.062016 0.490861 -41.00000 -1.50000 H50F 2 0.276786 0.023731 0.533818 -41.00000 -1.50000 AFIX 66 C51B 1 0.242508 -0.109579 0.548786 -41.00000 0.02355 C52B 1 0.290234 -0.145599 0.593935 -41.00000 0.01994 AFIX 43 H52B 2 0.331869 -0.121041 0.600348 -41.00000 -1.20000 AFIX 65 C53B 1 0.277041 -0.217550 0.629700 -41.00000 0.01934 AFIX 43 H53B 2 0.309660 -0.242168 0.660558 -41.00000 -1.20000 AFIX 65 C54B 1 0.216123 -0.253481 0.620317 -41.00000 0.02154 AFIX 43 H54B 2 0.207106 -0.302656 0.644761 -41.00000 -1.20000 AFIX 65 C55B 1 0.168396 -0.217462 0.575168 -41.00000 0.02385 AFIX 43 H55B 2 0.126761 -0.242020 0.568756 -41.00000 -1.20000 AFIX 65 C56B 1 0.181588 -0.145511 0.539403 -41.00000 0.02392 AFIX 43 H56B 2 0.148969 -0.120894 0.508545 -41.00000 -1.20000 AFIX 0 Part 0 C43 1 0.296759 0.793208 0.352341 11.00000 0.03973 0.03272 = 0.03812 -0.00306 0.00322 0.00144 F1 5 0.353949 0.805253 0.344182 11.00000 0.04532 0.07442 = 0.06148 -0.00509 0.01599 -0.00165 F2 5 0.302345 0.724944 0.392428 11.00000 0.05387 0.03894 = 0.03822 0.00539 -0.01348 -0.00720 F3 5 0.280129 0.879705 0.370008 11.00000 0.05796 0.02883 = 0.04896 -0.01463 0.01098 -0.00340 S1 7 0.240880 0.755222 0.285940 11.00000 0.05013 0.02372 = 0.02988 -0.00521 -0.00129 0.01569 O1 4 0.241831 0.837021 0.248784 11.00000 0.05900 0.04102 = 0.04112 0.00708 0.01723 0.01839 O2 4 0.262667 0.659332 0.273859 11.00000 0.06901 0.03620 = 0.05050 -0.01609 -0.00455 0.02636 N5 3 0.175040 0.754841 0.298729 11.00000 0.04457 0.01406 = 0.03302 -0.00007 -0.00565 0.00642 S2 7 0.146494 0.663764 0.323875 11.00000 0.05546 0.01466 = 0.03504 0.00363 -0.01951 -0.00325 O3 4 0.086609 0.636637 0.287913 11.00000 0.06436 0.04193 = 0.06167 0.01513 -0.03301 -0.02125 O4 4 0.189052 0.584922 0.348056 11.00000 0.08000 0.01543 = 0.04942 0.00793 -0.02399 0.00166 C44 1 0.129632 0.725339 0.384000 11.00000 0.07176 0.03188 = 0.05987 0.00695 0.01798 -0.01251 F4 5 0.181999 0.760708 0.419344 11.00000 0.10065 0.06056 = 0.04688 -0.02485 0.01830 -0.03305 F5 5 0.089964 0.800705 0.367413 11.00000 0.09392 0.04101 = 0.12683 0.01288 0.06544 0.00573 F6 5 0.104151 0.660845 0.412172 11.00000 0.11510 0.04865 = 0.08597 0.01114 0.03528 -0.03134 Part 1 21.0 Same C43 > F6 C45A 1 0.528151 0.939595 0.374589 21.00000 0.02571 0.02125 = 0.03915 -0.00394 0.01226 0.00317 F7A 5 0.524973 0.952212 0.427476 21.00000 0.04877 0.03590 = 0.03920 -0.00927 0.02139 0.00485 F8A 5 0.469525 0.937980 0.341157 21.00000 0.02947 0.03845 = 0.05637 -0.00394 0.00004 0.01038 F9A 5 0.558292 1.016208 0.360949 21.00000 0.05962 0.02094 = 0.05965 -0.00053 0.02184 -0.00556 S3A 7 0.568580 0.821293 0.371121 21.00000 0.01725 0.01865 = 0.01908 0.00001 0.00587 0.00045 O5A 4 0.531524 0.746074 0.387766 21.00000 0.02354 0.02320 = 0.02321 0.00428 0.01195 -0.00327 O6A 4 0.630893 0.838675 0.406550 21.00000 0.01873 0.04280 = 0.02754 -0.00648 0.00300 0.00157 N6A 3 0.569284 0.822973 0.307865 21.00000 0.02057 0.02326 = 0.02392 0.00049 0.00799 -0.00555 S4A 7 0.542142 0.741007 0.261004 21.00000 0.01552 0.02378 = 0.01824 0.00133 0.00435 -0.00047 O7A 4 0.531110 0.645397 0.281329 21.00000 0.02851 0.02333 = 0.02766 -0.00219 0.00725 -0.00339 O8A 4 0.576495 0.747566 0.220239 21.00000 0.03103 0.04669 = 0.02431 -0.00548 0.01391 -0.00688 C46A 1 0.464271 0.787649 0.224028 21.00000 0.01972 0.03419 = 0.04057 -0.00509 -0.00641 -0.00007 F10A 5 0.465923 0.880814 0.206588 21.00000 0.05338 0.04713 = 0.05257 0.01999 -0.01408 0.00795 F11A 5 0.439785 0.730837 0.178545 21.00000 0.03919 0.07434 = 0.04573 -0.02241 -0.02299 0.00141 F12A 5 0.425480 0.785290 0.256280 21.00000 0.01937 0.04879 = 0.06581 -0.01057 0.00880 0.00200 Part 0 Part 2 -21.0 Same C43 > F6 C45B 1 0.523486 0.926729 0.354592 -21.00000 0.03336 F7B 5 0.542455 0.975843 0.403650 -21.00000 0.05701 0.01896 = 0.03770 -0.01174 0.00402 0.00631 F8B 5 0.460996 0.927279 0.338390 -21.00000 0.02436 0.03469 = 0.02644 0.00459 0.01343 0.02404 F9B 5 0.543299 0.978283 0.316988 -21.00000 0.04147 0.02362 = 0.06603 0.01435 0.03363 0.00586 S3B 7 0.553668 0.798567 0.363130 -21.00000 0.02055 0.01953 = 0.01831 -0.00239 0.00640 0.00400 O5B 4 0.533267 0.761265 0.410239 -21.00000 0.02230 0.03693 = 0.00667 0.00548 -0.00074 0.00072 O6B 4 0.619813 0.810735 0.370964 -21.00000 0.00736 0.02545 = 0.02578 -0.00385 -0.00168 -0.00147 N6B 3 0.516201 0.744026 0.307832 -21.00000 0.01311 0.03005 = 0.01361 -0.00438 -0.00413 -0.01151 S4B 7 0.533295 0.735918 0.250154 -21.00000 0.03121 0.03045 = 0.01861 -0.00639 0.00612 -0.00729 O7B 4 0.526473 0.635078 0.230896 -21.00000 0.05874 0.01116 = 0.04813 0.00064 0.02746 -0.01025 O8B 4 0.586612 0.789420 0.245130 -21.00000 0.02054 0.02797 = 0.01439 -0.00219 0.00898 -0.00048 C46B 1 0.466158 0.800968 0.203022 -21.00000 0.01640 0.07195 = 0.04788 0.03551 0.01006 0.01359 F10B 5 0.468975 0.897656 0.216488 -21.00000 0.03832 F11B 5 0.468915 0.790011 0.150494 -21.00000 0.04529 F12B 5 0.412542 0.762769 0.207184 -21.00000 0.06544 PArt 0 Part 1 31.0 Same N5 > F6 N7A 3 0.100818 0.272395 0.482362 31.00000 0.02863 0.02779 = 0.02387 0.00243 0.00892 0.00131 S6A 7 0.078156 0.170188 0.503092 31.00000 0.01857 0.02367 = 0.01807 0.00356 -0.00174 -0.00038 O11A 4 0.048267 0.109564 0.455323 31.00000 0.04444 0.03590 = 0.02965 -0.00233 -0.00281 -0.02553 O12A 4 0.123620 0.125982 0.549048 31.00000 0.04830 0.04298 = 0.05137 0.01958 0.01051 0.00115 C48A 1 0.016171 0.214074 0.532432 31.00000 0.01873 F16A 5 -0.022655 0.275116 0.497038 31.00000 0.05467 F17A 5 0.040017 0.257407 0.581570 31.00000 0.04610 F18A 5 -0.016903 0.136820 0.542225 31.00000 0.03983 Part 2 -31.0 Same N5 > F6 N7B 3 0.113546 0.247756 0.475159 -31.00000 0.02311 0.02776 = 0.01424 0.00422 -0.00523 -0.01200 S6B 7 0.096537 0.143844 0.498302 -31.00000 0.03544 0.03058 = 0.01941 0.00678 -0.00539 -0.01642 O11B 4 0.084619 0.070065 0.454227 -31.00000 0.09685 0.04202 = 0.02546 -0.00393 -0.00096 -0.03579 O12B 4 0.131385 0.114771 0.553381 -31.00000 0.03671 0.01992 = 0.01284 0.00553 -0.00229 -0.00698 C48B 1 0.018824 0.171634 0.506205 -31.00000 0.02933 0.05808 = 0.06083 0.03435 -0.00629 -0.01730 F16B 5 -0.020921 0.193167 0.455902 -31.00000 0.03820 0.12415 = 0.09967 0.08217 -0.03660 -0.03938 F17B 5 0.020391 0.249600 0.540202 -31.00000 0.03021 0.08394 = 0.11646 0.01134 0.03189 -0.01103 F18B 5 -0.003860 0.094256 0.527064 -31.00000 0.03463 0.07054 = 0.07694 0.04137 0.00286 -0.02388 Part 0 HKLF 4 REM .\x24_04_c.res in P2(1)/c REM wR2 = 0.0888, GooF = S = 1.114, Restrained GooF = 1.108 for all data REM R1 = 0.0368 for 13149 Fo > 4sig(Fo) and 0.0400 for all 14346 data REM 1122 parameters refined using 348 restraints END WGHT 0.0288 21.0056 REM Highest difference peak 2.381, deepest hole -2.102, 1-sigma level 0.124 Q1 1 0.1888 0.3691 0.4018 11.00000 0.05 2.38 Q2 1 0.2190 0.3706 0.3405 11.00000 0.05 2.17 Q3 1 0.2060 0.3050 0.3826 11.00000 0.05 1.18 Q4 1 0.2010 0.4338 0.3563 11.00000 0.05 1.11 Q5 1 0.2066 0.4328 0.3845 11.00000 0.05 1.06 Q6 1 -0.0282 0.2442 0.4819 11.00000 0.05 0.96 Q7 1 -0.0203 0.3104 0.5140 11.00000 0.05 0.88 Q8 1 0.2433 0.3631 0.3871 11.00000 0.05 0.87 Q9 1 0.1898 -0.1868 0.5589 11.00000 0.05 0.85 Q10 1 0.2569 0.3644 0.2504 11.00000 0.05 0.83 Q11 1 0.1667 0.3742 0.3585 11.00000 0.05 0.82 Q12 1 0.2089 0.8393 0.3698 11.00000 0.05 0.78 Q13 1 0.3314 0.4197 0.3888 11.00000 0.05 0.73 Q14 1 0.0474 0.1240 0.2576 11.00000 0.05 0.72 Q15 1 0.2834 -0.0329 0.5610 11.00000 0.05 0.68 Q16 1 0.1583 0.3655 0.5302 11.00000 0.05 0.68 Q17 1 0.0790 0.3366 0.3331 11.00000 0.05 0.63 Q18 1 0.3874 0.1840 0.3834 11.00000 0.05 0.62 Q19 1 0.1776 0.3224 0.4746 11.00000 0.05 0.62 Q20 1 0.1401 0.7021 0.3521 11.00000 0.05 0.62 ; _shelx_res_checksum 43333 _shelx_hkl_file ; 2 0 0 2493.05 248.38 -2 0 0 2730.93 248.48 2 0 0 2544.25 248.48 2 0 0 2668.23 248.38 3 0 0 5394.26 503.15 -3 0 0 5179.08 503.35 4 0 0 268.17 24.50 -4 0 0 252.57 24.70 -4 0 0 241.68 24.60 -5 0 0 144.49 13.70 5 0 0 129.79 13.50 -5 0 0 139.19 13.80 -6 0 0 228.48 21.00 6 0 0 214.38 20.60 -6 0 0 188.38 20.70 7 0 0 37.80 4.60 -7 0 0 37.00 4.80 -7 0 0 40.10 5.20 -8 0 0 496.65 54.19 -8 0 0 617.14 54.69 8 0 0 570.14 54.09 -9 0 0 3436.36 327.07 -9 0 0 3418.56 326.77 9 0 0 3418.86 326.57 -10 0 0 1284.27 133.29 10 0 0 1445.86 133.39 -10 0 0 1489.45 133.99 -10 0 0 1352.16 133.59 11 0 0 261.07 24.40 -11 0 0 218.58 24.60 -11 0 0 240.68 24.60 -11 0 0 258.27 24.80 -11 0 0 224.38 24.40 -11 0 0 229.58 24.20 -11 0 0 290.97 25.30 12 0 0 655.03 58.79 -12 0 0 646.14 59.19 -12 0 0 563.24 58.49 -12 0 0 649.93 59.09 -12 0 0 649.43 59.59 -12 0 0 585.34 59.19 -12 0 0 516.05 58.69 13 0 0 19.60 3.60 -13 0 0 18.10 3.10 -13 0 0 10.80 3.80 -13 0 0 18.70 4.10 -13 0 0 8.10 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39.10 -19 -4 0 405.76 39.60 -19 -4 0 406.96 41.20 19 -4 0 386.46 39.00 -19 -4 0 398.26 39.40 -19 -4 0 384.06 40.90 -19 4 0 407.76 39.70 -19 4 0 376.66 39.00 -19 4 0 356.76 39.10 19 4 0 334.57 40.20 -20 -4 0 333.67 38.50 20 -4 0 377.36 36.80 -20 -4 0 336.07 38.30 -20 -4 0 356.66 37.00 -20 -4 0 352.96 37.20 20 -4 0 375.66 36.90 -20 4 0 362.46 37.40 -20 4 0 398.96 36.90 -20 4 0 382.56 37.00 20 4 0 311.47 38.20 21 -4 0 85.09 11.40 21 -4 0 85.59 12.20 -21 -4 0 76.59 13.60 -21 -4 0 59.99 12.30 -21 -4 0 83.09 11.60 -21 -4 0 78.09 11.60 -21 4 0 65.19 10.50 21 4 0 60.49 13.80 -21 4 0 51.89 10.00 22 -4 0 291.27 30.20 -22 -4 0 275.97 32.40 22 -4 0 286.47 31.20 -22 -4 0 331.37 30.80 -22 -4 0 274.57 30.30 -22 4 0 284.77 30.10 -22 4 0 244.48 29.70 -23 -4 0 112.49 15.90 23 -4 0 126.09 15.60 -23 -4 0 152.18 16.80 -23 4 0 79.59 13.70 -23 4 0 117.59 15.20 -24 -4 0 40.90 9.60 24 -4 0 62.39 10.70 -24 -4 0 63.09 11.30 -24 4 0 52.69 9.80 -24 4 0 42.90 9.30 25 -4 0 405.26 42.30 -25 -4 0 383.76 42.40 -25 -4 0 392.76 42.40 -25 4 0 426.16 42.20 0 -5 0 1.80 1.40 0 5 0 4.50 1.50 0 5 0 3.80 2.00 1 -5 0 1292.67 115.59 -1 -5 0 1296.27 115.49 -1 5 0 1183.68 115.99 -1 5 0 1130.59 115.39 1 5 0 1078.59 116.19 1 5 0 1259.57 115.39 -2 -5 0 742.23 75.39 2 -5 0 714.43 75.69 -2 5 0 809.82 75.59 -2 5 0 827.52 75.99 2 5 0 770.32 76.59 2 5 0 850.11 75.59 -3 -5 0 1122.09 107.99 3 -5 0 1163.08 108.39 -3 5 0 1173.68 108.29 3 5 0 1137.69 108.09 3 5 0 1045.00 109.29 -4 -5 0 2650.63 225.18 4 -5 0 2131.39 224.28 -4 -5 0 2114.59 223.88 -4 5 0 2328.37 224.28 -4 5 0 2596.44 224.38 -4 5 0 2313.27 224.28 4 5 0 2336.67 224.08 5 -5 0 81.89 9.40 -5 -5 0 62.19 9.50 -5 -5 0 59.19 9.50 -5 -5 0 98.29 11.50 -5 -5 0 68.29 8.10 -5 -5 0 75.59 9.80 5 -5 0 97.79 9.00 -5 5 0 95.29 9.60 -5 5 0 96.59 9.00 5 5 0 78.79 8.60 -5 5 0 82.49 8.50 6 -5 0 1538.65 137.09 -6 -5 0 1535.25 137.49 -6 -5 0 1357.36 138.09 -6 -5 0 1335.47 137.19 -6 -5 0 1242.28 137.59 -6 5 0 1454.15 136.89 -6 5 0 1417.76 136.99 -6 5 0 1383.16 136.69 -6 5 0 1637.74 137.19 -7 -5 0 5.10 3.10 7 -5 0 8.40 2.50 -7 -5 0 10.10 1.90 7 -5 0 7.50 2.70 -7 -5 0 7.20 3.80 -7 -5 0 8.70 2.90 -7 -5 0 10.70 3.40 -7 5 0 11.90 3.30 -7 5 0 13.40 3.10 -7 5 0 10.50 2.90 7 5 0 7.20 3.00 7 5 0 12.80 2.90 -7 5 0 9.30 2.00 -8 -5 0 220.68 24.60 -8 -5 0 223.68 24.00 8 -5 0 260.77 23.90 8 -5 0 234.98 23.60 -8 -5 0 234.18 25.00 8 -5 0 259.57 24.50 -8 -5 0 230.98 23.90 -8 -5 0 216.48 22.90 8 5 0 218.78 23.60 -8 5 0 257.97 23.60 -8 5 0 266.17 23.90 8 5 0 253.27 23.70 -8 5 0 220.28 23.10 9 -5 0 1318.67 135.29 -9 -5 0 1294.47 136.29 9 -5 0 1418.26 135.39 -9 -5 0 1310.97 136.49 -9 -5 0 1430.66 135.59 -9 -5 0 1325.87 134.59 9 -5 0 1559.44 135.49 -9 5 0 1269.77 134.89 -9 5 0 1512.45 135.59 9 5 0 1500.65 135.29 -9 5 0 1445.16 135.29 9 5 0 1529.25 135.29 -9 5 0 1457.85 135.09 -9 5 0 1424.56 135.09 10 -5 0 415.86 38.40 -10 -5 0 374.86 37.20 -10 -5 0 346.77 39.30 10 -5 0 365.86 38.00 -10 -5 0 312.27 38.70 10 -5 0 410.26 38.20 -10 -5 0 431.46 38.50 -10 -5 0 360.86 38.20 -10 5 0 384.56 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12.10 -19 -5 0 82.39 11.50 -19 -5 0 68.69 11.90 19 -5 0 76.69 10.70 -19 5 0 61.09 10.40 -19 5 0 66.09 10.50 -19 5 0 79.99 11.20 -20 -5 0 11.30 6.80 -20 -5 0 1.80 5.00 -20 -5 0 6.70 4.60 20 -5 0 -5.10 4.70 20 -5 0 2.50 4.90 -20 5 0 2.60 4.50 -20 5 0 8.00 5.60 -20 5 0 5.40 5.60 -21 -5 0 323.57 40.30 -21 -5 0 411.46 39.10 21 -5 0 388.96 38.50 21 -5 0 431.66 39.00 -21 5 0 332.77 38.20 -21 5 0 380.46 38.20 -22 -5 0 39.40 10.30 22 -5 0 18.40 7.20 -22 -5 0 40.70 8.30 -22 5 0 22.10 6.40 -22 5 0 24.90 6.80 23 -5 0 183.58 23.00 -23 -5 0 201.58 26.80 -23 -5 0 169.68 23.30 -23 5 0 196.28 22.80 -23 5 0 213.08 23.60 24 -5 0 153.68 18.70 -24 -5 0 133.29 19.00 -24 5 0 137.99 18.30 -24 5 0 148.99 18.40 -25 -5 0 86.09 13.10 25 -5 0 63.59 12.20 -25 5 0 72.69 11.70 -25 5 0 60.39 11.80 0 -6 0 26.10 5.20 0 -6 0 25.40 3.90 0 6 0 29.80 4.00 0 6 0 23.70 5.30 0 6 0 28.30 4.90 0 6 0 36.40 5.00 -1 -6 0 288.37 30.30 1 -6 0 278.27 30.20 -1 -6 0 316.47 29.50 1 -6 0 303.27 29.60 1 6 0 266.97 29.80 -1 6 0 284.57 29.70 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16.90 5.10 -18 6 0 8.20 5.40 -18 6 0 7.90 5.00 18 6 0 13.90 5.10 -19 -6 0 14.80 7.30 -19 -6 0 14.40 5.10 -19 -6 0 16.40 6.80 19 -6 0 8.30 4.80 19 -6 0 21.20 6.60 -19 6 0 17.10 6.10 -19 6 0 26.30 7.10 -19 6 0 19.60 6.00 19 6 0 10.50 5.40 20 -6 0 10.90 6.20 -20 -6 0 1.40 4.00 20 -6 0 7.80 5.40 -20 -6 0 8.90 7.30 -20 -6 0 5.00 7.60 20 6 0 5.60 5.20 -20 6 0 14.10 5.90 -20 6 0 17.00 5.50 -21 -6 0 21.10 8.50 -21 -6 0 11.30 5.20 21 -6 0 15.90 6.70 -21 6 0 15.90 6.30 21 6 0 8.10 5.80 -21 6 0 15.40 6.30 22 -6 0 126.59 15.90 -22 -6 0 123.19 16.30 -22 -6 0 118.59 18.80 22 6 0 88.39 14.60 -22 6 0 110.79 15.00 -22 6 0 97.09 14.80 -23 -6 0 19.60 6.90 23 -6 0 9.60 7.10 -23 -6 0 24.60 9.80 23 6 0 14.90 8.00 -23 6 0 15.30 7.10 -23 6 0 28.50 7.80 -24 -6 0 5.80 5.50 24 -6 0 23.50 7.60 -24 -6 0 12.60 9.50 -24 6 0 8.40 6.60 -24 6 0 -2.20 5.90 24 6 0 14.50 8.10 0 -7 0 2.40 2.00 0 -7 0 1.60 3.10 0 7 0 3.60 1.80 0 7 0 6.10 2.60 0 7 0 3.20 2.40 0 7 0 5.80 2.70 1 -7 0 212.78 18.70 -1 -7 0 147.89 19.20 -1 -7 0 178.48 20.50 1 -7 0 185.08 18.80 1 -7 0 200.78 19.50 -1 -7 0 186.68 18.40 -1 7 0 182.18 18.50 1 7 0 170.38 18.30 1 7 0 187.08 19.00 1 7 0 147.29 19.30 -1 7 0 190.08 18.90 1 7 0 176.38 18.60 -1 7 0 210.18 19.40 -1 7 0 201.88 18.80 -2 -7 0 5.50 4.30 2 -7 0 5.40 3.60 -2 -7 0 5.60 2.10 2 -7 0 3.20 2.80 2 -7 0 3.70 2.10 -2 -7 0 0.00 3.10 2 7 0 6.40 2.90 -2 7 0 6.70 2.90 2 7 0 3.30 2.00 -2 7 0 3.20 2.40 2 7 0 2.20 2.30 -2 7 0 1.10 2.10 -2 7 0 2.00 2.30 2 7 0 4.00 2.70 -3 -7 0 98.59 11.40 3 -7 0 116.09 11.90 3 -7 0 110.69 13.30 -3 -7 0 114.69 13.20 3 -7 0 81.19 11.90 -3 -7 0 138.39 14.10 3 7 0 107.19 14.30 -3 7 0 119.59 12.20 3 7 0 113.19 11.90 -3 7 0 109.39 11.70 -3 7 0 107.29 12.40 3 7 0 105.49 11.50 3 7 0 100.59 12.50 -3 7 0 124.49 12.30 4 -7 0 209.38 22.40 4 -7 0 225.48 22.50 4 -7 0 196.38 22.90 -4 -7 0 220.48 22.00 -4 -7 0 190.58 22.90 4 7 0 217.78 22.30 4 7 0 213.68 23.90 4 7 0 231.18 22.10 4 7 0 237.48 22.90 -4 7 0 229.88 22.50 -4 7 0 248.18 22.50 -4 7 0 213.58 22.40 -4 7 0 239.78 22.60 5 -7 0 85.29 9.80 -5 -7 0 79.09 8.50 5 -7 0 93.09 10.70 -5 -7 0 76.49 10.40 -5 -7 0 50.49 10.50 5 -7 0 73.09 9.40 5 7 0 76.59 9.90 5 7 0 76.09 11.50 -5 7 0 78.09 9.60 -5 7 0 96.09 9.80 5 7 0 85.69 9.30 -5 7 0 79.59 9.40 -5 7 0 97.29 10.00 5 7 0 85.89 9.60 -5 7 0 76.49 9.00 6 -7 0 410.16 37.60 6 -7 0 384.86 37.50 -6 -7 0 429.96 38.30 -6 -7 0 384.96 36.80 6 -7 0 327.67 37.60 -6 7 0 354.26 37.10 -6 7 0 449.46 37.60 -6 7 0 379.66 37.20 6 7 0 388.36 37.30 6 7 0 347.17 37.00 -6 7 0 383.66 37.30 6 7 0 321.27 38.80 -6 7 0 395.76 37.50 6 7 0 371.16 37.70 -7 -7 0 43.90 9.10 -7 -7 0 60.09 6.70 7 -7 0 52.19 7.60 7 -7 0 48.70 7.40 -7 -7 0 48.80 8.20 7 -7 0 72.59 8.80 -7 7 0 63.69 9.30 -7 7 0 57.49 7.70 -7 7 0 57.89 7.70 -7 7 0 49.90 7.20 -7 7 0 52.09 7.40 7 7 0 52.89 8.10 7 7 0 70.09 7.90 7 7 0 74.89 7.80 -8 -7 0 8.00 4.20 -8 -7 0 11.60 4.50 -8 -7 0 14.80 5.60 -8 -7 0 14.40 4.60 8 -7 0 11.70 4.40 -8 -7 0 8.70 2.30 8 -7 0 15.40 3.90 8 -7 0 12.70 3.40 -8 7 0 13.90 3.80 8 7 0 12.30 3.50 -8 7 0 11.50 3.60 -8 7 0 16.40 3.50 -8 7 0 10.50 3.70 8 7 0 18.70 3.90 9 -7 0 30.20 5.40 -9 -7 0 33.20 6.20 -9 -7 0 24.80 3.90 -9 -7 0 23.60 6.70 9 -7 0 25.20 5.80 9 -7 0 23.50 4.90 -9 -7 0 28.60 5.80 -9 -7 0 21.60 5.80 9 7 0 35.60 5.80 -9 7 0 30.80 5.20 -9 7 0 31.00 5.30 9 7 0 42.00 5.90 -9 7 0 27.70 5.40 -9 7 0 29.20 4.70 10 -7 0 84.09 11.70 -10 -7 0 126.49 13.10 10 -7 0 107.09 11.80 -10 -7 0 115.49 14.00 -10 -7 0 70.19 12.90 10 -7 0 91.29 11.90 -10 -7 0 69.99 11.40 -10 7 0 93.09 10.90 10 7 0 115.59 12.10 10 7 0 111.79 11.80 -10 7 0 110.69 12.30 -10 7 0 84.29 11.00 -10 7 0 74.19 10.90 11 -7 0 238.68 24.90 11 -7 0 262.97 24.60 11 -7 0 218.98 24.40 -11 -7 0 242.48 25.00 -11 -7 0 173.88 25.20 -11 -7 0 271.17 25.10 -11 -7 0 242.18 26.50 11 7 0 247.88 24.40 -11 7 0 281.77 24.50 -11 7 0 251.57 24.80 -11 7 0 218.18 24.20 -11 7 0 223.88 23.90 11 7 0 223.38 24.60 12 -7 0 128.39 15.90 12 -7 0 148.99 17.00 12 -7 0 111.09 15.50 -12 -7 0 135.39 16.70 -12 -7 0 129.79 17.90 -12 -7 0 139.59 19.00 -12 -7 0 141.49 15.70 -12 7 0 151.48 16.70 -12 7 0 118.89 15.60 -12 7 0 135.79 14.90 -12 7 0 152.28 15.90 12 7 0 156.58 15.50 13 -7 0 235.88 21.00 -13 -7 0 166.68 21.00 -13 -7 0 170.58 22.50 -13 -7 0 167.48 21.50 13 -7 0 155.28 20.90 -13 -7 0 214.78 22.50 -13 7 0 190.68 20.50 -13 7 0 201.38 21.00 -13 7 0 206.68 20.60 13 7 0 213.68 20.70 -13 7 0 198.78 20.60 14 -7 0 106.59 13.90 -14 -7 0 121.39 17.40 -14 -7 0 93.49 15.50 14 -7 0 118.29 14.50 -14 -7 0 130.79 15.20 -14 -7 0 147.99 15.70 14 7 0 125.89 14.60 -14 7 0 128.39 15.10 -14 7 0 112.99 14.00 -14 7 0 96.79 13.80 -15 -7 0 73.49 10.50 -15 -7 0 54.49 10.60 -15 -7 0 51.29 9.50 15 -7 0 66.09 9.50 15 -7 0 57.89 9.40 -15 -7 0 68.99 12.40 -15 7 0 61.39 9.20 15 7 0 76.99 10.00 -15 7 0 64.29 9.40 -15 7 0 74.59 10.50 16 -7 0 301.07 32.50 -16 -7 0 329.77 33.00 -16 -7 0 315.07 32.90 -16 -7 0 334.97 34.60 -16 -7 0 279.77 34.50 16 -7 0 334.07 32.60 -16 7 0 315.37 32.20 -16 7 0 340.57 33.10 -16 7 0 310.97 32.40 16 7 0 296.27 32.50 -17 -7 0 17.10 7.10 -17 -7 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156.38 3 8 0 1689.53 156.18 -3 8 0 1618.04 156.28 3 8 0 1664.83 158.08 -3 8 0 1562.24 156.58 -4 -8 0 1458.95 145.49 4 -8 0 1385.76 144.49 4 -8 0 1570.94 144.19 -4 -8 0 1408.66 144.59 4 -8 0 1616.64 144.19 -4 8 0 1583.34 144.09 4 8 0 1575.74 144.49 4 8 0 1554.14 143.79 -4 8 0 1522.85 144.29 -4 8 0 1502.45 144.09 -4 8 0 1560.94 143.59 4 8 0 1477.65 143.99 -4 8 0 1480.75 143.99 4 8 0 1294.67 145.39 5 -8 0 796.32 81.79 -5 -8 0 816.32 81.19 5 -8 0 782.72 81.69 5 -8 0 892.81 82.39 -5 -8 0 973.80 82.79 -5 8 0 908.31 81.79 5 8 0 873.91 81.69 5 8 0 848.42 81.39 -5 8 0 835.82 81.89 -5 8 0 903.31 81.89 5 8 0 910.51 82.29 -5 8 0 758.72 81.19 5 8 0 720.23 83.19 -5 8 0 836.82 81.69 -6 -8 0 2.20 1.70 6 -8 0 1.70 3.00 6 -8 0 0.80 2.50 -6 -8 0 4.70 3.70 -6 -8 0 2.40 4.80 6 -8 0 3.40 3.60 -6 8 0 2.20 2.80 6 8 0 -0.10 2.90 -6 8 0 -1.20 2.90 6 8 0 0.90 2.50 -6 8 0 1.80 2.80 6 8 0 3.70 3.10 6 8 0 -0.90 3.00 -6 8 0 -0.20 2.30 7 -8 0 1088.59 109.99 -7 -8 0 1070.09 111.69 7 -8 0 1150.48 109.99 7 -8 0 1085.69 110.29 -7 8 0 1206.08 109.79 7 8 0 1150.18 109.79 7 8 0 1077.29 110.19 7 8 0 1049.30 111.89 -7 8 0 1180.98 109.59 7 8 0 1174.88 109.69 -7 8 0 1144.99 109.89 -7 8 0 1266.17 110.09 -8 -8 0 57.69 9.30 8 -8 0 68.79 8.60 -8 -8 0 85.69 12.20 -8 -8 0 58.09 8.10 8 -8 0 55.19 8.40 8 -8 0 56.39 8.70 -8 8 0 51.19 8.20 8 8 0 48.80 10.30 -8 8 0 66.19 8.10 -8 8 0 56.09 8.20 8 8 0 67.29 8.30 -8 8 0 50.49 7.70 8 8 0 69.69 8.40 8 8 0 58.89 8.60 9 -8 0 368.06 38.80 9 -8 0 397.06 38.80 -9 -8 0 414.26 41.10 9 -8 0 355.56 39.00 -9 -8 0 363.26 39.30 9 8 0 324.47 38.90 -9 8 0 410.86 38.40 -9 8 0 395.96 38.50 -9 8 0 399.16 38.70 -9 8 0 414.96 38.90 9 8 0 356.76 41.00 9 8 0 459.45 38.90 -10 -8 0 304.37 26.90 10 -8 0 247.48 26.30 -10 -8 0 250.97 28.10 10 -8 0 199.58 25.50 -10 -8 0 326.57 27.20 10 -8 0 256.67 26.00 -10 8 0 264.37 25.70 10 8 0 246.48 25.80 -10 8 0 248.68 26.00 -10 8 0 238.88 25.60 -10 8 0 223.08 25.30 11 -8 0 10.80 4.40 -11 -8 0 15.60 4.70 -11 -8 0 20.90 7.10 11 -8 0 12.50 4.40 11 -8 0 20.60 5.80 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10.80 -10 -11 4 72.19 12.10 -10 -11 4 100.59 15.60 -10 11 4 85.69 11.50 10 11 -4 72.39 14.10 10 11 -4 49.70 10.90 -10 11 4 71.59 10.90 9 -11 -4 105.59 14.00 -9 -11 4 113.09 15.60 -9 -11 4 125.19 18.00 9 -11 -4 119.29 14.30 9 -11 -4 114.29 15.50 -9 11 4 111.39 14.20 9 11 -4 85.89 16.10 -9 11 4 124.59 14.80 9 11 -4 101.99 14.90 8 -11 -4 6.30 4.90 -8 -11 4 13.70 5.60 8 -11 -4 6.70 4.10 -8 -11 4 5.20 6.80 8 -11 -4 4.80 4.50 8 11 -4 3.40 4.30 -8 11 4 10.00 5.00 -8 11 4 1.80 3.60 8 11 -4 9.30 5.30 -7 -11 4 196.48 23.90 7 -11 -4 215.98 22.40 -7 -11 4 150.28 22.30 -7 -11 4 209.58 20.50 7 -11 -4 206.38 21.80 7 -11 -4 214.38 21.40 -7 11 4 191.98 20.90 7 11 -4 220.28 21.20 7 11 -4 148.69 23.40 -7 11 4 210.68 21.40 7 11 -4 161.68 21.80 -6 -11 4 34.00 5.90 6 -11 -4 36.50 6.90 6 -11 -4 35.20 6.80 -6 -11 4 37.20 9.60 -6 -11 4 42.40 8.80 6 -11 -4 40.10 8.30 6 11 -4 35.20 8.30 -6 11 4 43.20 7.10 6 11 -4 29.90 6.60 6 11 -4 41.30 7.00 -6 11 4 36.50 6.50 5 -11 -4 17.50 4.70 -5 -11 4 11.00 3.70 5 -11 -4 15.00 6.00 -5 -11 4 15.50 7.70 -5 -11 4 13.40 5.70 5 -11 -4 6.90 4.50 5 11 -4 13.70 4.90 5 11 -4 9.90 5.70 5 11 -4 17.40 4.80 -5 11 4 12.00 4.40 -5 11 4 12.90 5.00 -4 -11 4 9.50 3.40 4 -11 -4 11.50 5.30 4 -11 -4 2.90 3.60 4 -11 -4 8.80 5.20 -4 -11 4 3.00 4.60 -4 -11 4 7.50 7.20 -4 -11 4 3.10 4.20 4 11 -4 11.40 4.30 -4 11 4 5.80 4.90 4 11 -4 3.00 3.80 -4 11 4 8.50 4.80 -4 11 4 3.80 3.60 4 11 -4 6.60 3.90 -3 -11 4 99.39 13.50 -3 -11 4 102.59 16.90 -3 -11 4 118.39 16.20 3 -11 -4 131.19 14.40 3 -11 -4 139.59 16.60 -3 -11 4 110.49 14.00 -3 11 4 141.99 15.10 -3 11 4 145.99 15.00 3 11 -4 114.49 13.90 -3 11 4 120.69 14.60 3 11 -4 102.29 16.10 3 11 -4 125.99 15.30 2 -11 -4 9.80 5.30 -2 -11 4 18.40 4.70 2 -11 -4 21.90 5.10 -2 -11 4 21.70 8.70 -2 -11 4 22.60 6.90 -2 -11 4 18.70 5.00 2 11 -4 18.20 5.90 2 11 -4 24.60 5.40 2 11 -4 19.00 5.20 -2 11 4 16.10 5.40 -2 11 4 21.40 5.30 -2 11 4 25.00 5.30 -1 -11 4 31.30 6.10 1 -11 -4 35.40 6.10 -1 -11 4 32.20 6.00 -1 -11 4 35.10 7.70 1 -11 -4 25.50 7.00 1 11 -4 28.30 6.20 -1 11 4 22.30 5.70 -1 11 4 32.90 6.20 1 11 -4 29.40 5.90 -1 11 4 31.50 6.20 1 11 -4 25.50 7.00 0 -11 -4 131.19 19.10 0 -11 4 142.99 16.30 0 -11 4 152.88 18.10 0 -11 -4 143.99 18.10 0 -11 4 129.89 16.30 0 11 -4 160.18 17.50 0 11 4 141.59 16.60 0 11 4 105.99 15.90 0 11 4 135.39 16.60 0 11 -4 158.88 16.60 0 11 -4 163.18 17.50 1 -11 4 9.00 4.30 1 -11 4 16.00 6.10 1 -11 4 9.50 4.50 -1 -11 -4 13.90 5.50 -1 -11 -4 6.40 6.70 1 11 4 22.60 5.20 1 11 4 14.30 7.30 -1 11 -4 14.70 5.70 -1 11 -4 9.90 4.30 1 11 4 12.90 4.90 1 11 4 14.70 4.70 -1 11 -4 10.70 4.60 2 -11 4 109.69 14.90 -2 -11 -4 105.89 16.30 2 -11 4 106.49 13.50 2 -11 4 112.99 13.80 -2 -11 -4 116.09 15.70 -2 11 -4 113.29 13.20 2 11 4 127.99 14.00 2 11 4 100.49 13.40 2 11 4 120.19 14.30 2 11 4 118.79 16.60 -2 11 -4 87.69 13.20 -3 -11 -4 89.19 16.00 3 -11 4 150.28 15.10 -3 -11 -4 97.69 15.20 3 -11 4 119.29 14.30 3 -11 4 135.89 16.00 3 11 4 99.79 13.70 3 11 4 95.09 13.80 3 11 4 158.38 18.70 3 11 4 129.59 16.40 -3 11 -4 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11.20 -14 -11 -4 19.90 8.40 -14 -11 -4 29.20 8.90 14 -11 4 32.10 7.40 -14 11 -4 19.00 7.80 -14 11 -4 15.80 8.30 14 11 4 30.70 7.60 -14 11 -4 21.60 6.70 -15 -11 -4 5.70 7.60 -15 -11 -4 2.80 7.50 15 -11 4 6.90 5.50 -15 11 -4 13.10 7.00 15 11 4 4.90 6.60 -15 11 -4 1.10 5.10 -16 -11 -4 283.07 29.20 16 -11 4 199.78 24.60 -16 -11 -4 152.58 24.70 16 11 4 182.28 23.80 -16 11 -4 214.58 24.40 -16 11 -4 199.98 23.90 -17 -11 -4 8.70 8.30 -17 -11 -4 -4.10 7.00 17 -11 4 -5.60 6.70 17 11 4 6.80 5.60 -17 11 -4 1.90 6.70 -17 11 -4 8.80 5.60 18 -11 4 61.79 13.10 -18 -11 -4 94.99 17.70 -18 -11 -4 97.49 15.60 -18 11 -4 88.59 12.90 18 11 4 56.09 11.50 -18 11 -4 64.89 11.60 -19 -12 4 167.38 21.50 -19 -12 4 163.08 25.80 19 -12 -4 131.29 19.60 -19 12 4 128.99 18.70 19 12 -4 161.58 21.50 -19 12 4 166.48 20.00 -18 -12 4 116.29 15.80 18 -12 -4 68.79 12.80 -18 -12 4 78.69 17.70 18 12 -4 117.69 16.40 -18 12 4 111.99 14.70 -18 12 4 62.09 12.00 -17 -12 4 357.36 37.70 17 -12 -4 325.17 36.50 -17 12 4 333.37 36.20 17 12 -4 354.26 37.70 -17 12 4 361.86 36.90 -16 -12 4 5.30 8.00 16 -12 -4 3.90 5.50 -16 -12 4 -0.80 5.80 -16 12 4 8.60 7.10 -16 12 4 3.00 5.40 16 12 -4 10.80 6.90 -15 -12 4 365.96 45.70 -15 -12 4 420.86 43.50 15 -12 -4 419.06 43.60 15 -12 -4 468.95 42.60 -15 12 4 370.56 41.50 15 12 -4 354.46 42.90 -15 12 4 486.35 42.70 14 -12 -4 271.97 29.20 14 -12 -4 280.07 29.50 -14 -12 4 270.57 29.20 -14 -12 4 223.48 32.60 -14 12 4 218.98 28.10 -14 12 4 267.77 28.80 14 12 -4 271.17 30.20 13 -12 -4 108.39 15.10 -13 -12 4 141.69 17.40 -13 -12 4 142.39 20.90 13 -12 -4 110.19 16.90 -13 12 4 95.89 14.30 13 12 -4 103.89 16.20 -12 -12 4 185.58 25.40 12 -12 -4 254.27 25.80 -12 -12 4 235.78 30.20 12 -12 -4 220.08 25.00 -12 12 4 213.88 25.30 12 12 -4 258.87 27.30 -12 12 4 184.08 24.60 11 -12 -4 36.50 7.80 11 -12 -4 36.40 7.90 -11 -12 4 39.70 9.10 -11 -12 4 46.20 11.90 11 -12 -4 28.60 8.60 -11 12 4 40.40 8.70 11 12 -4 34.80 10.80 11 12 -4 40.40 8.90 -11 12 4 48.10 8.50 10 -12 -4 383.76 37.60 -10 -12 4 311.77 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131.99 13.40 -4 -4 9 130.79 13.30 4 -4 -9 143.99 14.30 4 -4 -9 113.19 13.10 -4 -4 9 120.79 14.60 -4 -4 9 125.59 13.20 4 4 -9 118.49 14.40 4 4 -9 136.49 14.00 4 4 -9 172.28 16.50 -4 4 9 135.59 13.60 -4 4 9 110.49 13.40 -4 4 9 128.79 13.50 3 -4 -9 96.49 10.30 -3 -4 9 98.89 10.40 -3 -4 9 86.89 10.70 3 -4 -9 94.09 11.70 3 -4 -9 91.09 10.60 -3 -4 9 124.79 12.60 3 -4 -9 99.09 12.60 -3 4 9 102.29 10.70 3 4 -9 133.39 13.70 -3 4 9 103.99 10.70 -3 4 9 72.49 10.90 3 4 -9 88.39 12.10 3 4 -9 117.79 11.40 2 -4 -9 6.00 2.00 2 -4 -9 8.00 4.10 -2 -4 9 4.20 2.40 -2 -4 9 9.60 2.40 2 -4 -9 9.00 2.80 2 -4 -9 11.00 3.50 2 4 -9 2.70 3.00 -2 4 9 6.50 2.60 2 4 -9 6.10 2.80 2 4 -9 9.00 5.50 -2 4 9 6.90 2.30 -2 4 9 8.00 2.90 -1 -4 9 4.20 1.80 -1 -4 9 -1.00 2.10 1 -4 -9 7.30 1.70 1 -4 -9 3.10 3.10 1 -4 -9 5.60 3.70 1 -4 -9 6.50 2.40 -1 4 9 2.70 2.20 -1 4 9 5.50 2.70 1 4 -9 6.10 6.30 -1 4 9 2.40 1.80 1 4 -9 3.20 2.80 1 4 -9 2.20 2.10 0 -4 9 358.56 34.10 0 -4 9 318.47 34.30 0 -4 9 362.86 34.30 0 -4 -9 314.97 35.50 0 -4 -9 341.57 33.90 0 4 9 383.96 34.50 0 4 9 372.16 34.80 0 4 -9 367.46 34.70 0 4 -9 309.57 35.10 0 4 9 384.76 34.40 1 -4 9 76.79 7.50 -1 -4 -9 82.29 10.10 -1 -4 -9 45.10 8.20 1 -4 9 58.09 7.70 1 -4 9 56.59 7.70 1 4 9 52.79 8.00 -1 4 -9 85.69 9.90 -1 4 -9 71.39 8.60 1 4 9 74.19 8.10 1 4 9 66.69 8.00 -2 -4 -9 139.09 14.90 2 -4 9 133.29 14.10 2 -4 9 144.69 14.30 -2 -4 -9 107.09 14.70 2 -4 9 135.79 14.20 -2 -4 -9 119.89 15.50 2 -4 9 146.59 14.10 2 4 9 155.68 14.40 2 4 9 145.29 14.70 -2 4 -9 147.79 14.60 -2 4 -9 123.69 14.80 2 4 9 153.18 14.30 -3 -4 -9 10.80 3.80 -3 -4 -9 12.00 4.70 3 -4 9 15.60 3.60 3 -4 9 19.00 3.30 3 -4 9 14.80 3.30 -3 -4 -9 11.20 3.80 3 -4 9 13.00 3.00 3 4 9 9.10 3.60 -3 4 -9 14.40 3.60 3 4 9 14.30 3.40 3 4 9 18.60 3.80 -3 4 -9 11.20 3.50 -3 4 -9 19.30 4.50 -4 -4 -9 631.24 58.79 4 -4 9 608.14 57.69 4 -4 9 596.74 57.49 -4 -4 -9 638.74 59.19 4 -4 9 626.24 57.59 4 -4 9 563.24 57.29 4 4 9 522.55 57.79 -4 4 -9 611.54 57.39 -4 4 -9 600.44 57.79 4 4 9 553.24 57.69 4 4 9 594.54 57.39 -4 4 -9 567.64 58.29 5 -4 9 2.80 2.30 5 -4 9 2.50 3.10 -5 -4 -9 -0.50 2.50 5 -4 9 -0.60 1.80 5 -4 9 6.20 2.80 -5 -4 -9 0.90 2.90 -5 -4 -9 4.50 3.40 -5 4 -9 3.30 2.70 5 4 9 4.20 2.70 -5 4 -9 1.10 2.30 5 4 9 0.50 2.00 5 4 9 -2.50 2.60 -5 4 -9 -0.20 2.60 6 -4 9 38.10 5.80 -6 -4 -9 40.20 7.20 6 -4 9 40.10 6.40 6 -4 9 38.30 6.00 -6 -4 -9 33.20 6.10 6 -4 9 48.00 6.60 -6 -4 -9 33.10 7.20 -6 4 -9 40.60 6.60 -6 4 -9 42.10 6.40 6 4 9 42.30 6.20 6 4 9 58.49 7.50 -6 4 -9 46.70 6.20 6 4 9 49.10 6.60 7 -4 9 79.09 8.80 -7 -4 -9 54.19 8.70 7 -4 9 56.29 8.60 7 -4 9 58.19 8.70 -7 -4 -9 58.99 9.90 -7 -4 -9 77.19 11.00 7 -4 9 65.99 8.80 -7 4 -9 74.09 9.70 7 4 9 68.89 9.30 -7 4 -9 77.19 9.00 -7 4 -9 86.69 9.50 7 4 9 58.69 8.50 7 4 9 77.59 9.00 8 -4 9 290.87 27.70 -8 -4 -9 259.27 28.00 8 -4 9 286.07 27.40 8 -4 9 287.57 28.20 -8 -4 -9 312.57 29.70 8 -4 9 272.67 27.70 -8 -4 -9 251.67 28.80 -8 4 -9 276.57 27.60 8 4 9 242.58 28.10 8 4 9 268.27 27.60 -8 4 -9 266.27 28.20 8 4 9 255.07 27.70 -8 4 -9 288.07 27.90 9 -4 9 6.30 3.90 9 -4 9 7.40 3.20 -9 -4 -9 0.20 3.60 -9 -4 -9 -0.30 2.80 -9 -4 -9 1.60 3.20 9 -4 9 5.90 3.20 9 -4 9 16.40 5.00 9 4 9 1.60 3.80 9 4 9 -1.70 2.50 9 4 9 -2.20 3.20 -9 4 -9 4.20 2.80 -9 4 -9 5.90 3.00 -9 4 -9 4.30 3.20 10 -4 9 6.30 4.40 10 -4 9 2.00 3.70 -10 -4 -9 -0.20 3.40 -10 -4 -9 4.40 5.00 -10 -4 -9 3.50 3.10 10 -4 9 8.20 3.30 10 -4 9 8.90 3.70 10 4 9 4.60 3.20 -10 4 -9 6.10 3.40 10 4 9 8.00 3.60 10 4 9 5.20 4.00 -10 4 -9 3.70 3.00 -10 4 -9 6.40 3.20 11 -4 9 6.40 3.70 -11 -4 -9 6.00 4.30 -11 -4 -9 0.10 3.80 11 -4 9 7.50 4.80 11 -4 9 4.00 3.20 -11 -4 -9 3.40 3.50 11 -4 9 2.90 3.70 -11 4 -9 2.70 3.30 -11 4 -9 5.00 3.10 11 4 9 2.40 3.70 11 4 9 -0.20 3.30 11 4 9 5.80 3.90 -11 4 -9 3.70 3.10 12 -4 9 75.29 10.30 12 -4 9 76.19 11.40 12 -4 9 55.69 10.60 -12 -4 -9 65.39 12.10 12 -4 9 77.79 9.90 -12 -4 -9 105.99 13.50 -12 -4 -9 76.29 11.00 12 4 9 85.29 11.40 12 4 9 76.49 10.30 12 4 9 63.99 10.10 -12 4 -9 68.89 10.30 -12 4 -9 87.29 11.60 -12 4 -9 75.89 10.30 13 -4 9 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18 5 -9 8.90 5.60 -18 5 9 8.80 4.30 -17 -5 9 79.89 10.10 -17 -5 9 88.99 12.10 17 -5 -9 98.39 12.90 17 -5 -9 85.19 11.20 -17 -5 9 109.29 15.00 -17 -5 9 78.09 10.10 -17 5 9 68.39 10.50 -17 5 9 86.49 11.70 17 5 -9 87.59 11.70 -17 5 9 83.29 10.70 -17 5 9 66.09 10.50 17 5 -9 70.09 13.10 -16 -5 9 9.60 3.10 -16 -5 9 10.10 6.00 -16 -5 9 5.50 4.20 16 -5 -9 13.70 5.40 16 -5 -9 2.20 4.10 -16 -5 9 2.80 2.60 -16 5 9 10.70 4.10 16 5 -9 9.40 4.80 -16 5 9 9.30 4.30 -16 5 9 7.10 3.60 -16 5 9 7.20 4.10 16 5 -9 6.20 5.10 -15 -5 9 1.10 4.10 -15 -5 9 0.90 2.20 15 -5 -9 4.60 2.80 15 -5 -9 3.40 4.60 -15 -5 9 2.10 3.50 -15 -5 9 3.10 2.60 15 5 -9 2.30 4.60 -15 5 9 0.40 2.60 -15 5 9 -1.90 3.20 -15 5 9 5.90 3.60 -15 5 9 0.40 3.30 15 5 -9 1.80 4.20 14 -5 -9 304.27 29.20 -14 -5 9 320.37 28.60 -14 -5 9 246.68 29.40 -14 -5 9 261.07 30.80 -14 -5 9 289.87 28.40 14 -5 -9 266.87 29.80 -14 5 9 309.87 28.90 -14 5 9 271.67 29.20 14 5 -9 307.07 29.40 -14 5 9 259.47 28.70 14 5 -9 308.27 31.10 -14 5 9 284.17 28.90 -13 -5 9 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553.94 53.39 -9 -5 9 566.84 53.49 -9 -5 9 598.94 55.89 9 -5 -9 525.35 53.69 9 -5 -9 565.24 54.59 9 5 -9 513.05 55.09 -9 5 9 563.24 53.59 -9 5 9 573.24 53.59 9 5 -9 480.15 53.79 -9 5 9 567.94 53.99 -8 -5 9 605.64 65.29 -8 -5 9 757.62 64.69 8 -5 -9 695.63 65.59 8 -5 -9 607.54 64.59 -8 -5 9 699.13 64.59 8 5 -9 660.53 64.99 -8 5 9 685.73 64.69 -8 5 9 602.04 64.49 -8 5 9 656.33 64.59 -8 5 9 708.83 65.09 7 -5 -9 349.07 35.50 7 -5 -9 344.57 34.60 -7 -5 9 374.26 34.60 -7 -5 9 332.27 36.40 -7 -5 9 384.66 34.60 -7 -5 9 311.07 35.20 -7 5 9 417.26 34.80 7 5 -9 336.87 34.90 -7 5 9 299.17 34.40 -7 5 9 371.36 34.60 -7 5 9 352.36 34.90 6 -5 -9 1432.16 126.99 6 -5 -9 1187.68 127.89 -6 -5 9 1314.17 127.89 -6 -5 9 1493.05 127.29 6 -5 -9 1284.27 127.19 -6 5 9 1249.47 126.99 6 5 -9 1467.15 127.59 -6 5 9 1234.38 127.19 6 5 -9 1236.98 128.49 -6 5 9 1367.36 127.09 -6 5 9 1300.17 127.49 5 -5 -9 165.08 16.00 -5 -5 9 157.48 14.80 5 -5 -9 121.19 14.60 5 -5 -9 141.89 16.60 -5 -5 9 147.49 15.70 5 -5 -9 153.88 14.80 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13 14 179.48 20.60 12 -13 -14 238.18 29.80 -12 -13 14 224.88 28.50 12 13 -14 183.88 26.90 12 13 -14 271.27 35.60 -12 13 14 261.47 26.10 11 -13 -14 182.88 25.50 -11 -13 14 257.17 26.70 -11 13 14 200.58 23.30 11 13 -14 209.08 30.20 11 13 -14 150.38 23.30 10 -13 -14 227.18 27.80 -10 -13 14 236.98 27.00 10 13 -14 220.68 31.60 10 13 -14 147.79 23.80 -10 13 14 232.68 25.10 -9 -13 14 25.00 6.20 9 -13 -14 37.40 9.00 -9 -13 14 21.20 8.50 9 13 -14 13.80 7.10 9 13 -14 10.40 10.30 -9 13 14 21.80 6.80 8 -13 -14 98.39 15.40 -8 -13 14 80.59 14.20 -8 -13 14 66.19 11.10 8 13 -14 109.69 20.00 -8 13 14 82.59 12.20 8 13 -14 60.49 12.30 -7 -13 14 63.29 12.20 7 -13 -14 48.80 11.20 -7 -13 14 55.89 9.30 7 13 -14 49.40 15.10 7 13 -14 52.59 9.90 -7 13 14 53.79 10.10 -6 -13 14 4.50 4.90 -6 -13 14 6.70 7.50 6 -13 -14 -0.40 4.40 6 13 -14 -1.50 4.70 -6 13 14 -4.70 4.30 -5 -13 14 101.69 16.50 -5 -13 14 137.89 15.20 5 -13 -14 86.59 15.90 5 13 -14 99.19 14.90 -5 13 14 120.39 15.10 4 -13 -14 105.69 17.60 -4 -13 14 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76.09 -5 0 16 783.92 76.29 5 0 -16 903.21 77.89 4 0 -16 15.40 4.90 4 0 -16 28.70 5.50 4 0 -16 23.50 5.60 -4 0 16 23.80 4.40 -4 0 16 25.70 4.70 -4 0 16 21.90 4.40 -4 0 16 27.10 4.20 4 0 -16 23.20 6.30 3 0 -16 384.86 41.70 3 0 -16 424.86 42.30 -3 0 16 419.66 41.60 3 0 -16 494.75 44.30 3 0 -16 447.46 43.20 -3 0 16 402.36 41.90 -3 0 16 430.36 41.80 -3 0 16 420.76 41.70 2 0 -16 945.01 83.19 2 0 -16 855.51 84.39 2 0 -16 746.93 83.29 -2 0 16 840.82 82.79 -2 0 16 873.21 83.29 2 0 -16 932.61 85.39 -2 0 16 833.62 82.89 -2 0 16 873.21 83.09 -1 0 16 30.60 4.60 1 0 -16 40.50 5.60 -1 0 16 28.50 5.00 -1 0 16 24.40 4.80 1 0 -16 19.30 6.10 1 0 -16 35.30 6.60 1 0 -16 29.60 6.50 -1 0 16 31.80 5.30 0 0 16 317.47 33.20 0 0 16 335.27 32.90 0 0 -16 351.36 33.40 0 0 16 325.97 32.80 0 0 16 351.56 33.60 0 0 -16 282.97 34.30 0 0 -16 379.16 35.40 0 0 16 334.77 33.00 1 0 16 243.28 27.30 1 0 16 259.47 27.00 -1 0 -16 311.87 29.40 1 0 16 262.47 26.80 1 0 16 292.27 27.80 -1 0 -16 275.07 27.60 1 0 16 289.97 27.10 -1 0 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22 168.18 22.30 -16 -8 22 170.58 20.00 16 -8 -22 157.28 22.50 -16 8 22 173.58 21.00 -16 8 22 187.38 21.30 16 8 -22 173.08 26.80 15 -8 -22 39.40 10.10 -15 -8 22 55.99 10.60 -15 -8 22 38.10 8.00 -15 8 22 37.60 9.00 15 8 -22 48.00 12.70 -14 -8 22 4.80 6.50 14 -8 -22 3.80 6.10 -14 -8 22 6.00 4.10 14 8 -22 4.80 6.10 -14 8 22 4.40 5.80 -13 -8 22 223.88 27.30 13 -8 -22 218.78 27.30 -13 -8 22 214.28 25.20 -13 8 22 248.88 26.20 13 8 -22 228.08 31.80 -12 -8 22 5.30 6.40 -12 -8 22 3.10 4.00 12 -8 -22 8.30 6.00 12 8 -22 4.50 5.70 -12 8 22 3.70 5.80 -11 -8 22 69.89 10.10 -11 -8 22 79.79 12.40 11 -8 -22 52.89 10.90 11 8 -22 56.09 13.50 11 8 -22 90.79 14.00 -11 8 22 64.49 11.00 -10 -8 22 224.18 27.00 10 -8 -22 290.57 29.50 -10 -8 22 283.17 29.40 10 8 -22 256.97 28.30 -10 8 22 276.67 28.10 10 8 -22 237.58 30.80 9 -8 -22 3.20 5.60 9 -8 -22 8.80 8.70 -9 -8 22 -1.00 7.20 -9 -8 22 11.60 4.60 9 8 -22 9.80 6.10 -9 8 22 14.40 6.00 9 8 -22 12.50 7.50 -8 -8 22 528.95 53.49 8 -8 -22 463.05 53.79 -8 -8 22 505.75 50.79 8 -8 -22 584.14 52.89 8 8 -22 520.95 51.39 8 8 -22 508.05 54.79 -8 8 22 471.35 51.09 7 -8 -22 27.50 10.20 -7 -8 22 25.90 6.50 7 -8 -22 25.80 7.80 7 8 -22 17.60 8.80 7 8 -22 25.90 7.10 -7 8 22 15.90 6.20 6 -8 -22 53.29 10.80 -6 -8 22 48.60 8.90 6 -8 -22 69.09 13.90 6 8 -22 53.49 9.60 -6 8 22 43.00 9.60 6 8 -22 58.69 12.40 5 -8 -22 244.68 33.20 5 -8 -22 323.87 31.80 -5 -8 22 297.67 30.20 5 8 -22 262.37 30.50 -5 8 22 327.97 30.80 5 8 -22 307.77 33.70 -5 8 22 268.27 30.70 4 -8 -22 15.30 7.00 -4 -8 22 9.60 5.20 4 -8 -22 19.80 10.30 -4 8 22 12.70 5.40 4 8 -22 8.10 5.90 4 8 -22 17.70 6.20 -4 8 22 7.30 5.50 3 -8 -22 263.67 30.50 -3 -8 22 226.58 26.30 -3 8 22 227.78 26.70 3 8 -22 224.78 25.90 3 8 -22 246.48 28.50 -3 8 22 243.88 25.70 -2 -8 22 162.58 17.80 2 -8 -22 145.19 22.30 -2 8 22 143.69 17.60 2 8 -22 134.39 20.80 2 8 -22 138.59 17.80 -2 8 22 150.48 18.00 -1 -8 22 570.04 53.89 1 -8 -22 428.96 56.49 -1 8 22 541.15 53.89 1 8 -22 630.04 54.49 -1 8 22 538.45 53.89 0 -8 22 128.49 16.60 0 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82.79 14.70 15 -5 -23 115.09 16.70 -15 -5 23 120.29 13.80 15 -5 -23 124.29 16.90 -15 5 23 91.69 13.60 -15 5 23 128.49 17.10 15 5 -23 88.19 17.60 -15 5 23 118.59 14.00 14 -5 -23 15.20 6.80 14 -5 -23 10.80 8.20 14 -5 -23 11.10 9.50 -14 -5 23 17.90 5.30 -14 -5 23 25.30 8.20 -14 5 23 30.90 6.70 14 5 -23 19.70 9.90 14 5 -23 30.60 10.40 -14 5 23 21.40 7.90 -14 5 23 12.90 5.60 13 -5 -23 42.90 11.20 -13 -5 23 29.00 7.00 13 -5 -23 30.30 9.50 -13 -5 23 37.90 8.90 13 -5 -23 53.19 9.80 -13 5 23 42.70 7.90 13 5 -23 29.50 10.60 -13 5 23 38.60 8.60 -13 5 23 30.20 7.00 13 5 -23 30.00 10.10 -12 -5 23 18.10 5.40 -12 -5 23 15.70 6.90 12 -5 -23 17.10 7.60 12 -5 -23 11.70 6.00 12 5 -23 18.70 8.10 12 5 -23 24.10 8.80 -12 5 23 21.60 5.70 -12 5 23 18.30 6.10 -12 5 23 23.70 6.90 11 -5 -23 7.60 8.20 -11 -5 23 6.40 6.30 -11 -5 23 5.20 5.40 -11 -5 23 3.60 4.70 11 -5 -23 3.00 4.90 11 5 -23 0.10 4.90 11 5 -23 8.00 6.90 -11 5 23 2.50 4.90 -11 5 23 -0.80 4.20 -10 -5 23 126.59 15.50 10 -5 -23 140.49 17.40 -10 -5 23 132.39 15.70 10 -5 -23 163.08 20.60 -10 -5 23 130.99 17.00 -10 5 23 109.29 15.30 10 5 -23 120.39 18.10 -10 5 23 142.79 16.60 10 5 -23 90.29 17.70 -9 -5 23 24.20 8.10 -9 -5 23 23.20 6.10 9 -5 -23 32.90 9.80 9 -5 -23 19.90 7.00 -9 -5 23 18.00 5.80 9 5 -23 20.50 8.20 -9 5 23 32.40 6.90 -9 5 23 43.30 8.40 9 5 -23 31.90 8.70 -8 -5 23 239.18 26.90 8 -5 -23 236.08 28.30 8 -5 -23 268.77 30.30 -8 -5 23 244.28 26.90 -8 5 23 234.68 27.20 8 5 -23 351.26 32.10 -8 5 23 254.37 27.90 8 5 -23 260.87 29.70 7 -5 -23 113.99 17.60 -7 -5 23 124.79 14.10 7 -5 -23 107.39 15.20 -7 -5 23 110.39 13.80 -7 5 23 118.79 15.50 7 5 -23 106.09 17.60 7 5 -23 111.19 16.80 -7 5 23 89.89 13.70 -6 -5 23 21.40 5.60 6 -5 -23 16.10 6.50 -6 -5 23 19.70 5.20 6 -5 -23 12.90 6.60 6 5 -23 14.30 7.70 6 5 -23 9.10 5.70 6 5 -23 12.10 6.60 -6 5 23 15.40 5.20 -6 5 23 8.50 4.80 -5 -5 23 68.49 9.50 -5 -5 23 68.89 9.70 5 -5 -23 64.39 12.70 5 -5 -23 56.99 11.80 5 5 -23 63.59 12.30 5 5 -23 59.09 12.40 5 5 -23 79.09 11.10 -5 5 23 57.19 10.30 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31.00 -9 -5 -23 341.87 35.00 9 5 23 288.47 30.40 -9 5 -23 209.78 30.80 9 5 23 314.57 30.60 10 -5 23 166.78 21.40 -10 -5 -23 154.88 22.30 -10 -5 -23 197.88 26.70 -10 5 -23 175.08 22.20 10 5 23 184.98 21.90 -20 -6 23 8.00 7.70 20 -6 -23 5.00 8.20 -20 -6 23 -0.50 4.40 -20 6 23 1.40 5.40 20 6 -23 2.30 8.30 -20 6 23 2.60 5.30 19 -6 -23 348.57 36.30 -19 -6 23 312.97 35.40 -19 -6 23 351.56 33.70 19 6 -23 228.28 38.50 -19 6 23 376.36 34.10 -19 6 23 312.67 34.10 -18 -6 23 180.98 21.20 -18 -6 23 162.78 22.70 18 -6 -23 216.78 24.90 18 6 -23 169.58 26.70 -18 6 23 209.48 21.60 -18 6 23 156.58 21.10 -17 -6 23 325.27 30.80 -17 -6 23 307.17 32.50 17 -6 -23 276.37 32.70 -17 6 23 311.27 31.10 -17 6 23 234.98 30.90 16 -6 -23 292.77 34.20 -16 -6 23 342.37 32.60 -16 -6 23 309.07 34.10 -16 6 23 317.47 33.00 16 6 -23 292.77 36.90 -16 6 23 317.47 32.60 -15 -6 23 25.00 5.90 -15 -6 23 26.00 8.30 15 -6 -23 16.00 7.30 -15 6 23 28.70 7.10 15 6 -23 18.40 10.40 -15 6 23 34.30 7.90 -14 -6 23 245.08 23.40 14 -6 -23 221.38 26.70 -14 -6 23 216.18 26.20 -14 6 23 209.78 24.00 14 6 -23 182.18 28.10 -14 6 23 219.28 24.90 -13 -6 23 84.09 12.70 13 -6 -23 65.99 12.10 -13 -6 23 55.79 9.50 -13 6 23 54.19 10.10 13 6 -23 75.49 15.20 -12 -6 23 47.20 10.70 12 -6 -23 62.89 11.10 -12 -6 23 64.09 9.90 12 -6 -23 70.19 13.60 12 6 -23 67.19 13.80 -12 6 23 56.49 9.80 11 -6 -23 247.38 26.80 11 -6 -23 253.87 28.30 -11 -6 23 240.68 26.40 -11 -6 23 252.57 25.30 11 6 -23 162.98 28.70 -11 6 23 213.38 27.90 -11 6 23 270.17 25.90 10 -6 -23 12.40 5.80 10 -6 -23 6.40 6.80 -10 -6 23 1.30 4.40 -10 -6 23 1.10 5.60 10 6 -23 -1.90 5.90 -10 6 23 -1.50 5.00 -10 6 23 -0.90 7.00 -9 -6 23 237.78 30.40 9 -6 -23 309.47 32.30 -9 -6 23 294.17 29.20 9 -6 -23 287.77 30.70 -9 6 23 292.37 29.70 9 6 -23 250.77 32.30 -9 6 23 287.37 30.30 8 -6 -23 183.18 21.50 8 -6 -23 162.38 22.80 -8 -6 23 185.88 20.30 -8 -6 23 159.48 18.80 -8 6 23 137.49 18.90 8 6 -23 152.08 22.90 -8 6 23 167.88 20.30 7 -6 -23 275.27 26.60 -7 -6 23 199.98 21.80 -7 -6 23 161.28 22.10 7 -6 -23 174.68 23.60 7 6 -23 228.28 23.80 -7 6 23 183.68 23.80 -7 6 23 212.88 23.30 7 6 -23 194.38 26.80 6 -6 -23 153.18 18.60 -6 -6 23 131.09 16.20 -6 -6 23 141.79 16.70 6 -6 -23 116.39 19.70 -6 6 23 136.59 17.00 6 6 -23 124.89 20.60 -6 6 23 124.29 17.60 6 6 -23 181.48 18.20 -5 -6 23 22.00 6.40 5 -6 -23 38.00 10.10 5 -6 -23 27.40 8.10 -5 -6 23 27.50 6.60 5 6 -23 24.80 8.30 5 6 -23 41.50 7.90 -5 6 23 42.60 8.90 -5 6 23 32.60 7.10 4 -6 -23 285.37 33.40 -4 -6 23 290.17 29.80 -4 -6 23 287.67 29.90 4 6 -23 305.87 30.30 -4 6 23 295.17 31.40 4 6 -23 258.97 32.30 -4 6 23 290.07 30.20 3 -6 -23 147.79 22.50 -3 -6 23 138.49 18.30 -3 -6 23 163.18 18.70 -3 6 23 194.28 29.10 3 6 -23 179.58 23.50 3 6 -23 167.08 19.60 -3 6 23 164.18 19.30 -2 -6 23 29.90 7.10 -2 -6 23 22.50 6.70 2 -6 -23 30.60 9.80 2 6 -23 45.80 10.10 -2 6 23 40.30 7.90 2 6 -23 46.70 8.30 -1 -6 23 503.75 42.10 1 -6 -23 374.26 45.20 -1 -6 23 427.16 41.80 1 6 -23 405.26 42.30 -1 6 23 429.66 42.10 1 6 -23 359.26 43.80 0 -6 23 35.40 6.90 0 -6 23 26.60 6.80 0 -6 23 29.60 7.40 0 -6 -23 38.00 10.30 0 -6 -23 33.10 10.50 0 6 23 31.10 7.30 0 6 -23 34.20 7.80 0 6 -23 37.40 9.30 1 -6 23 637.44 65.69 1 -6 23 607.14 65.69 -1 -6 -23 754.32 69.29 1 -6 23 686.23 65.69 -1 -6 -23 655.23 69.79 -1 6 -23 684.03 66.59 1 6 23 660.83 66.09 1 6 23 624.54 65.89 -1 6 -23 704.03 68.49 2 -6 23 43.10 7.60 2 -6 23 29.70 6.80 -2 -6 -23 37.30 11.20 2 6 23 31.00 7.40 -2 6 -23 33.10 7.90 2 6 23 26.40 6.50 -3 -6 -23 280.67 30.20 3 -6 23 225.38 25.40 3 -6 23 215.88 25.30 3 6 23 193.88 25.30 -3 6 -23 216.88 26.10 3 6 23 234.78 24.70 4 -6 23 362.66 39.50 4 -6 23 363.16 39.80 -4 -6 -23 480.25 44.90 -4 6 -23 406.06 40.60 4 6 23 360.96 39.80 4 6 23 378.46 39.80 5 -6 23 46.30 8.80 5 -6 23 63.19 10.50 -5 -6 -23 54.19 12.80 5 6 23 68.79 10.10 -5 6 -23 57.99 9.90 5 6 23 44.00 9.50 6 -6 23 326.87 36.80 6 -6 23 321.17 36.30 -6 -6 -23 415.96 41.40 6 6 23 356.46 36.80 -6 6 -23 339.97 37.10 6 6 23 365.06 37.00 7 -6 23 180.98 19.10 -7 -6 -23 154.58 23.40 7 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10.00 4.90 -14 7 23 9.70 6.20 14 7 -23 4.10 7.10 13 -7 -23 146.79 19.10 -13 -7 23 153.78 18.80 -13 -7 23 130.79 15.90 -13 7 23 120.79 16.40 13 7 -23 101.79 19.30 -12 -7 23 120.79 19.10 12 -7 -23 204.68 23.00 -12 -7 23 204.98 22.60 -12 7 23 188.68 21.00 12 7 -23 168.68 25.00 -11 -7 23 16.20 5.20 -11 -7 23 18.00 7.90 11 -7 -23 21.00 9.30 11 -7 -23 40.40 8.70 11 7 -23 22.30 8.90 -11 7 23 7.70 6.30 -10 -7 23 94.69 12.60 10 -7 -23 109.49 16.80 10 -7 -23 104.29 15.10 -10 -7 23 75.59 14.20 -10 7 23 89.49 13.20 10 7 -23 101.69 17.30 -9 -7 23 6.00 4.90 9 -7 -23 19.70 6.60 9 -7 -23 15.90 7.80 -9 -7 23 12.20 7.80 -9 7 23 12.00 5.80 9 7 -23 11.40 7.10 -8 -7 23 184.98 23.80 8 -7 -23 243.58 25.20 8 -7 -23 214.48 26.70 8 7 -23 238.88 25.30 -8 7 23 199.08 24.40 8 7 -23 215.98 29.00 7 -7 -23 57.49 13.00 7 -7 -23 74.69 11.60 -7 -7 23 51.19 9.20 -7 7 23 51.99 9.90 7 7 -23 55.19 10.20 7 7 -23 64.09 13.00 -6 -7 23 14.50 5.90 6 -7 -23 18.00 9.00 6 -7 -23 18.50 7.00 6 7 -23 25.20 8.60 6 7 -23 21.10 6.40 -6 7 23 8.50 6.30 5 -7 -23 321.67 32.60 5 -7 -23 276.07 29.80 -5 -7 23 242.98 28.80 5 7 -23 264.87 28.40 -5 7 23 288.07 28.60 5 7 -23 215.68 30.50 4 -7 -23 23.60 9.20 -4 -7 23 20.20 6.00 4 7 -23 33.30 7.10 4 7 -23 19.60 7.50 -4 7 23 29.20 6.70 3 -7 -23 146.29 21.90 -3 -7 23 159.88 17.80 3 7 -23 169.88 22.20 -3 7 23 125.99 17.60 3 7 -23 141.69 18.10 -2 -7 23 257.57 28.80 2 -7 -23 281.77 33.00 2 7 -23 270.37 31.50 -2 7 23 294.17 29.40 2 7 -23 270.07 29.40 -1 -7 23 23.80 6.80 1 -7 -23 25.80 9.80 1 7 -23 28.30 7.10 -1 7 23 24.90 7.50 -1 7 23 24.90 6.90 1 7 -23 25.60 8.40 0 -7 -23 351.76 36.70 0 -7 23 265.27 31.30 0 7 -23 321.07 32.30 0 7 23 292.47 31.70 0 7 -23 267.17 34.60 0 7 23 328.27 32.00 -1 -7 -23 18.60 8.90 1 -7 23 9.20 6.40 1 7 23 9.40 5.60 1 7 23 18.60 5.80 -1 7 -23 8.20 5.80 2 -7 23 280.07 28.80 -2 -7 -23 331.07 34.40 2 7 23 258.77 28.80 -2 7 -23 235.68 30.00 2 7 23 254.97 28.70 -3 -7 -23 129.99 22.10 3 -7 23 162.08 18.10 3 7 23 126.09 17.20 -3 7 -23 146.69 18.70 3 7 23 154.08 18.30 4 -7 23 78.39 12.10 4 -7 23 90.89 12.70 -4 -7 -23 98.99 17.60 4 7 23 80.79 12.60 4 7 23 83.29 12.50 -4 7 -23 82.79 12.80 5 -7 23 304.87 33.00 5 -7 23 315.87 33.30 -5 -7 -23 297.27 37.90 5 7 23 331.87 33.50 -5 7 -23 309.37 33.90 5 7 23 343.77 33.50 -6 -7 -23 4.60 8.00 6 -7 23 6.40 6.30 6 -7 23 6.90 5.00 6 7 23 2.60 5.70 -6 7 -23 1.80 5.00 6 7 23 3.60 4.50 7 -7 23 265.87 29.40 -7 -7 -23 302.97 34.70 7 -7 23 284.67 30.90 7 7 23 221.58 30.30 7 7 23 287.77 30.10 -7 7 -23 301.47 30.50 -18 -8 23 31.60 7.50 -18 -8 23 36.20 10.00 -18 8 23 38.90 9.30 18 8 -23 31.00 12.20 -18 8 23 29.00 8.90 -17 -8 23 5.20 6.80 -17 -8 23 -2.30 4.00 17 -8 -23 4.40 6.60 17 8 -23 3.10 7.10 -17 8 23 7.40 6.50 -17 8 23 -2.70 7.40 -16 -8 23 21.70 7.10 -16 -8 23 28.90 9.00 16 -8 -23 31.20 8.90 -16 8 23 16.40 7.60 16 8 -23 22.90 10.30 -15 -8 23 2.00 6.50 15 -8 -23 8.10 6.90 -15 -8 23 6.30 4.40 -15 8 23 4.00 6.60 15 8 -23 5.80 7.20 14 -8 -23 71.69 13.40 -14 -8 23 74.19 13.20 -14 -8 23 92.99 11.90 14 8 -23 78.89 15.60 -14 8 23 62.09 11.30 13 -8 -23 68.59 12.20 -13 -8 23 65.99 9.90 -13 -8 23 48.80 11.00 13 8 -23 56.19 13.90 -13 8 23 53.99 10.30 -12 -8 23 31.90 6.90 12 -8 -23 33.30 9.00 -12 -8 23 35.60 9.30 -12 8 23 20.00 7.30 12 8 -23 24.90 10.00 -11 -8 23 61.39 10.10 -11 -8 23 81.99 13.10 11 -8 -23 82.69 13.20 -11 8 23 64.29 11.00 11 8 -23 78.59 15.50 -10 -8 23 0.00 3.60 -10 -8 23 6.10 7.30 10 -8 -23 2.60 5.40 -10 8 23 6.30 5.90 10 8 -23 -6.00 5.10 10 8 -23 -8.80 7.50 -9 -8 23 2.40 4.30 -9 -8 23 1.60 8.00 9 -8 -23 14.50 9.20 9 -8 -23 14.90 6.90 9 8 -23 10.10 7.20 9 8 -23 10.10 6.90 -9 8 23 1.10 5.30 8 -8 -23 32.20 8.70 -8 -8 23 22.70 6.30 8 -8 -23 24.70 9.50 8 8 -23 22.00 7.30 8 8 -23 28.20 9.20 -8 8 23 28.20 7.60 -7 -8 23 10.80 5.40 7 -8 -23 21.30 9.60 7 -8 -23 16.40 6.70 -7 8 23 14.90 6.50 7 8 -23 13.70 7.80 7 8 -23 14.90 13.60 6 -8 -23 94.19 14.80 -6 -8 23 77.79 12.80 6 -8 -23 124.99 19.10 -6 8 23 92.39 13.70 6 8 -23 95.09 16.70 6 8 -23 111.99 14.10 5 -8 -23 5.70 6.10 5 -8 -23 3.00 7.80 -5 -8 23 6.40 4.90 5 8 -23 2.70 5.10 -5 8 23 1.50 5.50 5 8 -23 7.80 5.50 4 -8 -23 376.86 43.30 4 -8 -23 336.77 35.70 -4 -8 23 287.57 30.90 4 8 -23 300.57 34.10 4 8 -23 282.37 31.40 -4 8 23 257.57 31.20 3 -8 -23 8.70 8.60 -3 -8 23 5.20 4.90 3 8 -23 3.90 4.90 -3 8 23 2.60 5.30 -3 8 23 5.60 5.30 3 8 -23 4.20 5.50 2 -8 -23 2.60 7.30 -2 -8 23 6.90 5.30 2 8 -23 0.50 4.40 2 8 -23 6.30 6.40 -2 8 23 5.60 5.00 -2 8 23 1.10 4.60 1 -8 -23 11.60 8.40 -1 -8 23 2.80 5.00 1 8 -23 11.00 5.80 -1 8 23 9.40 5.30 -1 8 23 5.70 5.60 0 -8 23 15.20 6.30 0 -8 -23 18.80 9.70 0 8 23 2.10 6.10 0 8 23 11.80 5.00 0 8 -23 14.50 6.30 -1 -8 -23 15.20 9.00 1 -8 23 9.20 5.80 1 8 23 2.80 5.00 1 8 23 0.00 6.70 -1 8 -23 3.40 5.50 2 -8 23 41.00 8.70 -2 -8 -23 23.00 10.10 -2 8 -23 31.50 7.90 2 8 23 33.00 8.30 2 8 23 39.80 8.60 3 -8 23 43.10 9.00 -3 -8 -23 39.20 12.40 3 8 23 52.19 9.00 3 8 23 33.70 8.10 -3 8 -23 35.00 8.70 -4 -8 -23 39.80 12.90 4 -8 23 33.50 7.90 4 8 23 27.00 8.10 4 8 23 37.40 8.00 -4 8 -23 25.90 7.90 5 -8 23 55.29 9.30 -5 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10.90 2 -5 25 36.10 8.60 2 -5 25 40.00 8.20 -2 5 -25 70.39 12.60 2 5 25 53.49 9.40 -2 5 -25 56.09 10.00 3 -5 25 4.60 6.70 -3 -5 -25 -0.10 5.90 3 -5 25 -1.70 4.30 3 5 25 7.60 5.00 -3 5 -25 3.30 5.80 4 -5 25 33.80 9.20 4 -5 25 29.80 6.20 -4 -5 -25 22.40 9.40 4 5 25 22.00 7.40 -4 5 -25 18.30 7.10 5 -5 25 18.10 5.90 -5 -5 -25 18.50 9.10 5 5 25 20.80 6.60 -5 5 -25 20.20 7.40 6 -5 25 125.69 15.80 -6 -5 -25 136.19 21.80 -6 5 -25 95.99 16.00 6 5 25 133.59 16.50 -7 -5 -25 41.00 12.00 7 -5 25 34.90 8.50 -7 5 -25 53.19 10.00 7 5 25 46.60 9.60 7 5 25 39.70 9.00 -18 -6 25 319.07 33.60 -18 -6 25 247.88 31.70 18 -6 -25 249.78 34.50 -18 6 25 279.07 31.40 -18 6 25 302.47 31.40 18 6 -25 357.36 37.70 -17 -6 25 275.97 27.70 17 -6 -25 246.58 29.50 17 6 -25 189.68 31.00 -17 6 25 225.98 25.90 -17 6 25 215.78 26.40 -16 -6 25 9.20 7.60 16 -6 -25 17.00 7.20 -16 -6 25 2.00 4.70 -16 6 25 10.30 5.70 -16 6 25 11.20 6.70 16 6 -25 12.50 9.30 15 -6 -25 504.25 48.10 -15 -6 25 437.56 47.20 -15 -6 25 456.85 45.70 15 6 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152.08 20.80 0 5 -27 189.88 25.10 1 -5 27 53.19 8.90 1 -5 27 48.20 9.70 -1 -5 -27 36.50 11.30 -1 5 -27 57.19 10.30 1 5 27 36.40 9.00 -1 5 -27 53.19 11.80 2 -5 27 8.40 5.00 -2 -5 -27 14.70 8.40 2 -5 27 18.10 9.00 -2 5 -27 18.60 7.50 2 5 27 18.60 6.70 -3 -5 -27 12.10 8.50 3 -5 27 2.50 4.80 -3 5 -27 11.50 6.90 3 5 27 14.80 6.90 -15 -6 27 19.90 6.90 -15 -6 27 18.90 9.10 15 -6 -27 32.50 9.60 -15 6 27 15.50 6.70 15 6 -27 24.00 9.40 14 -6 -27 155.98 20.60 -14 -6 27 128.09 18.20 -14 -6 27 146.69 20.50 -14 6 27 149.29 19.60 14 6 -27 173.28 25.20 -13 -6 27 357.86 39.30 13 -6 -27 365.86 41.30 13 -6 -27 437.06 43.90 -13 -6 27 390.96 41.50 -13 6 27 360.56 39.80 -12 -6 27 107.69 15.10 12 -6 -27 116.59 17.60 12 -6 -27 172.38 22.00 -12 6 27 99.79 15.90 12 6 -27 105.49 19.60 11 -6 -27 414.66 47.70 -11 -6 27 487.55 46.60 11 -6 -27 531.95 50.49 -11 6 27 379.66 46.30 11 6 -27 477.95 50.69 10 -6 -27 -1.90 6.30 -10 -6 27 4.60 5.30 10 -6 -27 -0.60 5.90 10 6 -27 2.10 5.70 -10 6 27 -0.40 5.50 9 -6 -27 650.03 59.59 -9 -6 27 543.55 55.09 9 -6 -27 584.54 57.29 9 6 -27 447.16 58.09 -8 -6 27 24.70 6.90 8 -6 -27 48.80 12.30 8 6 -27 35.50 10.40 -8 6 27 30.20 8.30 -7 -6 27 58.49 10.30 7 -6 -27 90.89 16.20 7 6 -27 68.49 13.60 -7 6 27 57.59 10.60 6 -6 -27 266.67 28.10 -6 -6 27 150.48 22.40 -6 6 27 220.98 24.40 6 6 -27 198.28 28.10 -5 -6 27 31.40 7.70 5 -6 -27 44.00 12.50 -5 6 27 22.30 7.80 5 6 -27 38.30 10.70 4 -6 -27 221.88 28.30 -4 -6 27 156.98 21.20 -4 6 27 157.58 21.60 4 6 -27 221.08 25.00 3 -6 -27 136.79 20.40 -3 -6 27 129.99 15.60 3 6 -27 125.29 16.90 3 6 -27 111.99 18.00 -3 6 27 87.49 14.70 2 -6 -27 281.77 29.90 -2 -6 27 205.18 24.50 2 6 -27 235.58 26.60 2 6 -27 185.98 28.00 -2 6 27 197.88 24.90 1 -6 -27 233.58 30.10 -1 -6 27 224.48 23.80 -1 6 27 188.48 23.50 1 6 -27 190.18 24.00 1 6 -27 187.48 27.20 0 -6 -27 32.10 11.60 0 -6 27 25.90 7.80 0 6 -27 38.90 11.20 0 6 -27 53.29 10.40 0 6 27 38.50 9.10 1 -6 27 297.57 29.70 1 -6 27 263.27 30.80 -1 -6 -27 213.68 34.50 -1 6 -27 298.17 30.50 1 6 27 298.57 30.00 -13 -7 27 122.79 15.60 -13 -7 27 123.69 18.20 13 7 -27 101.69 20.00 12 -7 -27 167.78 24.60 12 -7 -27 179.48 22.40 -12 -7 27 154.58 19.30 -12 7 27 147.29 20.10 12 7 -27 140.19 23.40 11 -7 -27 73.19 12.50 -11 -7 27 47.40 10.10 11 -7 -27 64.99 14.70 -11 7 27 57.09 10.90 11 7 -27 47.20 12.90 -10 -7 27 342.67 37.10 10 -7 -27 378.86 41.80 10 -7 -27 324.07 38.50 10 7 -27 400.86 41.80 -10 7 27 347.97 37.80 9 -7 -27 24.20 9.00 9 -7 -27 36.40 11.30 -9 -7 27 19.70 6.60 -9 7 27 9.10 6.60 9 7 -27 23.70 9.10 -8 -7 27 199.18 25.20 8 -7 -27 270.27 30.20 8 7 -27 221.48 31.10 7 -7 -27 136.19 21.00 -7 -7 27 91.59 14.00 7 7 -27 96.99 17.60 -7 7 27 102.79 14.90 -6 -7 27 32.80 8.70 6 -7 -27 50.19 13.70 6 7 -27 68.09 13.30 -6 7 27 40.60 9.40 5 -7 -27 221.08 28.50 -5 -7 27 180.28 22.60 5 7 -27 186.18 27.00 -4 -7 27 7.30 5.80 4 -7 -27 0.30 7.60 4 7 -27 2.70 6.20 -4 7 27 -2.20 5.90 4 7 -27 5.70 7.60 -3 -7 27 177.08 22.20 3 -7 -27 162.58 27.00 3 7 -27 191.58 26.70 -3 7 27 225.88 23.90 3 7 -27 219.78 24.20 2 -7 -27 65.19 15.80 -2 -7 27 78.99 11.80 -2 7 27 71.09 12.20 2 7 -27 73.29 14.50 2 7 -27 88.19 13.00 -1 -7 27 48.20 10.10 1 -7 -27 73.29 16.00 -1 7 27 68.49 11.50 1 7 -27 56.69 11.20 8 -8 -27 16.70 10.20 8 8 -27 19.30 8.40 -7 -8 27 6.10 5.50 7 -8 -27 -1.90 8.10 -7 8 27 1.30 6.00 7 8 -27 4.60 7.30 6 -8 -27 108.89 20.10 -6 -8 27 85.99 13.40 6 8 -27 92.39 17.50 18 0 -28 -0.10 5.90 18 0 -28 3.80 9.60 -18 0 28 3.00 5.10 -18 0 28 11.00 6.30 17 0 -28 222.68 30.20 -17 0 28 233.88 25.20 -17 0 28 228.38 25.10 17 0 -28 183.98 26.30 -16 0 28 109.49 14.80 -16 0 28 100.59 14.90 16 0 -28 123.39 17.20 16 0 -28 103.09 19.10 -15 0 28 43.30 8.80 15 0 -28 37.70 10.10 -15 0 28 41.40 9.00 15 0 -28 66.99 14.40 14 0 -28 589.74 70.39 -14 0 28 690.83 67.19 14 0 -28 694.93 68.69 -14 0 28 739.83 67.29 13 0 -28 10.70 8.80 13 0 -28 19.50 7.70 -13 0 28 10.00 5.70 -13 0 28 13.40 6.50 12 0 -28 585.94 61.39 -12 0 28 578.64 57.39 12 0 -28 651.63 59.09 -12 0 28 491.05 57.09 -11 0 28 263.37 28.90 -11 0 28 278.37 29.00 11 0 -28 274.77 33.30 -10 0 28 246.58 25.50 -10 0 28 210.38 25.20 10 0 -28 218.28 30.90 -9 0 28 478.55 49.80 -9 0 28 452.55 49.70 9 0 -28 564.64 54.69 8 0 -28 120.19 20.60 -8 0 28 128.79 16.30 -8 0 28 131.89 16.20 -7 0 28 397.56 39.50 7 0 -28 372.36 43.00 6 0 -28 238.88 28.50 -6 0 28 215.68 25.40 -5 0 28 242.88 27.00 5 0 -28 268.17 31.20 4 0 -28 384.16 43.10 -4 0 28 390.16 39.60 -3 0 28 2.30 4.80 3 0 -28 8.30 6.10 -2 0 28 412.36 40.40 2 0 -28 376.06 43.60 1 0 -28 11.60 6.80 -1 0 28 6.10 4.70 0 0 28 154.98 19.90 0 0 -28 183.18 24.60 -1 0 -28 15.30 6.80 1 0 28 6.90 4.60 2 0 28 0.70 4.70 -2 0 -28 0.20 5.80 3 0 28 123.19 17.80 -3 0 -28 172.78 23.10 4 0 28 12.80 4.90 -4 0 -28 14.40 8.10 18 -1 -28 208.48 30.20 -18 -1 28 232.78 25.80 18 1 -28 202.28 30.80 -18 1 28 227.98 25.40 -17 -1 28 7.20 5.70 17 -1 -28 -3.90 7.60 -17 -1 28 5.80 6.10 17 -1 -28 -4.60 5.00 -17 1 28 11.40 6.10 17 1 -28 7.40 6.70 17 1 -28 0.80 8.10 -17 1 28 -1.90 5.30 -16 -1 28 78.79 11.40 16 -1 -28 87.69 13.90 -16 -1 28 85.09 11.80 16 -1 -28 90.49 17.30 16 1 -28 50.59 12.50 -16 1 28 66.89 11.30 16 1 -28 74.59 15.80 -16 1 28 53.89 10.30 15 -1 -28 73.89 15.30 -15 -1 28 109.29 14.70 -15 -1 28 126.19 15.50 15 -1 -28 130.99 20.70 -15 1 28 114.19 15.00 15 1 -28 117.19 16.90 -15 1 28 91.09 14.40 15 1 -28 136.49 20.90 14 -1 -28 6.10 6.30 -14 -1 28 14.60 6.00 -14 -1 28 0.00 5.60 14 -1 -28 5.10 8.20 -14 1 28 10.50 5.40 14 1 -28 3.10 7.40 14 1 -28 10.00 7.00 -14 1 28 12.70 5.80 -13 -1 28 351.66 36.90 13 -1 -28 322.37 40.70 13 -1 -28 377.56 38.80 -13 -1 28 366.06 37.20 -13 1 28 312.77 36.80 -13 1 28 419.56 37.70 13 1 -28 380.56 38.90 -12 -1 28 51.79 9.50 12 -1 -28 68.69 11.90 -12 -1 28 55.79 9.60 12 -1 -28 57.99 13.00 -12 1 28 51.79 9.60 -12 1 28 35.50 8.60 12 1 -28 49.99 13.20 12 1 -28 59.89 11.90 11 -1 -28 132.79 20.70 11 -1 -28 134.59 18.20 -11 -1 28 118.99 15.10 -11 -1 28 111.59 15.10 -11 1 28 94.69 14.80 -11 1 28 132.69 15.60 11 1 -28 108.29 19.20 -10 -1 28 444.56 48.50 10 -1 -28 498.05 52.89 -10 -1 28 576.24 49.00 10 1 -28 485.55 52.49 -10 1 28 460.55 48.70 -10 1 28 443.96 48.70 9 -1 -28 100.29 17.00 -9 -1 28 114.39 13.10 -9 -1 28 82.49 11.50 9 1 -28 68.39 15.30 -9 1 28 71.69 11.80 -8 -1 28 196.88 21.60 -8 -1 28 204.38 21.60 8 -1 -28 176.08 25.70 -8 1 28 167.28 21.20 8 1 -28 178.98 26.00 -7 -1 28 22.00 7.30 -7 -1 28 32.00 6.70 7 -1 -28 29.80 10.20 7 1 -28 41.40 11.10 -7 1 28 15.10 6.10 -6 -1 28 318.97 31.00 -6 -1 28 293.37 30.40 6 -1 -28 308.17 34.50 -6 1 28 277.07 30.40 6 1 -28 264.17 33.70 -5 -1 28 145.19 17.40 5 -1 -28 125.29 20.30 -5 1 28 148.59 17.00 5 1 -28 130.09 20.80 -4 -1 28 30.90 8.00 4 -1 -28 33.30 10.00 -4 1 28 30.10 6.90 4 1 -28 37.20 10.40 -3 -1 28 346.97 36.50 3 -1 -28 382.86 40.50 -3 1 28 335.47 36.50 2 -1 -28 4.60 7.00 -2 -1 28 6.70 4.20 -2 1 28 2.40 4.00 2 1 -28 8.70 6.30 -1 -1 28 273.47 33.70 1 -1 -28 319.07 37.10 -1 1 28 333.27 34.20 1 1 -28 404.86 38.40 0 -1 -28 4.40 5.20 0 -1 28 4.70 4.00 0 1 28 6.50 5.20 0 1 -28 5.30 5.90 -1 -1 -28 76.69 14.60 1 -1 28 76.09 11.20 -1 1 -28 75.29 14.50 1 1 28 89.69 12.30 2 -1 28 111.99 14.20 -2 -1 -28 124.69 19.10 2 1 28 81.49 13.90 -2 1 -28 116.69 18.30 3 -1 28 0.30 4.40 -3 -1 -28 3.70 7.10 3 1 28 -3.90 4.50 -3 1 -28 7.60 6.00 17 -2 -28 33.90 11.90 17 -2 -28 42.20 9.90 -17 -2 28 26.00 7.60 -17 2 28 22.00 7.00 -17 2 28 28.80 8.10 17 2 -28 28.00 11.30 17 2 -28 34.60 10.40 16 -2 -28 5.40 6.60 16 -2 -28 9.50 8.80 -16 -2 28 8.80 6.30 -16 2 28 0.90 4.70 16 2 -28 5.90 8.70 -16 2 28 9.00 6.80 16 2 -28 9.30 6.60 15 -2 -28 0.60 7.10 15 -2 -28 -2.30 5.90 -15 -2 28 13.10 5.90 15 2 -28 -0.20 7.70 -15 2 28 8.20 5.30 15 2 -28 2.70 6.50 -15 2 28 6.80 6.40 -14 -2 28 2.50 5.00 14 -2 -28 -2.20 6.70 -14 -2 28 -2.70 5.60 14 -2 -28 -0.60 5.60 -14 2 28 -3.70 4.80 -14 2 28 5.20 6.00 14 2 -28 -4.70 6.20 14 2 -28 15.70 9.60 -13 -2 28 47.90 9.20 13 -2 -28 57.99 13.80 -13 -2 28 26.80 8.30 13 -2 -28 47.30 10.50 13 2 -28 66.09 14.50 -13 2 28 62.69 10.50 13 2 -28 47.30 10.90 -13 2 28 44.30 9.20 12 -2 -28 -2.40 5.80 -12 -2 28 -2.10 5.00 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385.36 45.80 -14 -4 28 445.96 44.00 14 -4 -28 401.76 45.80 14 -4 -28 447.26 48.10 14 4 -28 438.36 48.80 -14 4 28 456.15 44.30 13 -4 -28 97.69 17.50 -13 -4 28 99.19 16.10 -13 -4 28 73.59 11.90 13 -4 -28 77.09 13.90 -13 4 28 83.99 12.90 13 4 -28 76.59 16.40 12 -4 -28 517.05 49.99 12 -4 -28 567.84 52.69 -12 -4 28 418.76 47.60 -12 4 28 451.55 48.00 12 4 -28 422.16 51.49 11 -4 -28 346.37 37.10 -11 -4 28 308.47 32.40 11 -4 -28 320.67 34.40 11 4 -28 279.27 36.00 -11 4 28 298.37 32.80 10 -4 -28 151.68 21.40 10 -4 -28 216.38 25.40 -10 -4 28 126.39 17.40 -10 4 28 142.89 18.40 10 4 -28 117.49 21.60 9 -4 -28 471.85 49.10 -9 -4 28 438.36 44.70 -9 4 28 392.86 44.70 9 4 -28 465.95 48.90 -8 -4 28 8.10 5.70 8 -4 -28 8.60 8.00 -8 4 28 2.60 5.10 8 4 -28 7.00 6.80 -7 -4 28 572.94 54.09 7 -4 -28 523.35 57.39 7 4 -28 554.64 57.69 -7 4 28 501.95 54.29 -6 -4 28 123.39 15.30 6 -4 -28 119.79 19.60 -6 -4 28 123.99 15.40 6 4 -28 111.29 19.00 -6 4 28 109.99 15.50 5 -4 -28 178.88 27.20 -5 -4 28 245.48 23.50 -5 -4 28 183.78 22.70 5 4 -28 223.88 25.90 -5 4 28 174.08 22.90 -4 -4 28 511.65 47.10 -4 -4 28 479.15 47.00 4 4 -28 410.76 49.90 -4 4 28 462.95 47.30 -3 -4 28 69.69 9.90 3 -4 -28 50.49 13.20 -3 -4 28 47.30 9.40 3 4 -28 56.89 12.00 -3 4 28 49.99 9.10 -2 -4 28 294.27 29.50 2 -4 -28 312.77 34.50 -2 -4 28 286.77 29.90 -2 4 28 219.48 30.00 2 4 -28 279.47 32.90 -1 -4 28 9.80 7.40 -1 -4 28 19.80 6.10 1 -4 -28 10.90 8.30 1 4 -28 13.10 7.20 -1 4 28 -0.10 5.30 0 -4 -28 499.45 47.40 0 -4 28 376.56 41.90 0 4 -28 370.26 44.90 0 4 28 436.96 42.80 1 -4 28 33.00 7.90 -1 -4 -28 47.80 12.10 -1 4 -28 40.80 10.40 1 4 28 21.80 7.60 -1 4 -28 27.40 9.50 -2 -4 -28 107.79 19.10 -2 4 -28 122.19 16.20 -2 4 -28 87.49 16.50 -14 -5 28 8.90 6.50 14 -5 -28 26.00 8.40 14 -5 -28 28.80 11.30 -14 -5 28 23.70 9.80 -14 5 28 25.40 7.00 14 5 -28 20.90 8.30 13 -5 -28 306.17 29.90 -13 -5 28 195.18 27.30 13 -5 -28 264.17 34.10 -13 -5 28 323.37 32.40 -13 5 28 243.18 28.30 13 5 -28 208.68 32.50 -12 -5 28 26.20 7.10 12 -5 -28 35.70 9.80 12 -5 -28 26.60 10.40 -12 5 28 31.50 7.90 12 5 -28 24.30 9.60 11 -5 -28 307.37 34.80 11 -5 -28 347.47 33.30 -11 -5 28 277.47 30.30 11 5 -28 282.27 34.20 -11 5 28 229.68 31.00 -10 -5 28 174.88 22.60 10 -5 -28 203.98 27.40 10 -5 -28 237.78 26.40 -10 5 28 192.18 23.50 10 5 -28 182.98 27.40 9 -5 -28 67.09 14.20 -9 -5 28 70.69 10.70 -9 5 28 50.59 10.60 9 5 -28 70.19 14.50 8 -5 -28 352.06 38.70 -8 -5 28 354.76 34.90 8 5 -28 306.87 37.90 -8 5 28 320.87 35.10 -7 -5 28 24.60 6.60 7 -5 -28 17.90 8.40 -7 5 28 13.30 6.50 7 5 -28 27.90 9.80 -6 -5 28 354.66 36.50 6 -5 -28 384.86 40.90 -6 5 28 363.96 37.10 6 5 -28 320.57 39.70 5 -5 -28 70.39 15.20 -5 -5 28 90.49 11.70 -5 5 28 70.19 11.90 5 5 -28 72.09 14.60 -4 -5 28 61.69 10.70 4 -5 -28 67.89 14.70 -4 5 28 68.99 11.10 4 5 -28 66.39 13.80 -3 -5 28 183.88 19.90 3 -5 -28 165.08 24.50 -3 5 28 128.09 19.00 3 5 -28 170.58 24.40 -2 -5 28 9.70 6.00 -2 -5 28 11.80 6.70 2 -5 -28 7.40 8.60 2 5 -28 2.70 5.80 -2 5 28 3.80 5.70 -1 -5 28 129.79 15.00 1 -5 -28 93.59 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197.68 21.40 -11 1 29 185.58 21.30 11 1 -29 186.48 25.80 10 -1 -29 8.20 7.10 -10 -1 29 0.70 5.60 -10 -1 29 -4.70 3.90 10 1 -29 -4.80 6.10 -10 1 29 -4.40 4.20 -9 -1 29 182.68 23.00 -9 -1 29 186.68 23.10 9 -1 -29 224.28 29.00 -9 1 29 221.18 23.90 9 1 -29 204.18 28.50 -8 -1 29 60.69 10.10 -8 -1 29 55.89 9.70 8 -1 -29 76.29 15.20 8 1 -29 56.99 17.40 -8 1 29 39.30 8.80 -7 -1 29 160.08 17.40 7 -1 -29 155.58 22.70 -7 -1 29 148.89 17.00 7 1 -29 105.09 19.10 -7 1 29 108.79 15.80 6 -1 -29 327.87 38.80 -6 -1 29 359.96 34.90 -6 1 29 318.27 34.60 6 1 -29 331.27 38.70 5 -1 -29 59.89 13.80 -5 -1 29 37.60 8.20 -5 1 29 48.20 8.60 5 1 -29 68.49 13.60 4 -1 -29 168.78 25.20 -4 -1 29 140.69 19.60 4 1 -29 175.88 25.10 -4 1 29 201.98 20.90 -3 -1 29 162.88 20.40 3 -1 -29 185.38 25.50 3 1 -29 185.28 25.40 -3 1 29 160.48 20.30 -2 -1 29 60.69 10.00 2 -1 -29 72.09 14.10 -2 1 29 55.99 9.90 2 1 -29 59.89 13.30 1 -1 -29 170.68 25.90 -1 -1 29 191.08 22.10 -1 1 29 157.98 21.70 1 1 -29 242.18 26.00 0 -1 -29 120.59 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17.50 6.40 14 -3 -29 19.10 8.10 -14 -3 29 11.20 6.10 14 -3 -29 29.70 11.20 14 3 -29 8.40 8.10 -14 3 29 12.20 8.50 14 3 -29 12.70 9.80 -14 3 29 18.30 5.90 13 -3 -29 123.09 20.60 -13 -3 29 126.79 16.20 13 -3 -29 125.09 18.60 -13 3 29 126.39 16.50 13 3 -29 105.49 20.60 13 3 -29 162.88 23.30 12 -3 -29 42.40 11.10 12 -3 -29 50.49 13.60 -12 -3 29 38.90 8.60 12 3 -29 59.39 14.20 -12 3 29 36.40 8.30 -11 -3 29 130.69 15.60 11 -3 -29 111.29 19.00 11 3 -29 78.99 17.00 -11 3 29 124.79 15.60 -10 -3 29 -3.00 5.10 -10 -3 29 4.30 6.80 10 -3 -29 0.50 7.00 -10 3 29 -1.20 5.50 10 3 -29 1.00 6.70 -9 -3 29 334.77 34.20 9 -3 -29 326.57 38.00 -9 -3 29 331.27 34.30 -9 3 29 316.87 34.30 9 3 -29 327.37 38.10 -8 -3 29 113.79 15.80 8 -3 -29 135.29 21.30 -8 -3 29 146.69 16.40 8 3 -29 135.99 20.90 -8 3 29 101.99 15.60 -7 -3 29 169.58 20.40 7 -3 -29 149.29 25.10 -7 -3 29 150.88 20.00 7 3 -29 215.88 26.90 -7 3 29 186.78 21.00 -6 -3 29 370.76 39.00 -6 -3 29 379.36 39.20 6 -3 -29 419.26 43.70 -6 3 29 361.26 39.20 6 3 -29 374.66 42.80 -5 -3 29 95.99 12.80 -5 -3 29 86.09 12.70 5 -3 -29 93.19 16.90 -5 3 29 80.89 12.80 5 3 -29 80.99 15.80 -4 -3 29 316.87 31.40 -4 -3 29 264.87 31.80 4 -3 -29 338.67 35.90 -4 3 29 270.37 31.10 4 3 -29 289.97 34.70 3 -3 -29 76.39 15.00 -3 -3 29 59.79 10.10 3 3 -29 77.69 14.60 -3 3 29 54.19 10.10 2 -3 -29 36.50 10.50 -2 -3 29 16.50 5.90 2 3 -29 22.80 9.20 -2 3 29 27.90 7.50 -1 -3 29 131.99 15.70 1 -3 -29 110.59 19.50 -1 3 29 101.89 15.20 1 3 -29 126.79 19.40 0 -3 -29 21.90 8.90 0 -3 29 20.00 6.40 0 3 29 20.20 7.00 0 3 -29 42.00 11.20 13 -4 -29 12.60 7.20 -13 -4 29 19.60 7.00 13 -4 -29 24.20 10.60 -13 4 29 8.80 5.90 13 4 -29 20.60 9.60 12 -4 -29 20.30 8.40 -12 -4 29 16.70 6.50 12 -4 -29 24.20 10.30 12 4 -29 14.20 8.10 -12 4 29 20.50 6.90 11 -4 -29 -1.30 8.20 11 -4 -29 -3.30 6.80 -11 -4 29 2.30 5.50 -11 4 29 -0.90 5.10 11 4 -29 0.70 6.10 10 -4 -29 0.40 6.90 -10 -4 29 1.70 5.20 10 4 -29 14.00 8.40 -10 4 29 10.30 5.10 -9 -4 29 3.80 4.90 9 -4 -29 5.90 6.80 -9 4 29 9.10 5.60 9 4 -29 2.70 6.30 -8 -4 29 106.19 14.90 8 -4 -29 121.99 19.90 -8 4 29 100.79 14.90 8 4 -29 117.29 19.50 -7 -4 29 45.30 9.00 7 -4 -29 48.50 12.40 -7 4 29 38.60 8.30 7 4 -29 34.50 11.30 6 -4 -29 -7.50 5.80 -6 -4 29 4.60 6.00 -6 -4 29 -4.30 5.20 -6 4 29 8.90 5.80 6 4 -29 0.10 6.00 -5 -4 29 23.40 7.00 -5 -4 29 23.30 6.80 5 -4 -29 33.90 10.70 5 4 -29 27.10 9.90 -5 4 29 18.60 7.00 -4 -4 29 -6.10 5.50 -4 -4 29 0.00 4.10 4 -4 -29 4.70 6.90 -4 4 29 -4.30 4.70 4 4 -29 0.60 5.10 -3 -4 29 1.70 6.20 -3 -4 29 2.00 3.90 3 -4 -29 3.00 7.00 3 4 -29 0.90 5.30 -3 4 29 1.50 5.20 2 -4 -29 2.00 7.90 -2 -4 29 -0.30 4.40 -2 -4 29 8.00 7.30 2 4 -29 6.40 6.90 -2 4 29 5.50 5.80 1 -4 -29 4.00 6.70 1 4 -29 2.60 7.50 -11 -5 29 194.28 25.00 11 -5 -29 258.17 31.80 11 -5 -29 266.97 29.10 -11 5 29 158.98 24.70 11 5 -29 267.37 29.90 -10 -5 29 12.40 5.90 10 -5 -29 19.30 9.30 10 5 -29 9.20 7.10 -10 5 29 17.00 6.20 9 -5 -29 70.59 15.00 -9 -5 29 71.69 11.10 9 5 -29 69.89 14.70 -9 5 29 54.09 11.30 -8 -5 29 46.60 9.80 8 -5 -29 62.79 13.60 -8 5 29 50.29 9.90 8 5 -29 57.19 13.40 7 -5 -29 1.20 7.10 -7 -5 29 8.90 6.00 -7 5 29 2.20 5.80 7 5 -29 2.30 6.50 6 -5 -29 156.88 21.50 -6 -5 29 82.09 13.30 6 5 -29 85.79 17.20 -6 5 29 91.39 13.90 5 -5 -29 6.00 8.00 -5 -5 29 0.50 5.70 5 5 -29 -2.00 4.60 -5 5 29 9.20 5.90 -4 -5 29 127.09 15.80 4 -5 -29 158.98 23.20 -4 5 29 80.19 15.20 4 5 -29 144.39 21.50 -13 0 30 201.28 24.10 13 0 -30 184.28 28.70 -13 0 30 238.78 24.60 12 0 -30 36.50 11.90 -12 0 30 37.10 8.70 -12 0 30 54.39 10.20 11 0 -30 545.95 53.49 -11 0 30 400.76 47.90 -11 0 30 504.35 48.60 -10 0 30 200.08 23.80 -10 0 30 177.68 23.20 10 0 -30 255.47 31.10 -9 0 30 89.39 13.20 9 0 -30 91.39 17.50 8 0 -30 597.74 58.29 -8 0 30 473.95 52.99 -7 0 30 0.80 4.20 7 0 -30 0.80 6.20 6 0 -30 270.37 31.00 -6 0 30 217.68 27.00 5 0 -30 391.56 45.30 -5 0 30 423.76 41.80 -4 0 30 60.49 9.80 4 0 -30 42.20 11.60 3 0 -30 637.14 67.39 2 0 -30 -0.70 6.00 -2 0 30 -3.10 4.20 -13 -1 30 80.29 12.00 13 -1 -30 82.19 14.60 13 -1 -30 68.09 15.10 -13 -1 30 70.39 11.50 -13 1 30 75.49 11.50 -13 1 30 93.29 12.60 13 1 -30 48.10 13.60 -12 -1 30 219.88 24.30 12 -1 -30 198.88 29.30 -12 -1 30 212.08 23.90 -12 1 30 162.98 23.00 -12 1 30 213.68 24.00 12 1 -30 236.98 29.80 -11 -1 30 37.40 7.80 -11 -1 30 23.50 7.40 11 -1 -30 50.99 12.80 11 1 -30 35.50 11.50 -11 1 30 17.60 7.70 10 -1 -30 52.09 13.10 -10 -1 30 36.40 8.80 -10 -1 30 39.20 8.30 -10 1 30 26.90 7.80 10 1 -30 59.19 13.50 -9 -1 30 145.29 18.60 -9 -1 30 136.29 17.90 9 -1 -30 157.78 23.80 9 1 -30 165.88 24.40 -9 1 30 140.19 18.50 -8 -1 30 6.00 5.30 -8 -1 30 5.00 7.30 8 -1 -30 1.50 6.80 8 1 -30 7.50 6.50 -8 1 30 1.30 4.20 7 -1 -30 154.98 24.40 -7 -1 30 186.28 20.60 7 1 -30 153.78 24.20 -7 1 30 180.28 20.30 -6 -1 30 62.69 10.20 6 -1 -30 57.89 14.00 6 1 -30 77.59 15.00 -6 1 30 57.39 10.40 -5 -1 30 0.90 5.10 5 -1 -30 11.00 7.00 5 1 -30 3.80 6.90 -5 1 30 5.30 5.20 4 -1 -30 347.47 44.80 4 1 -30 485.85 46.60 -4 1 30 402.16 41.70 3 -1 -30 74.09 14.10 -3 -1 30 49.99 9.90 3 1 -30 63.59 13.80 -3 1 30 49.40 9.80 2 -1 -30 336.77 35.60 -2 -1 30 259.37 30.80 2 1 -30 282.87 34.60 -2 1 30 298.47 31.10 -12 -2 30 -0.70 5.90 -12 -2 30 12.60 6.00 12 -2 -30 -2.80 6.50 -12 2 30 -4.50 5.30 12 2 -30 7.80 9.30 -11 -2 30 5.20 5.70 -11 -2 30 11.00 5.80 11 -2 -30 7.00 8.50 -11 2 30 7.70 5.80 11 2 -30 4.20 8.20 -10 -2 30 17.40 6.30 -10 -2 30 8.60 6.10 10 -2 -30 -1.00 7.60 10 2 -30 -5.40 4.50 -10 2 30 -5.10 4.00 -9 -2 30 10.30 5.00 9 -2 -30 2.10 7.20 -9 -2 30 5.40 6.60 9 2 -30 1.20 6.80 -9 2 30 -2.20 4.90 -8 -2 30 20.70 7.50 8 -2 -30 28.90 11.20 -8 -2 30 35.30 7.50 -8 2 30 27.00 7.20 8 2 -30 33.40 10.20 -7 -2 30 4.50 4.70 7 -2 -30 0.70 7.70 -7 -2 30 5.20 6.60 -7 2 30 -1.00 5.30 7 2 -30 6.00 6.50 6 -2 -30 -1.80 6.70 -6 -2 30 4.90 4.80 -6 -2 30 -0.40 9.30 6 2 -30 -5.00 4.70 -6 2 30 6.80 4.90 -5 -2 30 2.00 5.00 5 -2 -30 0.40 6.60 -5 2 30 4.70 4.70 5 2 -30 -2.40 4.90 4 -2 -30 36.90 11.10 -4 -2 30 61.29 9.70 4 2 -30 58.69 13.20 -4 2 30 49.99 9.90 -3 -2 30 -3.50 4.20 3 -2 -30 -0.70 5.50 -3 2 30 4.90 4.30 3 2 -30 2.50 6.10 -11 -3 30 179.08 20.50 11 -3 -30 181.58 26.10 11 3 -30 147.29 24.90 -11 3 30 170.38 21.10 -10 -3 30 151.18 18.60 10 -3 -30 199.78 25.90 10 3 -30 127.39 22.20 -10 3 30 142.39 18.90 9 -3 -30 109.69 18.80 -9 -3 30 105.99 12.90 -9 -3 30 55.29 11.50 9 3 -30 96.89 17.30 -9 3 30 75.49 11.80 -8 -3 30 6.70 5.60 -8 -3 30 -4.70 5.10 8 -3 -30 5.80 8.30 -8 3 30 1.70 7.20 8 3 -30 -1.10 5.40 7 -3 -30 118.69 19.70 -7 -3 30 108.79 14.40 -7 -3 30 83.59 13.40 -7 3 30 104.59 13.90 7 3 -30 103.39 18.80 6 -3 -30 59.69 14.60 -6 -3 30 68.09 10.20 -6 -3 30 76.49 11.40 6 3 -30 61.09 14.40 -6 3 30 56.39 10.30 5 -3 -30 90.89 16.70 -5 -3 30 102.19 13.60 -5 -3 30 57.69 11.40 -5 3 30 93.19 13.20 5 3 -30 97.69 17.20 4 -3 -30 128.09 22.00 -4 -3 30 150.68 18.50 -4 3 30 161.98 19.00 4 3 -30 164.58 23.50 0 0 0 0.00 0.00 _computing_structure_solution 'SHELXT 2018/2 (Sheldrick, 2018)' _chemical_name_common '4-Fe' _chemical_formula_moiety ) C44 H36 Au F6 Fe N5 O4 P2 S2, 2(C2 F6 N O4 S2), C7 H8, C H2 Cl2 ) _exptl_absorpt_correction_type 'multi-scan' _exptl_absorpt_correction_T_max 0.6465 _exptl_absorpt_correction_T_min 0.4617 _exptl_absorpt_process_details 'SADABS' _cell_measurement_reflns_used 9981 _cell_measurement_theta_min 2.30 _cell_measurement_theta_max 26.34 _exptl_crystal_description 'block' _exptl_crystal_colour 'yellow' _diffrn_radiation_source 'microsource' _diffrn_radiation_monochromator 'multilayer-optics' _diffrn_measurement_device_type 'CCD area detector' _diffrn_measurement_method 'omega scans' _computing_data_collection 'SMART (Bruker, 2001)' _computing_cell_refinement 'SMART' _computing_data_reduction 'SAINT-PLUS (Bruker, 2009)' _computing_structure_solution 'SHELXT 2018/2 (Sheldrick, 2018)' _computing_structure_refinement 'SHELXL-2018/3 (Sheldrick, 2018)' _computing_molecular_graphics 'PLATON (Spek, 2009)' _computing_publication_material 'SHELXL2018' _atom_sites_solution_primary dual ; _shelx_hkl_checksum 30621